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Understanding the deformation behavior of 17-4 precipitate hardenable stainless steel produced by direct metal laser sintering using micropillar compression and TEM

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Abstract

Micropillar compression testing and transmission electron microscopy were used to investigate the deformation mechanisms under compression in 17-4 precipitation-hardening stainless steel, fabricated by direct metal laser sintering. The as-built specimen as well as that aged for 4 h at 866 K contained fractions of retained austenite, while that aged for 60 min at 755 K was fully martensitic. It was observed that the columnar elongated grains underwent martensite/austenite phase changes with changes in the aging temperature. The precipitate phase that developed with aging enhanced the material hardness and yield strength, with values being higher in the case of the specimen aged at a lower temperature for a shorter time. The results showed that the microstructures and properties of 17-4 stainless steel specimens fabricated by DMLS vary significantly from those of specimens produced using conventional methods.

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References

  1. Kruth J-P, Leu M-C, Nakagawa T (1998) Progress in additive manufacturing and rapid prototyping. CIRP Annals-Manufacturing Technology 47:525–540

    Article  Google Scholar 

  2. Gibson I, Rosen DW, Stucker B (2010) Additive manufacturing technologies. Springer

  3. Wong KV, Hernandez A (2012) A review of additive manufacturing. ISRN Mechanical Engineering 2012

  4. Kruth J-P, Mercelis P, Van Vaerenbergh J, Froyen L, Rombouts M (2005) Binding mechanisms in selective laser sintering and selective laser melting. Rapid Prototyp J 11:26–36

    Article  Google Scholar 

  5. Agarwala M, Bourell D, Beaman J, Marcus H, Barlow J (1995) Direct selective laser sintering of metals. Rapid Prototyp J 1:26–36

    Article  Google Scholar 

  6. Gu D, Meiners W, Wissenbach K, Poprawe R (2012) Laser additive manufacturing of metallic components: materials, processes and mechanisms. Int Mater Rev 57:133–164

    Article  Google Scholar 

  7. AL-Mangour B (2015) Powder metallurgy of stainless steel: state-of-the art, challenges, and development. Stainless steel: microstructure, mechanical properties and methods of application. Nova Science Publishers. p. 37–80

  8. Mirzadeh H, Najafizadeh A, Moazeny M (2009) Flow curve analysis of 17-4 PH stainless steel under hot compression test. Metall Mater Trans A 40:2950–2948

    Article  Google Scholar 

  9. Viswanathan U, Nayar P, Krishnan R (1989) Kinetics of precipitation in 17–4 PH stainless steel. Mater Sci Technol 5:346–349

    Article  Google Scholar 

  10. Mirzadeh H, Najafizadeh A (2009) Aging kinetics of 17-4 PH stainless steel. Mater Chem Phys 116:119–124

    Article  Google Scholar 

  11. Murayama M, Hono K, Katayama Y (1999) Microstructural evolution in a 17-4 PH stainless steel after aging at 400 C. Metall Mater Trans A 30:345–353

    Article  Google Scholar 

  12. Murr LE, Martinez E, Hernandez J, Collins S, Amato KN, Gaytan SM, et al. (2012) Microstructures and properties of 17-4 PH stainless steel fabricated by selective laser melting. Journal of Materials Research and Technology 1:167–177

    Article  Google Scholar 

  13. Rafi HK, Pal D, Patil N, Starr TL, Stucker BE (2014) Microstructure and mechanical behavior of 17-4 precipitation hardenable steel processed by selective laser melting. J Mater Eng Perform 23:4421–4428

    Article  Google Scholar 

  14. Facchini L, Vicente N, Lonardelli I, Magalini E, Robotti P, Molinari A (2010) Metastable austenite in 17–4 precipitation-hardening stainless steel produced by selective laser melting. Adv Eng Mater 12:184–188

    Article  Google Scholar 

  15. Gu H, Gong H, Pal D, Rafi K, Starr T, Stucker B (2013) Influences of energy density on porosity and microstructure of selective laser melted 17-4PH stainless steel. 2013 Solid Freeform Fabrication Symposium. p. 474

  16. Starr TL, Rafi K, Stucker B, Scherzer CM (2012) Controlling phase composition in selective laser melted stainless steels. Power (W): 195:195

  17. Gratton A (2012) Comparison of mechanical, metallurgical properties of 17-4PH stainless steel between direct metal laser sintering (DMLS) and traditional manufacturing methods

  18. AlMangour B, Yang J-M (2016) Improving the surface quality and mechanical properties by shot-peening of 17-4 stainless steel fabricated by additive manufacturing. Materials & Design

  19. Oliver WC, Pharr GM (1992) An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J Mater Res 7:1564–1583

    Article  Google Scholar 

  20. Gao H, Huang Y, Nix W, Hutchinson J (1999) Mechanism-based strain gradient plasticity—I. Theory. Journal of the Mechanics and Physics of Solids 47:1239–1263

    Article  MathSciNet  MATH  Google Scholar 

  21. Uchic MD, Shade PA, Dimiduk DM (2009) Plasticity of micrometer-scale single crystals in compression. Annu Rev Mater Res 39:361–386

    Article  Google Scholar 

  22. Zhang H, Schuster BE, Wei Q, Ramesh KT (2006) The design of accurate micro-compression experiments. Scr Mater 54:181–186

    Article  Google Scholar 

  23. Fei H, Abraham A, Chawla N, Jiang H (2012) Evaluation of micro-pillar compression tests for accurate determination of elastic-plastic constitutive relations. J Appl Mech 79:061011

    Article  Google Scholar 

  24. Pinkerton AJ, Li L (2003) The effect of laser pulse width on multiple-layer 316L steel clad microstructure and surface finish. Appl Surf Sci 208:411–416

    Article  Google Scholar 

  25. Vilaro T, Colin C, Bartout J-D (2011) As-fabricated and heat-treated microstructures of the Ti-6Al-4V alloy processed by selective laser melting. Metall Mater Trans A 42:3190–3199

    Article  Google Scholar 

  26. Hsiao C, Chiou C, Yang J (2002) Aging reactions in a 17-4 PH stainless steel. Mater Chem Phys 74:134–142

    Article  Google Scholar 

  27. Viswanathan U, Banerjee S, Krishnan R (1988) Effects of aging on the microstructure of 17-4 PH stainless steel. Mater Sci Eng A 104:181–189

    Article  Google Scholar 

  28. Takaki S, Fukunaga K, Syarif J, Tsuchiyama T (2004) Effect of grain refinement on thermal stability of metastable austenitic steel. Mater Trans 45:2245–2251

    Article  Google Scholar 

  29. Ul’yanin E, Sorokina N, Zaretskii YM (1969) Properties of austenitic steel with nickel and nitrogen at low temperatures. Metal Science and Heat Treatment 11:681–682

    Article  Google Scholar 

  30. Suryanarayana C, NortonMG (2013) X-ray diffraction: a practical approach. Springer Science & Business Media

  31. Kiener D, Motz C, Dehm G (2009) Micro-compression testing: a critical discussion of experimental constraints. Mater Sci Eng A 505:79–87

    Article  Google Scholar 

  32. Volkert CA, Lilleodden ET (2006) Size effects in the deformation of sub-micron Au columns. Philos Mag 86:5567–5579

    Article  Google Scholar 

  33. AlMangour B, Grzesiak D, Yang J-M (2016) Rapid fabrication of bulk-form TiB2/316L stainless steel nanocomposites with novel reinforcement architecture and improved performance by selective laser melting. J Alloys Compd 680:480–493

    Article  Google Scholar 

  34. Allain S, Chateau J-P, Bouaziz O, Migot S, Guelton N (2004) Correlations between the calculated stacking fault energy and the plasticity mechanisms in Fe–Mn–C alloys. Mater Sci Eng A 387:158–162

    Article  Google Scholar 

  35. Abbaschian R, Reed-Hill, RE, (2008) Physical metallurgy principles. Cengage Learning

  36. Kanagarajah P, Brenne F, Niendorf T, Maier H (2013) Inconel 939 processed by selective laser melting: effect of microstructure and temperature on the mechanical properties under static and cyclic loading. Mater Sci Eng A 588:188–195

    Article  Google Scholar 

  37. Wu W, Hwu L, Lin D, Lee J (2000) The relationship between alloying elements and retained austenite in martensitic stainless steel welds. Scr Mater 42:1071–1076

    Article  Google Scholar 

  38. Bhaduri A, Sujith S, Srinivasan G, Gill T, Mannan S (1995) Optimized postweld heat treatment procedures for 17-4 PH stainless steels. Weld J 74:153

    Google Scholar 

  39. Zhang S, Findley K (2013) Quantitative assessment of the effects of microstructure on the stability of retained austenite in TRIP steels. Acta Mater 61:1895–1903

    Article  Google Scholar 

  40. Jiang B, Sun L, Li R, Hsu T (1995) Influence of austenite grain size on γ-ε martensitic transformation temperature in Fe-Mn-Si-Cr alloys. Scr Metall Mater 33:63–68

    Article  Google Scholar 

  41. Colaço R, Vilar R (2004) Stabilisation of retained austenite in laser surface melted tool steels. Mater Sci Eng A 385:123–127

    Article  Google Scholar 

  42. Vamsi Krishna B, Bandyopadhyay A (2009) Surface modification of AISI 410 stainless steel using laser engineered net shaping (LENS™). Mater Des 30:1490–1496

    Article  Google Scholar 

  43. Kim H-J, Kweon Y-G (1996) The effects of retained austenite on dry sliding wear behavior of carburized steels. Wear 193:8–15

    Article  Google Scholar 

  44. Nakagawa H, Miyazaki T (1999) Effect of retained austenite on the microstructure and mechanical properties of martensitic precipitation hardening stainless steel. J Mater Sci 34:3901–3908

    Article  Google Scholar 

  45. Bhambroo R, Roychowdhury S, Kain V, Raja V (2013) Effect of reverted austenite on mechanical properties of precipitation hardenable 17-4 stainlesssteel. Mater Sci Eng A 568:127–133

    Article  Google Scholar 

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Correspondence to Bandar AlMangour.

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AlMangour, B., Yang, JM. Understanding the deformation behavior of 17-4 precipitate hardenable stainless steel produced by direct metal laser sintering using micropillar compression and TEM. Int J Adv Manuf Technol 90, 119–126 (2017). https://doi.org/10.1007/s00170-016-9367-9

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  • DOI: https://doi.org/10.1007/s00170-016-9367-9

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