Abstract
The microstructure and microhardness of copper subjected to large strains either using one or a combination of severe plastic deformation (SPD) processing techniques was evaluated. The individual SPD techniques used include equal-channel angular pressing (ECAP), high-pressure torsion (HPT), and chip formation during machining (M). Microstructural characterization using orientation imaging microscopy provided detailed information on the grain sizes and misorientation statistics after different processing routes. Vickers indentation analysis was used to evaluate the hardness of the deformed samples. The results show that excellent microstructures and properties are achieved when these three processes are used in combination, including grain sizes in the range of ~0.2–0.3 μm and hardness values up to >1,900 MPa.
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Segal VM, Reznikov VI, Drobyshevskiy AE, Kopylov VI (1981) Russ Metall 1:99
Valiev RZ, Langdon TG (2006) Prog Mater Sci 51:881. doi:https://doi.org/10.1016/j.pmatsci.2006.02.003
Zhilyaev AP, Lee S, Nurislamova GV, Valiev RZ, Langdon TG (2001) Scripta Mater 44:2753. doi:https://doi.org/10.1016/S1359-6462(01)00955-1
Zhilyaev AP, Nurislamova GV, Kim B-K, Baró MD, Szpunar JA, Langdon TG (2003) Acta Mater 51:753. doi:https://doi.org/10.1016/S1359-6454(02)00466-4
Swaminathan S, Brown TL, Chandrasekar S, McNelley TR, Compton WD (2007) Scripta Mater 56:1047. doi:https://doi.org/10.1016/j.scriptamat.2007.02.034
Swaminathan S, Ravi Shankar M, Rao BC, Compton WD, Chandrasekar S, King AH, Trumble KP (2007) J Mater Sci 42:1529. doi:https://doi.org/10.1007/s10853-006-0745-9
Furukawa M, Iwahashi Y, Horita Z, Nemoto M, Langdon TG (1998) Mater Sci Eng A 257:328. doi:https://doi.org/10.1016/S0921-5093(98)00750-3
Oh-ishi K, Horita Z, Furukawa M, Nemoto M, Langdon TG (1998) Metall Mater Trans 29A:2011. doi:https://doi.org/10.1007/s11661-998-0027-z
Wang J, Iwahashi Y, Horita Z, Furukawa M, Nemoto M, Valiev RZ, Langdon TG (1996) Acta Mater 44:2973. doi:https://doi.org/10.1016/1359-6454(95)00395-9
Furukawa M, Iwahashi Y, Horita Z, Nemoto M, Tsenev NK, Valiev RZ, Langdon TG (1997) Acta Mater 45:4751. doi:https://doi.org/10.1016/S1359-6454(97)00120-1
Ferrasse S, Segal VM, Hartwig KT, Goforth RE (1997) Metall Mater Trans 28A:1047. doi:https://doi.org/10.1007/s11661-997-0234-z
Hasegawa H, Komura S, Utsunomiya A, Horita Z, Furukawa M, Nemoto M, Langdon TG (1999) Mater Sci Eng A 265:188. doi:https://doi.org/10.1016/S0921-5093(98)01136-8
Neishi K, Horita Z, Langdon TG (2002) Mater Sci Eng A 325:54. doi:https://doi.org/10.1016/S0921-5093(01)01404-6
Dalla Torre F, Lapovok R, Sandlin J, Thomson PF, Davies CHJ, Pereloma EV (2004) Acta Mater 52:4819. doi:https://doi.org/10.1016/j.actamat.2004.06.040
Brandstetter S, Zhang K, Escuadro A, Weertman JR, Van Swygenhoven H (2008) Scripta Mater 58:61. doi:https://doi.org/10.1016/j.scriptamat.2007.08.042
Zhilyaev AP, Gimazov AA, Raab GI, Langdon TG (2008) Mater Sci Eng A 486:123
OIM user’s manual, EDAX-TSL, E. Mahway, NJ, 2005
Zhilyaev AP, Oh-ishi K, Raab GI, McNelley TR (2006) Ultrafine grained materials IV. In: Zhu YT, Langdon TG, Horita Z, Zehetbauer MJ, Semiatin SL, Lowe TC (eds) The Minerals, Metals and Materials society, Warrendale, PA, p 113
Dutkiewicz J, Kuśnierz J, Maziarz W, Lejkowska M, Garbacz H, Lewandowska M, Dobromysloa AV, Kurzydlowski KJ (2005) Phys Stat Sol (a) 202:2309. doi:https://doi.org/10.1002/pssa.200521235
Todaka Y, Umemoto M, Yamazaki A, Sasaki J, Tsuchiya K (2008) Mater Trans 49:7. doi:https://doi.org/10.2320/matertrans.ME200713
Zhilyaev AP, Gimazov AA, Soshnikova EP, Révész Á, Langdon TG (2008) Mater Sci Eng A 489:207
Zhilyaev AP, Garcia-Infanta JM, Carreno F, Langdon TG, Ruano OA (2007) Scripta Mater 57:763. doi:https://doi.org/10.1016/j.scriptamat.2007.06.029
Jiang H, Zhu YT, Butt DP, Alexandrov IV, Lowe TC (2000) Mater Sci Eng A 290:128. doi:https://doi.org/10.1016/S0921-5093(00)00919-9
Degtyarev MV, Chashchukhina TI, Voronova LM, Patselov AM, Pilyugin VP (2007) Acta Mater 55:6039. doi:https://doi.org/10.1016/j.actamat.2007.04.017
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One of the authors (APZ) thanks the Spanish Ministry of Education and Science (under the Ramón y Cajal program) for financial support. Another author (TGL) was supported by the National Science Foundation of the United States under Grant No. DMR-0243331.
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Zhilyaev, A.P., Swaminathan, S., Gimazov, A.A. et al. An evaluation of microstructure and microhardness in copper subjected to ultra-high strains. J Mater Sci 43, 7451–7456 (2008). https://doi.org/10.1007/s10853-008-2714-y
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DOI: https://doi.org/10.1007/s10853-008-2714-y