Volume 399, Issue 2 | Analytical and Bioanalytical Chemistry

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Volume 399, Issue 2

January 2011

Heparin Characterization (pp. 525-794)

45 articles in this issue

New developments in the characterization of heparin and its impurities
Cynthia K. Larive
Editorial Open access 30 November 2010 Pages: 525 - 526
Analysis and characterization of heparin impurities
Szabolcs Beni
John F. K. Limtiaco
Cynthia K. Larive
Review Open access 03 September 2010 Pages: 527 - 539
Hyphenated techniques for the analysis of heparin and heparan sulfate
Bo Yang
Kemal Solakyildirim
Robert J. Linhardt
Review 19 September 2010 Pages: 541 - 557
Applications of isotopes in advancing structural and functional heparanomics
Vy M. Tran
Thao K. N. Nguyen
Balagurunathan Kuberan
Review 14 September 2010 Pages: 559 - 570
Electrochemical heparin sensing at liquid/liquid interfaces and polymeric membranes
Shigeru Amemiya
Yushin Kim
Benjamin Kabagambe
Review 05 August 2010 Pages: 571 - 579
Characterization of currently marketed heparin products: key tests for quality assurance
David A. Keire
Hongping Ye
Ali Al-Hakim
Paper in forefront 01 August 2010 Pages: 581 - 591
NMR methods to monitor the enzymatic depolymerization of heparin
John F. K. Limtiaco
Szabolcs Beni
Cynthia K. Larive
Paper in Forefront Open access 04 September 2010 Pages: 593 - 603
Comparison of established and novel purity tests for the quality control of heparin by means of a set of 177 heparin samples
Susanne Alban
Susanne Lühn
Ulrike Holzgrabe
Original Paper 08 September 2010 Pages: 605 - 620
¹H NMR signal at 2.10 ppm in the spectrum of KMnO₄-bleached heparin sodium: identification of the chemical origin using an NMR-only approach
E. Kellenbach
K. Sanders
F. C. Girard
Original Paper 11 November 2010 Pages: 621 - 628
Quantification of chondroitin sulfate and dermatan sulfate in danaparoid sodium by ¹H NMR spectroscopy and PLS regression
B. Üstün
K. B. Sanders
E. R. Kellenbach
Original Paper 23 September 2010 Pages: 629 - 634
Determination of galactosamine impurities in heparin samples by multivariate regression analysis of their ¹H NMR spectra
Qingda Zang
David A. Keire
William J. Welsh
Original Paper 16 October 2010 Pages: 635 - 649
NMR of heparin API: investigation of unidentified signals in the USP-specified range of 2.12–3.00 ppm
Sarah E. Lee
Edward K. Chess
Edwin G. Moore
Original Paper 15 October 2010 Pages: 651 - 662
Determination of the primary structure and carboxyl pK _As of heparin-derived oligosaccharides by band-selective homonuclear-decoupled two-dimensional ¹H NMR
Khanh Nguyen
Dallas L. Rabenstein
Original Paper Open access 03 October 2010 Pages: 663 - 671
Simple fluorescence assay for quantification of OSCS in heparin
Susanne Lühn
Simone Schiemann
Susanne Alban
Original Paper 16 June 2010 Pages: 673 - 680
Combination of a two-step fluorescence assay and a two-step anti-Factor Xa assay for detection of heparin falsifications and protein in heparins
Susanne Alban
Susanne Lühn
Simone Schiemann
Original Paper 16 October 2010 Pages: 681 - 690
Comparative study of Factor Xa fluorogenic substrates and their influence on the quantification of LMWHs
Vanessa Castro-López
Leanne F. Harris
Anthony J. Killard
Original Paper 24 October 2010 Pages: 691 - 700
The use of circular dichroism as a simple heparin-screening strategy
F. E. Stanley
A. M. Stalcup
Original Paper 16 October 2010 Pages: 701 - 706
The development of an FIA-CD strategy for screening sulfated polysaccharides using antimalarial drugs and related species as probes
F. E. Stanley
A. M. Warner
A. M. Stalcup
Original Paper 13 October 2010 Pages: 707 - 716
Development and qualification of a size exclusion chromatography coupled with multiangle light scattering method for molecular weight determination of unfractionated heparin
John Beirne
Hilary Truchan
Lin Rao
Original Paper 14 September 2010 Pages: 717 - 725
Targeted analysis of glycomics liquid chromatography/mass spectrometry data
Jonathan M. Dreyfuss
Christopher Jacobs
Joseph Zaia
Original Paper 16 October 2010 Pages: 727 - 735
Analysis of E. coli K5 capsular polysaccharide heparosan
Mellisa Ly
Zhenyu Wang
Robert J. Linhardt
Original Paper 21 April 2010 Pages: 737 - 745
New developments in quantitative polymerase chain reaction applied to control the quality of heparins
Cécile Auguste
Stéphanie Dereux
Pascal Anger
Original Paper 08 October 2010 Pages: 747 - 755
A quantitative PCR method to quantify ruminant DNA in porcine crude heparin
Sean P. Concannon
P. Brett Wimberley
Wesley E. Workman
Original Paper Open access 07 November 2010 Pages: 757 - 762
Protamine neutralisation of low molecular weight heparins and their oligosaccharide components
Mette Schroeder
John Hogwood
Kristian B. Johansen
Original Paper 05 October 2010 Pages: 763 - 771
Heparin-immobilized microspheres for the capture of cytokines
Jia Duo
Julie A. Stenken
Original Paper 09 September 2010 Pages: 773 - 782
In vitro and in vivo affinity microdialysis sampling of cytokines using heparin-immobilized microspheres
Jia Duo
Julie A. Stenken
Original Paper 30 October 2010 Pages: 783 - 793
Application of fully automated online solid phase extraction-liquid chromatography-electrospray-tandem mass spectrometry for the determination of sulfonamides and their acetylated metabolites in groundwater
M. Jesús García-Galán
Teresa Garrido
Damià Barceló
Original Paper 09 November 2010 Pages: 795 - 806
Cleanup strategies and advantages in the determination of several therapeutic classes of pharmaceuticals in wastewater samples by SPE–LC–MS/MS
M. A. Sousa
C. Gonçalves
M. F. Alpendurada
Original Paper 20 October 2010 Pages: 807 - 822
Shotgun lipidomics for candidate biomarkers of urinary phospholipids in prostate cancer
Hye Kyeong Min
Sangsoo Lim
Myeong Hee Moon
Original Paper 17 October 2010 Pages: 823 - 830
Carbon nanoparticles in lateral flow methods to detect genes encoding virulence factors of Shiga toxin-producing Escherichia coli
P. Noguera
G. A. Posthuma-Trumpie
A. van Amerongen
Original Paper Open access 28 October 2010 Pages: 831 - 838
Simultaneous quantitative profiling of N-acyl-l-homoserine lactone and 2-alkyl-4(1H)-quinolone families of quorum-sensing signaling molecules using LC-MS/MS
Catharine A. Ortori
Jean-Frédéric Dubern
David A. Barrett
Original Paper 28 October 2010 Pages: 839 - 850
Retinol fluorescence in lecithin/n-butanol/water aggregates: a new improvement for its analysis in cosmetics without pretreatment
M. P. San Andrés
S. Vera
M. Valiente
Original Paper 29 October 2010 Pages: 851 - 859
Accelerated sample treatment for screening of banned doping substances by GC–MS: ultrasonication versus microwave energy
M. Galesio
M. Mazzarino
J. L. Capelo
Original Paper 29 October 2010 Pages: 861 - 875
A liquid chromatography/tandem mass spectrometry (LC-MS/MS) method for the determination of phenolic polycyclic aromatic hydrocarbons (OH-PAH) in urine of non-smokers and smokers
Bernhard Ramsauer
Katharina Sterz
Francis Cheung
Original Paper 03 November 2010 Pages: 877 - 889
Determination of pharmaceuticals, steroid hormones, and endocrine-disrupting personal care products in sewage sludge by ultra-high-performance liquid chromatography–tandem mass spectrometry
Yiyi Yu
Qiuxin Huang
Xianzhi Peng
Original Paper 28 October 2010 Pages: 891 - 902
Retention modelling of polychlorinated biphenyls in comprehensive two-dimensional gas chromatography
Angelo Antonio D’Archivio
Angela Incani
Fabrizio Ruggieri
Original Paper 23 October 2010 Pages: 903 - 913
LC–MS–MS determination of ibuprofen, 2-hydroxyibuprofen enantiomers, and carboxyibuprofen stereoisomers for application in biotransformation studies employing endophytic fungi
Keyller Bastos Borges
Anderson Rodrigo Moraes de Oliveira
Pierina Sueli Bonato
Original Paper 16 November 2010 Pages: 915 - 925
A novel total reflection X-ray fluorescence procedure for the direct determination of trace elements in petrochemical products
Amedeo Cinosi
Nunzio Andriollo
Damiano Monticelli
Original Paper 03 November 2010 Pages: 927 - 933
Development and in-house validation of allergen-specific ELISA tests for the quantification of Dau c 1.01, Dau c 1.02 and Dau c 4 in carrot extracts (Daucus carota)
Kay Foetisch
Lotte Dahl
Thomas Holzhauser
Original Paper 03 November 2010 Pages: 935 - 943
GC-MS determination of parabens, triclosan and methyl triclosan in water by in situ derivatisation and stir-bar sorptive extraction
Ana María Casas Ferreira
Monika Möder
María Esther Fernández Laespada
Original Paper 28 October 2010 Pages: 945 - 953
Dispersive solid-phase extraction for in-sorbent Fourier-transform infrared detection and identification of nerve agent simulants in analysis for verification of chemical weapon convention
Prabhat Garg
Deepak Pardasani
D. K. Dubey
Original Paper 08 November 2010 Pages: 955 - 963
Automatic optosensing device based on photo-induced fluorescence for determination of piceid in cocoa-containing products
Lucía Molina-García
Antonio Ruiz-Medina
Maria Luisa Fernández-de Córdova
Original Paper 16 October 2010 Pages: 965 - 972
Particle size characterization of titanium dioxide in sunscreen products using sedimentation field-flow fractionation–inductively coupled plasma–mass spectrometry
Atitaya Samontha
Juwadee Shiowatana
Atitaya Siripinyanond
Original Paper 16 October 2010 Pages: 973 - 978
Production and analytical characterization of neopterin immunoreagents for biosensor developments
Ivo Cernoch
Erwin Schleicher
Milan Franek
Technical Note 19 November 2010 Pages: 979 - 986
pH optimization for a reliable quantification of brain tumor cell and tissue extracts with ¹H NMR: focus on choline-containing compounds and taurine
O. Robert
J. Sabatier
M. Malet-Martino
Technical Note 11 November 2010 Pages: 987 - 999