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Magnetic and Structural Properties of Novel-Coated Ni0.5Co0.5Fe1.6Gd0.2Mo0.1Sm0.1O4 Spinel Ferrite Nanomaterial: Experimental and Theoretical Investigations

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Abstract

The fabrication of magnetic coated nanoparticles in a single step is a challenge for nanotechnology applications. In this paper, Ni0.5Co0.5Fe1.6Gd0.2Mo0.1Sm0.1O4 nanoparticles coated with oleic acid were prepared by the one-step co-precipitation method for the first time. The thermal behavior of the obtained precipitate (uncalcined powder) was studied by TGA and DSC analysis. X-ray diffraction (XRD) shows the formation of a pure phase of oleic acid–coated spinel structure nanoparticles with a crystallite size of 23 nm. Rietveld refinement analysis shows a group space of Fd-3 m. The cation distribution analysis shows the formation of a mixed structure. Infrared spectroscopy analysis (FTIR) shows the formation of crystallographic sites of the spinel structure and that the nanoparticles are coated with a single layer of oleic acid. The morphology analysis indicates the formation of spherical nanoparticles with different sizes. Magnetic measurements were performed at three different temperatures 5, 80, and 300 K and show promising magnetic properties in terms of magnetization and coercivity. Density functional theory (DFT) calculations were also performed in this work on undoped and Mo-, Sm-, and Gd-doped Ni-Co ferrite systems to get an insight into the electronic structure of these systems. These results demonstrate that these nanoparticles can be used in several nanotechnological applications, including wireless communication technology.

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  1. Nanoscience and Nanotechnology Unit, E.N.S Rabat, Energy Research Centre, Mohammed V University, B.P. 5118, Takaddoum Rabat, Morocco

    A. Hssaini, M. Belaiche, M. Elansary, C. Ahmani Ferdi & Y. Mouhib

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  1. A. Hssaini
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  2. M. Belaiche
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Hssaini, A., Belaiche, M., Elansary, M. et al. Magnetic and Structural Properties of Novel-Coated Ni0.5Co0.5Fe1.6Gd0.2Mo0.1Sm0.1O4 Spinel Ferrite Nanomaterial: Experimental and Theoretical Investigations. J Supercond Nov Magn 35, 2799–2820 (2022). https://doi.org/10.1007/s10948-022-06307-4

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