Abstract
The mechanical behavior and the microstructural evolution of 17-4 precipitation hardenable (PH) stainless steel processed using selective laser melting have been studied. Test coupons were produced from 17-4 PH stainless steel powder in argon and nitrogen atmospheres. Characterization studies were carried out using mechanical testing, optical microscopy, scanning electron microscopy, and x-ray diffraction. The results show that post-process heat treatment is required to obtain typically desired tensile properties. Columnar grains of smaller diameters (<2 µm) emerged within the melt pool with a mixture of martensite and retained austenite phases. It was found that the phase content of the samples is greatly influenced by the powder chemistry, processing environment, and grain diameter.
Similar content being viewed by others
References
F. Abe, K. Osakada, M. Shiomi, K. Uematsu, and M. Matsumoto, The Manufacturing of Hard Tools from Metallic Powders by Selective Laser Melting, J. Mater. Process. Technol., 2001, 111, p 210–213
G.N. Levy, The Role and Future of the Laser Technology in Additive Manufacturing Environment, Phys. Procedia, 2010, 5, p 65–80
M. Shellabear and O. Nyrhilä, DMLS—Development History and State of the Art, LANE 2004 Conference, Erlangen, Germany, Sept. 21-24, 2004
M.S. Wong, C.J. Tsopanos, and I. Sutcliffe, Owen, Selective Laser Melting of Heat Transfer Devices, Rapid Prototyping J., 2007, 13(5), p 291–297
L.E. Murr, S.A. Quinones, S.M. Gaytan, M.I. Lopez, A. Rodela, E.Y. Martinez, D.H. Hernandez, E. Martinez, F. Medina, and R.B. Wicker, Microstructure and Mechanical Behavior of Ti–6Al–4V Produced by Rapid-Layer Manufacturing, for Biomedical Applications, J Mech. Behav. Biomed., 2009, 2, p 20–32
R. Li, Y. Shi, Z. Wang, L. Wang, J. Liu, and W. Jiang, Densification Behavior of Gas and Water Atomized 316L Stainless Steel Powder During Selective Laser Melting, Appl. Surf. Sci., 2010, 256(13), p 4350–4356
L. Facchini, N. Vicente, Jr., I. Lonardelli, E. Magalini, P. Robotti, and A. Molinari, Metastable Austenite in 17–4 Precipitation-Hardening Stainless Steel Produced by Selective Laser Melting, Adv. Eng. Mater., 2010, 12(3), p 184–189
C.P. Paul, P. Ganesh, S.K. Mishra, P. Bhargava, J. Negi, and A.K. Nath, Investigating Laser Rapid Manufacturing for Inconel-625 Components, Opt. Laser Technol., 2007, 39, p 800–805
Z.H. Liu, D.Q. Zhang, and C.K. Chua, Crystal Structure Analysis of M2 High Speed Steel Parts Produced by Selective Laser Melting, Mater. Charact., 2013, 84, p 72–80
A. Takaichi, T. Nakamoto, N. Joko, N. Nomura, Y. Tsutsumi, and S. Migita, Microstructure and Mechanical Properties of Co-29Cr-6Mo Alloy Fabricated by Selective Laser Melting Process for Dental Applications, J. Mech. Behav. Biomed. Mater., 2013, 21, p 67–76
S. Pauly, L. Loeber, R. Petters, M. Stoica, S. Scudino, U. Kuehn, and J. Eckert, Processing Metallic Glasses by Selective Laser Melting, Mater. Today, 2013, 16, p 37–41
X.P. Li, C.W. Kang, H. Huang, L.C. Zhang, and T.B. Sercombe, Selective Laser Melting of an Al86Ni6Y4.5Co2La1.5 Metallic Glass: Processing, Microstructure Evolution and Mechanical Properties, Mater. Sci. Eng., A, 2014, 606, p 370–379
D. Gu and Q. Jia, Novel Crystal Growth of In Situ WC in Selective Laser Melted W-C-Ni Ternary System, J. Am. Ceram. Soc., 2014, 97(3), p 684–687
L. Thijs, M.L.M. Sistiaga, R. Wauthle, Q. Xie, J.P. Kruth, and J.V. Humbeeck, Strong Morphological and Crystallographic Texture and Resulting Yield Strength in Selective Melted Tantalum, Acta Mater., 2013, 61(12), p 4657–4668
B. Song, S. Dong, and C. Coddet, Rapid In Situ Fabrication of Fe/SiC Nanocomposites by Selective Laser Melting Directly from a Mixed Powder of Microsized Fe and SiC, Scripta Mater., 2014, 75, p 90–93
B. Vrancken, L. Thijis, J.P. Kruth, and J.V. Humbeeck, Microstructure and Mechanical Properties of a Novel β Titanium Metallic Composite by Selective Laser Melting, Acta Mater., 2014, 68, p 150–158
W.F. Smith, Structure and Properties of Engineering Alloys, 2nd ed., McGraw-Hill Inc., New York, 1993, p 328–335
M. Murayama, Y. Katayama, and K. Hono, Microstructural Evolution in a 17-4 PH Stainless Steel after Aging at 400°C, Metall. Mater. Trans. A, 1999, 30A, p 345–353
K.C. Hsu and C.K. Lin, High-Temperature Fatigue Crack Growth Behavior of 17-4 PH Stainless Steels, Metall. Mater. Trans. A, 2004, 35A, p 3018–3024
P.G.E. Jerrard, L. Hao, and K.E. Evans, Experimentation Investigation into Selective Laser Melting of Austenitic and Martensitic Stainless Steel Powder Mixtures, J Manuf. Eng., 2009, 223(11), p 1409–1416
J.H. Wu and C.K. Lin, Tensile and Fatigue Properties of 17-4 PH Stainless Steel at High Temperatures, Metall. Mater. Trans. A, 2002, 33A, p 1715–1724
U.K. Viswanathan, S. Banerjee, and R. Krishnan, Effects of Aging on the Microstructure of 17-4 PH Stainless Steel, Mater. Sci. Eng., A, 1988, 104, p 181–189
M. Shellabear and O. Nyrhila, Materials for Direct Metal Laser-Sintering, White Paper, EOS GmbH
T.L. Starr, T.J. Gornet, J.S. Usher, and C. M. Scherzer, “DMLS Mechanical Properties: Tensile and Fatigue Properties of GP1,” EOS North America Users Day, May 17, 2010
L. Thijs, F. Verhaeghe, T. Craeghs, J.V. Humbeeck, and J.P. Kruth, A Study of the Microstructural Evolution During Selective Laser Melting of Ti-6Al-4V, Acta Mater., 2010, 58, p 3303–3312
T. Vilaro, C. Colin, and J.D. Bartout, As-Fabricated and Heat-Treated Microstructures of the Ti-6Al-4V Alloy Processed by Selective Laser Melting, Metall. Mater. Trans. A, 2011, 42, p 3190–3199
E.A. Ul’yanin, N.A. Sorokina, and M. Zaretskii Ya, Properties of Austenitic Steel with Nickel and Nitrogen at Low Temperatures, Met. Sci. Heat Treat., 1969, 11(9), p 681–682
W. Wu, L.Y. Hwu, D.Y. Lin, and J.L. Lee, The Relationship Between Alloying Elements and Retained Austenite in Martensitic Stainless Steel Welds, Scripta Mater., 2000, 42, p 1071–1076
H.J. Kim and Y.G. Kweon, The Effects of Retained Austenite on Dry Sliding Wear Behavior of Carburized Steels, Wear, 1996, 193(1), p 8–15
A. Kokosza and J. Pacyna, Evaluation of Retained Austenite Stability in Heat Treated Cold Work Tool Steel, J. Mater. Process. Technol., 2005, 162, p 327–331
A.K. Bhaduri, S. Sujith, G. Srinivasan, T.P.S. Gill, and S.L. Mannan, Optimized Post Weld Heat Treatment Procedures for 17-4 PH Stainless Steels, Weld. J. Res. Suppl., 1995, 51, p 153–159
B. Rajan, S. Roychowdhury, K. Vivekanand, and V.S. Raja, Effect of Reverted Austenite on Mechanical Properties of Precipitation Hardenable 17-4 Stainless Steel, Mater. Sci. Eng., A, 2013, 568, p 127–133
S. Zhang and K.O. Findley, Quantitative Assessment of the Effects of Microstructure on the Stability of Retained Austenite in TRIP Steels, Acta Mater., 2013, 61(6), p 1895–1903
S. Takaki, K. Fukunaga, J. Syarif, and T. Tsuchiyama, Effect of Grain Refinement on Thermal Stability of Metastable Austenitic Steel, Mater. Trans., 2004, 45(7), p 2245–2251
B.H. Jiang, L. Sun, R. Li, and T.Y. Hsu, Influence of Austenite Grain Size on γ-ε Martensitic Transformation Temperature in Fe-Mn-Si-Cr Alloys, Scripta Metall. Mater., 1995, 33(1), p 63–68
R. Colaco and R. Vilar, Stabilisation of Retained Austenite in Laser Surface Melted Tool Steels, Mater. Sci. Eng., A, 2004, 385, p 123–127
B. Vamsi Krishna and A. Bandyopadhyay, Surface Modification of AISI, 410 Stainless Steel Using Laser Engineered Net Shaping (LENS™), Mater. Des., 2009, 30, p 1490–1496
R. Colaco and R. Vilar, Effect of the Processing Parameters on the Proportion of Retained Austenite in Laser Surface Melted Tool Steels, J. Mater. Sci. Lett., 1998, 17(7), p 563–567
D. Das, A.K. Dutta, and K.K. Ray, Sub-zero Treatments of AISI, D2 steel: Part I. Microstructure and Hardness, Mater. Sci. Eng., A, 2010, 527, p 2182–2193
Acknowledgments
The authors thank Office of Naval Research for support through Grant Numbers N00014‐09‐1‐0147 and N00014‐10‐1‐0800.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Rafi, H.K., Pal, D., Patil, N. et al. Microstructure and Mechanical Behavior of 17-4 Precipitation Hardenable Steel Processed by Selective Laser Melting. J. of Materi Eng and Perform 23, 4421–4428 (2014). https://doi.org/10.1007/s11665-014-1226-y
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-014-1226-y