Abstract
Micropillar compression testing and transmission electron microscopy were used to investigate the deformation mechanisms under compression in 17-4 precipitation-hardening stainless steel, fabricated by direct metal laser sintering. The as-built specimen as well as that aged for 4 h at 866 K contained fractions of retained austenite, while that aged for 60 min at 755 K was fully martensitic. It was observed that the columnar elongated grains underwent martensite/austenite phase changes with changes in the aging temperature. The precipitate phase that developed with aging enhanced the material hardness and yield strength, with values being higher in the case of the specimen aged at a lower temperature for a shorter time. The results showed that the microstructures and properties of 17-4 stainless steel specimens fabricated by DMLS vary significantly from those of specimens produced using conventional methods.
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Kruth J-P, Leu M-C, Nakagawa T (1998) Progress in additive manufacturing and rapid prototyping. CIRP Annals-Manufacturing Technology 47:525–540
Gibson I, Rosen DW, Stucker B (2010) Additive manufacturing technologies. Springer
Wong KV, Hernandez A (2012) A review of additive manufacturing. ISRN Mechanical Engineering 2012
Kruth J-P, Mercelis P, Van Vaerenbergh J, Froyen L, Rombouts M (2005) Binding mechanisms in selective laser sintering and selective laser melting. Rapid Prototyp J 11:26–36
Agarwala M, Bourell D, Beaman J, Marcus H, Barlow J (1995) Direct selective laser sintering of metals. Rapid Prototyp J 1:26–36
Gu D, Meiners W, Wissenbach K, Poprawe R (2012) Laser additive manufacturing of metallic components: materials, processes and mechanisms. Int Mater Rev 57:133–164
AL-Mangour B (2015) Powder metallurgy of stainless steel: state-of-the art, challenges, and development. Stainless steel: microstructure, mechanical properties and methods of application. Nova Science Publishers. p. 37–80
Mirzadeh H, Najafizadeh A, Moazeny M (2009) Flow curve analysis of 17-4 PH stainless steel under hot compression test. Metall Mater Trans A 40:2950–2948
Viswanathan U, Nayar P, Krishnan R (1989) Kinetics of precipitation in 17–4 PH stainless steel. Mater Sci Technol 5:346–349
Mirzadeh H, Najafizadeh A (2009) Aging kinetics of 17-4 PH stainless steel. Mater Chem Phys 116:119–124
Murayama M, Hono K, Katayama Y (1999) Microstructural evolution in a 17-4 PH stainless steel after aging at 400 C. Metall Mater Trans A 30:345–353
Murr LE, Martinez E, Hernandez J, Collins S, Amato KN, Gaytan SM, et al. (2012) Microstructures and properties of 17-4 PH stainless steel fabricated by selective laser melting. Journal of Materials Research and Technology 1:167–177
Rafi HK, Pal D, Patil N, Starr TL, Stucker BE (2014) Microstructure and mechanical behavior of 17-4 precipitation hardenable steel processed by selective laser melting. J Mater Eng Perform 23:4421–4428
Facchini L, Vicente N, Lonardelli I, Magalini E, Robotti P, Molinari A (2010) Metastable austenite in 17–4 precipitation-hardening stainless steel produced by selective laser melting. Adv Eng Mater 12:184–188
Gu H, Gong H, Pal D, Rafi K, Starr T, Stucker B (2013) Influences of energy density on porosity and microstructure of selective laser melted 17-4PH stainless steel. 2013 Solid Freeform Fabrication Symposium. p. 474
Starr TL, Rafi K, Stucker B, Scherzer CM (2012) Controlling phase composition in selective laser melted stainless steels. Power (W): 195:195
Gratton A (2012) Comparison of mechanical, metallurgical properties of 17-4PH stainless steel between direct metal laser sintering (DMLS) and traditional manufacturing methods
AlMangour B, Yang J-M (2016) Improving the surface quality and mechanical properties by shot-peening of 17-4 stainless steel fabricated by additive manufacturing. Materials & Design
Oliver WC, Pharr GM (1992) An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J Mater Res 7:1564–1583
Gao H, Huang Y, Nix W, Hutchinson J (1999) Mechanism-based strain gradient plasticity—I. Theory. Journal of the Mechanics and Physics of Solids 47:1239–1263
Uchic MD, Shade PA, Dimiduk DM (2009) Plasticity of micrometer-scale single crystals in compression. Annu Rev Mater Res 39:361–386
Zhang H, Schuster BE, Wei Q, Ramesh KT (2006) The design of accurate micro-compression experiments. Scr Mater 54:181–186
Fei H, Abraham A, Chawla N, Jiang H (2012) Evaluation of micro-pillar compression tests for accurate determination of elastic-plastic constitutive relations. J Appl Mech 79:061011
Pinkerton AJ, Li L (2003) The effect of laser pulse width on multiple-layer 316L steel clad microstructure and surface finish. Appl Surf Sci 208:411–416
Vilaro T, Colin C, Bartout J-D (2011) As-fabricated and heat-treated microstructures of the Ti-6Al-4V alloy processed by selective laser melting. Metall Mater Trans A 42:3190–3199
Hsiao C, Chiou C, Yang J (2002) Aging reactions in a 17-4 PH stainless steel. Mater Chem Phys 74:134–142
Viswanathan U, Banerjee S, Krishnan R (1988) Effects of aging on the microstructure of 17-4 PH stainless steel. Mater Sci Eng A 104:181–189
Takaki S, Fukunaga K, Syarif J, Tsuchiyama T (2004) Effect of grain refinement on thermal stability of metastable austenitic steel. Mater Trans 45:2245–2251
Ul’yanin E, Sorokina N, Zaretskii YM (1969) Properties of austenitic steel with nickel and nitrogen at low temperatures. Metal Science and Heat Treatment 11:681–682
Suryanarayana C, NortonMG (2013) X-ray diffraction: a practical approach. Springer Science & Business Media
Kiener D, Motz C, Dehm G (2009) Micro-compression testing: a critical discussion of experimental constraints. Mater Sci Eng A 505:79–87
Volkert CA, Lilleodden ET (2006) Size effects in the deformation of sub-micron Au columns. Philos Mag 86:5567–5579
AlMangour B, Grzesiak D, Yang J-M (2016) Rapid fabrication of bulk-form TiB2/316L stainless steel nanocomposites with novel reinforcement architecture and improved performance by selective laser melting. J Alloys Compd 680:480–493
Allain S, Chateau J-P, Bouaziz O, Migot S, Guelton N (2004) Correlations between the calculated stacking fault energy and the plasticity mechanisms in Fe–Mn–C alloys. Mater Sci Eng A 387:158–162
Abbaschian R, Reed-Hill, RE, (2008) Physical metallurgy principles. Cengage Learning
Kanagarajah P, Brenne F, Niendorf T, Maier H (2013) Inconel 939 processed by selective laser melting: effect of microstructure and temperature on the mechanical properties under static and cyclic loading. Mater Sci Eng A 588:188–195
Wu W, Hwu L, Lin D, Lee J (2000) The relationship between alloying elements and retained austenite in martensitic stainless steel welds. Scr Mater 42:1071–1076
Bhaduri A, Sujith S, Srinivasan G, Gill T, Mannan S (1995) Optimized postweld heat treatment procedures for 17-4 PH stainless steels. Weld J 74:153
Zhang S, Findley K (2013) Quantitative assessment of the effects of microstructure on the stability of retained austenite in TRIP steels. Acta Mater 61:1895–1903
Jiang B, Sun L, Li R, Hsu T (1995) Influence of austenite grain size on γ-ε martensitic transformation temperature in Fe-Mn-Si-Cr alloys. Scr Metall Mater 33:63–68
Colaço R, Vilar R (2004) Stabilisation of retained austenite in laser surface melted tool steels. Mater Sci Eng A 385:123–127
Vamsi Krishna B, Bandyopadhyay A (2009) Surface modification of AISI 410 stainless steel using laser engineered net shaping (LENS™). Mater Des 30:1490–1496
Kim H-J, Kweon Y-G (1996) The effects of retained austenite on dry sliding wear behavior of carburized steels. Wear 193:8–15
Nakagawa H, Miyazaki T (1999) Effect of retained austenite on the microstructure and mechanical properties of martensitic precipitation hardening stainless steel. J Mater Sci 34:3901–3908
Bhambroo R, Roychowdhury S, Kain V, Raja V (2013) Effect of reverted austenite on mechanical properties of precipitation hardenable 17-4 stainlesssteel. Mater Sci Eng A 568:127–133
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AlMangour, B., Yang, JM. Understanding the deformation behavior of 17-4 precipitate hardenable stainless steel produced by direct metal laser sintering using micropillar compression and TEM. Int J Adv Manuf Technol 90, 119–126 (2017). https://doi.org/10.1007/s00170-016-9367-9
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DOI: https://doi.org/10.1007/s00170-016-9367-9