Abstract
A novel rolling technique, i.e., skew rolling, was applied to a non-oriented electrical steel containing 0.9 wt% Si, aiming at altering the texture of the final sheets that usually contain the magnetically unfavorable <111>//ND fiber after conventional rolling and annealing. The texture after skew cold rolling was compared to those obtained from conventional rolling and cross rolling and significantly different textures were observed. The cold-rolled steel sheets were then annealed and the texture evolution was investigated using a quasi in situ electron backscatter diffraction technique, i.e., tracking the microtexture of the same area at various holding times at the same temperature. The development of the recrystallization microstructure and microtexture (nucleation and grain growth) was characterized and the effect of skew rolling on the final texture was studied. The mechanisms governing the formation of the final recrystallization texture, e.g., preferential nucleation and selective growth, were elucidated.
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References
Kestens L, Jacobs S (2008) Texture control during the manufacturing of nonoriented electrical steels. Texture Stress Microstruct 2008:1–9. doi:10.1155/2008/173083
Landgraf FJG (2012) Nonoriented electrical steels. JOM 64(7):764–771. doi:10.1007/s11837-012-0356-7
Hou CK, Liao CC (2008) Effect of cerium content on the magnetic properties of non-oriented electrical steels. ISIJ Int 48(4):531–539. doi:10.2355/isijinternational.48.531
Oda Y, Toda H, Shiga N, Kasai S, Hiratani T (2014) Effect of Si content on iron loss of electrical steel sheet under compressive stress. IEEE Trans Magn 50(4):1–4. doi:10.1109/TMAG.2013.2290321
Nakayama T, Tanaka T (1997) Effects of titanium on magnetic properties of semi-processed non-oriented electrical steel sheets. J Mater Sci 32(4):1055–1059. doi:10.1023/a:1018590725223
Chang SK (2006) Effects of Co, Mo, and Ni on magnetic properties in 3Si–0.1Sn–0.08Sb alloyed non-oriented electrical steels. J Mater Sci 41(22):7380–7386. doi:10.1007/s10853-006-0805-1
Barros J, Schneider J, Verbeken K, Houbaert Y (2008) On the correlation between microstructure and magnetic losses in electrical steel. J Magn Magn Mater 320(20):2490–2493. doi:10.1016/j.jmmm.2008.04.056
Shiozaki M, Kurosaki Y (1989) The effects of grain size on the magnetic properties of nonoriented electrical steel sheets. J Mater Eng 11(1):37–43. doi:10.1007/BF02833752
Pan H, Zhang Z, Xie J (2016) The effects of recrystallization texture and grain size on magnetic properties of 6.5 wt% Si electrical steel. J Magn Magn Mater 401:625–632. doi:10.1016/j.jmmm.2015.10.047
Moses AJ, Thursby GJ (1983) Improvement of magnetic properties of electrical steels using a surface diffusion technique. J Mater Sci 18(6):1657–1665. doi:10.1007/bf00542060
Cullity B, Graham C (2009) Ferrimagnetism. Introduction to magnetic materials, 2nd edn, Wiley, New York pp 175–195
Matsumura K, Fukuda B (1984) Recent developments of non-oriented electrical steel sheets. IEEE Trans Magn 20(5):1533–1538
Tomida T, Sano N, Ueda K, Fujiwara K, Takahashi N (2003) Cube-textured Si-steel sheets by oxide-separator-induced decarburization and growth mechanism of cube grains. J Magn Magn Mater 254–255:315–317. doi:10.1016/S0304-8853(02)00810-7
Equihua-Guillén F, Salinas-Rodríguez A (2011) Role of the austenite-ferrite transformation start temperature on the high-temperature ductility of electrical steels. J Mater Eng Perform 20(1):102–107. doi:10.1007/s11665-010-9643-z
Liu H-T, Liu Z-Y, Sun Y, Gao F, Wang G-D (2013) Development of λ-fiber recrystallization texture and magnetic property in Fe–6.5 wt% Si thin sheet produced by strip casting and warm rolling method. Mater Lett 91:150–153. doi:10.1016/j.matlet.2012.09.046
Hayakawa Y, Kurosawa M (2002) Orientation relationship between primary and secondary recrystallized texture in electrical steel. Acta Mater 50(18):4527–4534. doi:10.1016/S1359-6454(02)00271-9
Kestens L, Jonas J, Van Houtte P, Aernoudt E (1996) Orientation selection during static recrystallization of cross rolled non-oriented electrical steels. Textures Microstruct 27(1):321–336
Sanjari M, He Y, Hilinski EJ, Yue S, Kestens LAI (2016) Development of the {113} 〈uvw〉 texture during the annealing of a skew cold rolled non-oriented electrical steel. Scripta Mater 124:179–183. doi:10.1016/j.scriptamat.2016.07.005
He Y, Hilinski E (2016) Skew rolling and its effect on the deformation textures of non-oriented electrical steels. J Mater Process Tech (in press)
Park J-T, Szpunar JA (2003) Evolution of recrystallization texture in nonoriented electrical steels. Acta Mater 51(11):3037–3051. doi:10.1016/S1359-6454(03)00115-0
Pedrosa JSM, Paolinelli SdC, Cota André B (2015) Influence of initial annealing on structure evolution and magnetic properties of 3.4% Si non-oriented steel during final annealing. J Magn Magn Mater 393:146–150. doi:10.1016/j.jmmm.2015.05.058
Li H-Z, Liu Z-Y, Wang X-L, Ren H-M, Li C-G, Cao G-M, Wang G-D (2017) \left\{114 \right\} \langle 4\overline{8} 1\rangle $$ 114 〈4 8 ¯ 1〉 Annealing texture in twin-roll casting non-oriented 6.5 wt% Si electrical steel. J Mater Sci 52(1):247–259. doi:10.1007/s10853-016-0327-4
Mishra S, Därmann C, Lücke K (1984) On the development of the goss texture in iron-3% silicon. Acta Metall 32(12):2185–2201. doi:10.1016/0001-6160(84)90161-5
Doherty RD (1985) Nucleation and growth kinetics of different recrystallization texture components. Scr Metall 19(8):927–930. doi:10.1016/0036-9748(85)90284-4
Sebald R, Gottstein G (2002) Modeling of recrystallization textures: interaction of nucleation and growth. Acta Mater 50(6):1587–1598. doi:10.1016/S1359-6454(02)00020-4
Rollett A, Humphreys F, Rohrer GS, Hatherly M (2004) Recrystallization and related annealing phenomena. Elsevier, oxford
Bachmann F, Hielscher R, Schaeben H (2010) Texture analysis with MTEX–free and open source software toolbox. Solid state phenomena. Trans Tech Publications, Zurich-Durnten, pp 63–68
Nguyen-Minh T, Sidor JJ, Petrov RH, Kestens LAI (2012) Occurrence of shear bands in rotated Goss ({1 1 0}〈1 1 0〉) orientations of metals with bcc crystal structure. Scr Mater 67(12):935–938. doi:10.1016/j.scriptamat.2012.08.017
Quadir MZ, Duggan BJ (2006) A microstructural study of the origins of γ recrystallization textures in 75% warm rolled IF steel. Acta Mater 54(16):4337–4350. doi:10.1016/j.actamat.2006.05.026
Doherty RD, Hughes DA, Humphreys FJ, Jonas JJ, Jensen DJ, Kassner ME, King WE, McNelley TR, McQueen HJ, Rollett AD (1997) Current issues in recrystallization: a review. Mater Sci Eng A 238(2):219–274. doi:10.1016/S0921-5093(97)00424-3
Jonas J, Kestens L (2005) Transformation and recrystallization textures associated with steel processing. ASM Handbook 14A, vol 14. ASM International, Russell Township, pp 685–700
He Y, Hilinski E, Li J (2015) Texture evolution of a non-oriented electrical steel cold rolled at directions different from the hot rolling direction. Metall Mater Trans A 46(11):5350–5365
Aernoudt E, Houtte PV, Leffers T (2006) Deformation and textures of metals at large strain. Mater Sci Technol. doi:10.1002/9783527603978.mst0050
Tóth LS, Jonas JJ, Daniel D, Ray RK (1990) Development of ferrite rolling textures in low- and extra low-carbon steels. Metall Trans A 21(11):2985–3000. doi:10.1007/bf02647219
Xu W, Ferry M (2010) Recrystallisation textures in cold rolled low carbon steel containing ferritic and bainitic microstructures. Mater Sci Technol 26(10):1159–1172
Sidor JJ, Verbeken K, Gomes E, Schneider J, Calvillo PR, Kestens LAI (2012) Through process texture evolution and magnetic properties of high Si non-oriented electrical steels. Mater Charact 71:49–57. doi:10.1016/j.matchar.2012.06.006
Park JT, Szpunar JA (2005) Texture development during grain growth in nonoriented electrical steels. ISIJ Int 45(5):743–749. doi:10.2355/isijinternational.45.743
Sanjari M, Farzadfar SF, Sakai T, Utsunomiya H, Essadiqi E, Jung I-H, Yue S (2013) Microstructure and texture evolution of Mg3Zn3Ce magnesium alloys sheets and associated restoration mechanisms during annealing. Mater Sci Eng A 561:191–202. doi:10.1016/j.msea.2012.10.075
Agnew SR, Yoo MH, Tomé CN (2001) Application of texture simulation to understanding mechanical behavior of Mg and solid solution alloys containing Li or Y. Acta Mater 49(20):4277–4289. doi:10.1016/s1359-6454(01)00297-x
Sha YH, Sun C, Zhang F, Patel D, Chen X, Kalidindi SR, Zuo L (2014) Strong cube recrystallization texture in silicon steel by twin-roll casting process. Acta Mater 76:106–117. doi:10.1016/j.actamat.2014.05.020
Murakami K, Morishige N, Ushioda K (2012) The effect of cold rolling reduction on shear band and texture formation in Fe-3% Si alloy. Materials science forum. Trans Tech Publications, Zurich-Durnten, pp 158–163
Liu H-T, Li H-Z, Li H-L, Gao F, Liu G-H, Luo Z-H, Zhang F-Q, Chen S-L, Cao G-M, Liu Z-Y, Wang G-D (2015) Effects of rolling temperature on microstructure, texture, formability and magnetic properties in strip casting Fe-6.5 wt% Si non-oriented electrical steel. J Magn Magn Mater 391:65–74. doi:10.1016/j.jmmm.2015.04.105
Dorner D, Zaefferer S, Raabe D (2007) Retention of the Goss orientation between microbands during cold rolling of an Fe3%Si single crystal. Acta Mater 55(7):2519–2530. doi:10.1016/j.actamat.2006.11.048
Ushioda K, Nakanishi S, Morikawa T, Higashida K, Suwa Y, Murakami K (2013) Evolution of heterogeneous deformation structure and recrystallization texture of steel. Materials science forum. Trans Tech Publication, Zurich-Durnten, pp 58–65
Duggan BJ, Roberts WT (1975) Recrystallization textures in an iron-1. 2% copper alloy. Met Sci J 9(10):449–454
Gobernado P, Petrov RH, Kestens LAI (2012) Recrystallized {3 1 1} 〈1 3 6〉 orientation in ferrite steels. Scr Mater 66(9):623–626. doi:10.1016/j.scriptamat.2012.01.056
Verbeken K, Kestens L, Jonas JJ (2003) Microtextural study of orientation change during nucleation and growth in a cold rolled ULC steel. Scr Mater 48(10):1457–1462. doi:10.1016/S1359-6462(03)00078-2
Verbeken K, Kestens L (2003) Strain-induced selective growth in an ultra low carbon steel after a small rolling reduction. Acta Mater 51(6):1679–1690. doi:10.1016/S1359-6454(02)00569-4
Nakamura S, Homma H (2004) Micro-scale OIM study on the recrystallization process of cold rolled α-fiber single crystal. Mater Sci Forum 467:159–164
Gobernado P, Petrov R, Ruiz D, Leunis E, Kestens LAI (2010) Texture evolution in Si-alloyed ultra low-carbon steels after severe plastic deformation. Adv Eng Mater 12(10):1077–1081. doi:10.1002/adem.201000075
Verbeken K, Kestens L, Nave MD (2005) Re-evaluation of the Ibe-Lücke growth selection experiment in a Fe–Si single crystal. Acta Mater 53(9):2675–2682. doi:10.1016/j.actamat.2005.02.030
Song XL, Peng K, Zhang PP, Wu JY, Zhou J, Jia J, Fan LX (2013) Effect of phosphorus contents on texture and grain boundary character for the annealing high strength Ti-IF steels. Adv Mater Res 652–654:929–933. doi:10.4028/www.scientific.net/AMR.652-654.929
Zhang ZW, Wang WH, Zou Y, Baker I, Chen D, Liang YF (2015) Control of grain boundary character distribution and its effects on the deformation of Fe–6.5 wt% Si. J Alloy Compd 639:40–44. doi:10.1016/j.jallcom.2015.03.129
Acknowledgements
Funding for this work was provided by Natural Resources Canada through the Program of Energy Research and Development. United States Steel Corporation Research and Technology Center (Munhall, PA) is gratefully acknowledged for melting, hot rolling and hot band annealing of the steel plates. The authors are grateful to Michael Attard, Darren Bibby, Raul Santos, Renata Zavadil, Jian Li and Pei Liu for their contributions to this project. Dr. Mark Kozdras is thanked for his careful review on the manuscript. Peter Badgley from the United States Steel Corporation Canada (Hamilton, ON) is gratefully acknowledged for coordinating this research.
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Sanjari, M., He, Y., Hilinski, E.J. et al. Texture evolution during skew cold rolling and annealing of a non-oriented electrical steel containing 0.9 wt% silicon. J Mater Sci 52, 3281–3300 (2017). https://doi.org/10.1007/s10853-016-0616-y
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DOI: https://doi.org/10.1007/s10853-016-0616-y