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Electrochemical sensor based on Ni/N-doped graphene oxide for the determination of hydroquinone and catechol

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Abstract

Developing excellent electrochemical sensors for the determination of pollutants in the environment is crucial to advances of human detection technology. In this work, Ni/N-doped graphene oxide (Ni/N-GO) composite was constructed as an electrochemical sensor (Ni/N-GO/GCE) for the selective determination of catechol (CC) and hydroquinone (HQ). Thereinto, the Ni/N-GO composite was prepared by a high-temperature thermal reduction method. Also, a series of characterizations and electrochemical measurements were used to research the electrochemical properties of Ni/N-GO/GCE to detect CC and HQ. Furthermore, the oxidation peak potentials of CC and HQ on Ni/N-GO/GCE were 0.07 and 0.17 V, respectively, allowing selective detection of HQ and CC. Ni/N-GO/GCE exhibited linear responses toward CC and HQ in the concentration ranges of 1.4 ~ 800 and 1.0 ~ 800 μM, respectively. Besides, the detection limits were calculated as 0.06 and 0.16 μM (S/N = 3) through differential pulse voltammetry, respectively. Under optimized experimental conditions, the electrochemical sensor revealed excellent catalytic performance for the redox of CC and HQ. Finally, the results showed that Ni/N-GO/GCE was a promising electrode with superb long-term stability and reproducibility for the determination of hydroquinone isomers.

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Acknowledgements

This work was supported by the Sichuan Provincial College Students Innovation and Entrepreneurship Training Program (Grant No. S202010619008) and the International Science and Technology Cooperation Laboratory of Micro-nanoparticle Application Research of Southwest University of Science and Technology (Grant No. 19MNA001). National Natural Science Foundation of China (41872039 and 41831285).)

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  1. School of Materials and Chemistry, Southwest University of Science and Technology, Mianyang, 621010, People’s Republic of China

    Lei Liao, Pengcheng Zhou, Feng Xiao, Weishan Tang, Maojie Zhao, Rong Su, Ping He & Dingming Yang

  2. International Science and Technology Cooperation Laboratory of Micro-Nanoparticle Application Research, Southwest University of Science and Technology, Mianyang, 621010, People’s Republic of China

    Ping He

  3. Key Laboratory of Solid Waste Treatment and Resource Recycle, Southwest University of Science and Technology, Mianyang, 621010, People’s Republic of China

    Liang Bian

  4. School of Basic Medical Sciences, Southwest Medical University, Luzhou, 646000, People’s Republic of China

    Bin Tang

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  1. Lei Liao
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Liao, L., Zhou, P., Xiao, F. et al. Electrochemical sensor based on Ni/N-doped graphene oxide for the determination of hydroquinone and catechol. Ionics 29, 1605–1615 (2023). https://doi.org/10.1007/s11581-023-04892-5

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