Skip to main content
Log in

Effects of temperature and acid solution on the physical and tensile mechanical properties of red sandstones

  • Research Article
  • Published:
Environmental Science and Pollution Research Aims and scope Submit manuscript

Abstract

Recent infrastructure development in China and other developing countries has attracted global attention. As a control project of traffic engineering, tunnels also have rapidly increased. However, fire accidents induced by traffic accident or gas explosion frequently occur in tunnels, causing irreversible damage to the tunnel rocks. Moreover, the corrosive effects of acid rain or polluted groundwater have a long-term effect on the tunnel and surrounding rocks. In this paper, physical and thermophysical properties tests as well as Brazilian splitting test were conducted on red sandstone specimens after heating at a variety of different temperature and acidic solution erosion. The responses of surface features, mass, P wave velocity, porosity and thermal conductivity, and the tensile strength of the red sandstone were compared and analyzed. In addition, the effects of high temperature (25–1000 °C) and acidic solution on microscopic structures, defect morphology, and mineral reaction of the red sandstone were observed and analyzed. The experimental results show that high temperature and acidic chemical solution significantly affects the physical and mechanical properties of the rock mass. The typical parameters, such as surface features, mass and P wave velocity, porosity, thermal conductivity, and tensile strength, are closely affected by acidity. In addition, we observed that the physical properties of red sandstones change with temperature and can be divided into three stages, and at 300–800 °C stage, they significantly declined. The results provide a basis for rock damage and failure induced by fire and acidic groundwater seepage in tunnels.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14
Fig. 15
Fig. 16
Fig. 17
Fig. 18
Fig. 19

Similar content being viewed by others

Data availability

The datasets used and/or analyzed during the current study are available from the corresponding author on reasonable request.

References

  • Brotóns V, Tomás R, Ivorra S, Alarcón JC (2013) Temperature influence on the physical and mechanical properties of a porous rock: San Julian’s calcarenite. Eng Geol 167:117–127

    Article  Google Scholar 

  • Cen D, Huang D (2017) Direct shear tests of sandstone under constant normal tensile stress condition using a simple auxiliary device. Rock Mech Rock Eng 50:1425–1438

    Article  Google Scholar 

  • Cen D, Huang D, Song Y, Jiang Q (2020) Direct tensile behavior of limestone and sandstone with bedding planes at different strain rates. Rock Mech Rock Eng 53:2643–2651

    Article  Google Scholar 

  • Csáki Š, Ondruška J, Trnovcová V, Štubňa I, Dobroň P, Vozár L (2018) Temperature dependence of the AC conductivity of illitic clay. Appl Clay Sci 157:19–23

    Article  CAS  Google Scholar 

  • Dehestani A, Hosseini M, Beydokhti AT (2020) Effect of wetting–drying cycles on mode I and mode II fracture toughness of sandstone in natural (pH = 7) and acidic (pH = 3) environments. Theor Appl Fract Mech 107:102512

    Article  CAS  Google Scholar 

  • Elimbi A, Tchakoute HK, Njopwouo D (2011) Effects of calcination temperature of kaolinite clays on the properties of geopolymer cements. Constr Build Mater 25:2805–2812

    Article  Google Scholar 

  • Escalera E, Tegman R, Antti M-L, Odén M (2014) High temperature phase evolution of Bolivian kaolinitic–illitic clays heated to 1250 °C. Appl Clay Sci 101:100–105

    Article  CAS  Google Scholar 

  • Feng X, Ding W (2007) Experimental study of limestone micro-fracturing under a coupled stress, fluid flow and changing chemical environment. Int J Rock Mech Min Sci 44:437–448

    Article  Google Scholar 

  • Feng X, Chen S, Zhou H (2004) Real-time computerized tomography (CT) experiments on sandstone damage evolution during triaxial compression with chemical corrosion. Int J Rock Mech Min Sci 41:181–192

    Article  Google Scholar 

  • Feng X, Ding W, Zhang D (2009) Multi-crack interaction in limestone subject to stress and flow of chemical solutions. Int J Rock Mech Min Sci 46:159–171

    Article  Google Scholar 

  • Geng J, Sun Q (2018) Effects of high temperature treatment on physical-thermal properties of clay. Thermochim Acta 666:148–155

    Article  CAS  Google Scholar 

  • Gualtieri ML, Gualtieri AF, Gagliardi S, Ruffini P, Ferrari R, Hanuskova M (2010) Thermal conductivity of fired clays: effects of mineralogical and physical properties of the raw materials. Appl Clay Sci 49:269–275

    Article  CAS  Google Scholar 

  • Han J, Sun Q, Xing H, Zhang Y, Sun H (2017) Experimental study on thermophysical properties of clay after high temperature. Appl Therm Eng 111:847–854

    Article  Google Scholar 

  • Hu J, Sun Q, Chen S, Zhang W (2018) The thermodynamic properties variation of cemented clay after treatment at high temperatures. Constr Build Mater 182:523–529

    Article  CAS  Google Scholar 

  • Huang D, Cen D, Song Y (2020a) Comparative investigation on the compression–shear and tension–shear behaviour of sandstone at different shearing rates. Rock Mech Rock Eng 53:3111–3131

    Article  Google Scholar 

  • Huang D, Guo YQ, Cen DF, Zhong Z, Song YX (2020b) Experimental investigation on shear mechanical behavior of sandstone containing a pre-existing flaw under unloading normal stress with constant shear stress. Rock Mech Rock Eng 53:3779–3792

    Article  Google Scholar 

  • Huo RK, Li SG, Ding Y (2018a) Experimental study on physicochemical and mechanical properties of mortar subjected to acid corrosion. Adv Mater Sci Eng 2018:1–11

    Article  CAS  Google Scholar 

  • Huo RK, Li SG, Han F, Li J (2018b) Experimental study on the characteristics of sandstone subjected to acid corrosion. IOP Conference Series: Earth and Environmental Science 153:022031

    Google Scholar 

  • Jia X, O'Connor D, Hou D, Jin Y, Li G, Zheng C, Ok YS, Tsang DCW, Luo J (2019) Groundwater depletion and contamination: spatial distribution of groundwater resources sustainability in China. Sci Total Environ 672:551–562

    Article  CAS  Google Scholar 

  • Kumari WGP, Ranjith PG, Perera MSA, Li X, Li LH, Chen BK, Isaka BLA, De Silva VRS (2018) Hydraulic fracturing under high temperature and pressure conditions with micro CT applications: geothermal energy from hot dry rocks. Fuel 230:138–154

    Article  CAS  Google Scholar 

  • Li H, Yang D, Zhong Z, Sheng Y, Liu X (2018a) Experimental investigation on the micro damage evolution of chemical corroded limestone subjected to cyclic loads. Int J Fatigue 113:23–32

    Article  CAS  Google Scholar 

  • Li H, Zhong Z, Liu X, Sheng Y, Yang D (2018b) Micro-damage evolution and macro-mechanical property degradation of limestone due to chemical effects. Int J Rock Mech Min Sci 110:257–265

    Article  Google Scholar 

  • Li S, Huo R, Wang B, Ren Z, Ding Y, Qian M, Qiu T (2018c) Experimental study on physicomechanical properties of sandstone under acidic environment. Advances in Civil Engineering 2018:1–15

    Article  Google Scholar 

  • Li S, Huo R, Yoshiaki F, Ren D, Song Z (2019a) Effect of acid-temperature-pressure on the damage characteristics of sandstone. Int J Rock Mech Min Sci 122:104079

    Article  Google Scholar 

  • Li X, Qu D, Luo Y, Ma R, Xu K, Wang G (2019b) Damage evolution model of sandstone under coupled chemical solution and freeze-thaw process. Cold Reg Sci Technol 162:88–95

    Article  Google Scholar 

  • Liao J, Zhao Y, Liu Q, Tang L (2020) Experimental study on shear strength characteristics of limestone under acidizing corrosion. Journal of Mining & Safety Engineering 37(3):639–646

    Google Scholar 

  • Liu S, Xu J (2015) An experimental study on the physico-mechanical properties of two post-high-temperature rocks. Eng Geol 185:63–70

    Article  Google Scholar 

  • Liu Q, Qian Z, Wu Z (2017) Micro/macro physical and mechanical variation of red sandstone subjected to cyclic heating and cooling: an experimental study. Bull Eng Geol Environ 78:1485–1499

    Article  CAS  Google Scholar 

  • Lu Z, Chen C, Feng X, Zhang Y (2014) Strength failure and crack coalescence behavior of sandstone containing single pre-cut fissure under coupled stress, fluid flow and changing chemical environment. J Cent South Univ 21:1176–1183

    Article  CAS  Google Scholar 

  • Ma D, Duan H, Liu W, Ma X, Tao M (2020a) Water–sediment two-phase flow inrush hazard in rock fractures of overburden strata during coal mining. Mine Water Environ 39:308–319

    Article  CAS  Google Scholar 

  • Ma D, Duan H, Zhang Q, Zhang J, Li W, Zhou Z, Liu W (2020b) A numerical gas fracturing model of coupled thermal, flowing and mechanical effects. Computers, Materials & Continua 65:2123–2141

    Article  Google Scholar 

  • Ma D, Zhang J, Duan H, Huang Y, Li M, Sun Q, Zhou N (2020c) Reutilization of gangue wastes in underground backfilling mining: overburden aquifer protection. Chemosphere 264:128400

    Article  CAS  Google Scholar 

  • Miao S, Cai M, Guo Q, Wang P, Liang M (2016) Damage effects and mechanisms in granite treated with acidic chemical solutions. Int J Rock Mech Min Sci 88:77–86

    Article  Google Scholar 

  • Miras A, Galán E, González I, Romero-Baena A, Martín D (2018) Mineralogical evolution of ceramic clays during heating. An ex/in situ X-ray diffraction method comparison study. Appl Clay Sci 161:176–183

    Article  CAS  Google Scholar 

  • Ohno I, Harada K, Yoshitomi C (2006) Temperature variation of elastic constants of quartz across the α-β transition. Phys Chem Miner 33:1–9

    Article  CAS  Google Scholar 

  • Peng J, Rong G, Yao M, Wong LNY, Tang Z (2018) Acoustic emission characteristics of a fine-grained marble with different thermal damages and specimen sizes. Bull Eng Geol Environ 78:4479–4491

    Article  Google Scholar 

  • Qi J, Sui W, Liu Y, Zhang D (2015) Slaking process and mechanisms under static wetting and drying cycles slaking tests in a red strata mudstone. Geotech Geol Eng 33:959–972

    Article  Google Scholar 

  • Ranjith PG, Viete DR, Chen BJ, Perera MSA (2012) Transformation plasticity and the effect of temperature on the mechanical behaviour of Hawkesbury sandstone at atmospheric pressure. Eng Geol 151:120–127

    Article  Google Scholar 

  • Ren R, Zhou H, Hu Z, He S, Wang X (2019) Statistical analysis of fire accidents in Chinese highway tunnels 2000–2016. Tunn Undergr Space Technol 83:452–460

    Article  Google Scholar 

  • Sha S, Rong G, Peng J, Li B, Wu Z (2019) Effect of open-fire-induced damage on Brazilian tensile strength and microstructure of granite. Rock Mech Rock Eng 52:4189–4202

    Article  Google Scholar 

  • Sha S, Rong G, Chen Z, Li B, Zhang Z (2020) Experimental evaluation of physical and mechanical properties of geothermal reservoir rock after different cooling treatments. Rock Mech Rock Eng 53:4967–4991

    Article  Google Scholar 

  • Singh UK, Ramanathan AL, Subramanian V (2018) Groundwater chemistry and human health risk assessment in the mining region of East Singhbhum, Jharkhand, India. Chemosphere 204:501–513

    Article  CAS  Google Scholar 

  • Sirdesai NN, Singh TN, Pathegama Gamage R (2017) Thermal alterations in the poro-mechanical characteristic of an Indian sandstone–a comparative study. Eng Geol 226:208–220

    Article  Google Scholar 

  • Sun H, Sun Q, Deng W, Zhang W, Lü C (2017) Temperature effect on microstructure and P-wave propagation in Linyi sandstone. Appl Therm Eng 115:913–922

    Article  Google Scholar 

  • Sun Q, Zhang W, Zhu Y, Huang Z (2019) Effect of high temperatures on the thermal properties of granite. Rock Mech Rock Eng 52:2691–2699

    Article  Google Scholar 

  • Swab JJ, Yu J, Gamble R, Kilczewski S (2011) Analysis of the diametral compression method for determining the tensile strength of transparent magnesium aluminate spinel. Int J Fract 172:187–192

    Article  Google Scholar 

  • Tian H, Ziegler M, Kempka T (2014) Physical and mechanical behavior of claystone exposed to temperatures up to 1000 °C. Int J Rock Mech Min Sci 70:144–153

    Article  Google Scholar 

  • Ulusay R, Hudson JA (2007) The complete ISRM suggested methods for rock characterization, testing and monitoring: 1974–2006. ISRM Commission on Testing Methods, Ankata

    Google Scholar 

  • Vázquez P, Shushakova V, Gómez-Heras M (2015) Influence of mineralogy on granite decay induced by temperature increase: experimental observations and stress simulation. Eng Geol 189:58–67

    Article  Google Scholar 

  • Wu Y, Huang Z, Zhao K, Zeng W, Gu Q, Zhang R (2020) Unsteady seepage solutions for hydraulic fracturing around vertical wellbores in hydrocarbon reservoirs. Int J Hydrog Energy 45:9496–9503

    Article  CAS  Google Scholar 

  • Xie S, Shao J (2006) Elastoplastic deformation of a porous rock and water interaction. Int J Plast 22:2195–2225

    Article  Google Scholar 

  • Xie SY, Shao JF, Xu WY (2011) Influences of chemical degradation on mechanical behaviour of a limestone. Int J Rock Mech Min Sci 48:741–747

    Article  Google Scholar 

  • Xu J, Wu H, Cheng L, Liu J, Zhou W (2012) Experimental study of shearing failure properties of sandstone under acidic conditions. Chin J Rock Mech Eng 31(2):3897–3903

    Google Scholar 

  • Yang X, Jiang A, Li M (2019) Experimental investigation of the time-dependent behavior of quartz sandstone and quartzite under the combined effects of chemical erosion and freeze–thaw cycles. Cold Reg Sci Technol 161:51–62

    Article  Google Scholar 

  • Yao H, Feng X, Cui Q, Zhou H (2009) Meso-mechanical experimental study of meso-fraeturing process of limestone under coupled chemical corrosion and water pressure. Rock Soil Mech 30(1):59–66

    CAS  Google Scholar 

  • Yavuz H, Demirdag S, Caran S (2010) Thermal effect on the physical properties of carbonate rocks. Int J Rock Mech Min Sci 47:94–103

    Article  Google Scholar 

  • Yu L, Zhang Z, Wu J, Liu R, Qin H, Fan P (2020) Experimental study on the dynamic fracture mechanical properties of limestone after chemical corrosion. Theor Appl Fract Mech 108:102620

    Article  CAS  Google Scholar 

  • Zeng W, Huang Z, Wu Y, Li S, Zhang R, Zhao K (2020) Experimental investigation on mining-induced strain and failure characteristics of rock masses of mine floor. Geomatics, Natural Hazards and Risk 11:491–509

    Article  Google Scholar 

  • Zhao Z, Liu Z, Pu H, Li X (2018) Effect of thermal treatment on Brazilian tensile strength of granites with different grain size distributions. Rock Mech Rock Eng 51:1293–1303

    Article  Google Scholar 

  • Zhou C, Yang X, Liang Y, Du Z, Liu Z, Huang W, Ming W (2019) Classification of red-bed rock mass structures and slope failure modes in South China. Geosciences 9:273

    Article  Google Scholar 

  • Zhu WC, Tang CA (2006) Numerical simulation of Brazilian disk rock failure under static and dynamic loading. Int J Rock Mech Min Sci 43:236–252

    Article  Google Scholar 

  • Zhu S, Zhang W, Sun Q, Deng S, Geng J, Li C (2017) Thermally induced variation of primary wave velocity in granite from Yantai: experimental and modeling results. Int J Therm Sci 114:320–326

    Article  Google Scholar 

Download references

Acknowledgments

We thank the anonymous reviewers for their comments on our paper.

Funding

This study received financial support from the National Natural Science Foundation of China (41702326); the Innovative Experts, Long-term Program of Jiangxi Province (jxsq2018106049); the Jiangxi Provincial Natural Science Foundation (20202ACB214006); and the Supported by Program of Qingjiang Excellent Young Talents, Jiangxi University of Science and Technology.

Author information

Authors and Affiliations

Authors

Contributions

All the authors have designed this study equally. YW collected the data for this research work. SL and QG analyzed and interpreted the results of the study. ZH and WZ drafted the initial manuscript. ZH and KZ have revised and restructured the manuscript.

Corresponding authors

Correspondence to Wei Zeng or Kui Zhao.

Ethics declarations

Conflict of interest

The authors declare that they have no conflict of interest.

Additional information

Responsible Editor: Philippe Garrigues

Publisher’s note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Huang, Z., Zeng, W., Wu, Y. et al. Effects of temperature and acid solution on the physical and tensile mechanical properties of red sandstones. Environ Sci Pollut Res 28, 20608–20623 (2021). https://doi.org/10.1007/s11356-020-11866-x

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11356-020-11866-x

Keywords

Navigation