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Synthesis of Silver Nanoparticles by Biogenic Methods: Characterization and Development of a Sensor Sensible to Pharmaceutical Medicine Paracetamol

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Abstract

In this study, silver nanoparticles (Ag NPs) were synthesized in biogenic methods. It is aimed to improve the electrochemical sensor efficiency of synthesized Ag NPs against the pharmaceutical drug paracetamol. For this purpose, fourier transmission infrared spectroscopy (FTIR), ultra-violet visible spectroscopy (Uv–vis), X-ray differentiation (XRD), and transmission electron spectroscopy (TEM) analyses were performed to elucidate the structure of the synthesized Ag NPs. In the TEM characterization results, the mean size of the NPs was found to be 19.035 nm using TEM characterization and the XRD results, the crystalline size of the NPs was 11.66 nm. Sensor studies were performed with cyclic voltammetry (CV) and differential pulse voltammetry (DPV) techniques. Paracetamol showed a sensitivity of approximately 0.4 V to Ag NPs in this study. The linear ranges of this study are 6.5–14.5 µM, with a limit of detection (LOD) of 5.79 µM and a limit of quantification (LOQ) of 17.56 µM.

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Authors and Affiliations

  1. School of Resources and Environment, University of Electronic Science and Technology of China, Chengdu, People’s Republic of China

    Fatemeh Karimi

  2. Sen Research Group, Department of Biochemistry, University of Dumlupinar, 43000, Kutahya, Turkey

    Elif Esra Altuner, Aysenur Aygun, Ramazan Bayat & Fatih Sen

  3. Program of Medical Laboratory and Techniques, Department of Medical Services and Techniques, Europe Vocational School, Kocaeli Health and Technology University, Kocaeli, Turkey

    Elif Esra Altuner

  4. Institute of de Alta Investigacion, Universidad de Tarapaca, 1000000, Arica, Chile

    Saravanan Rajendran

  5. School of Engineering, Lebanese American University, Byblos, Lebanon

    Fatemeh Karimi

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  1. Fatemeh Karimi
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Karimi, F., Altuner, E.E., Aygun, A. et al. Synthesis of Silver Nanoparticles by Biogenic Methods: Characterization and Development of a Sensor Sensible to Pharmaceutical Medicine Paracetamol. Top Catal 67, 585–593 (2024). https://doi.org/10.1007/s11244-023-01887-4

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