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Recent Developments in Femtosecond Laser-Enabled TriBeam Systems

  • Short Pulsed Lasers for Materials Modification, Characterization, and Synthesis
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Abstract

Streams of multimodal three-dimensional (3D) and four-dimensional (4D) data are revolutionizing our ability to design and predict the behavior of a broad array of advanced materials systems. Over the last 10 years, a new 3D imaging platform consisting of a femtosecond (fs) pulsed laser coupled with a focused ion beam scanning electron microscope (FIB SEM) has been developed by UC Santa Barbara in collaboration with Thermo Fisher Scientific (formerly FEI). The femtosecond-laser-enabled FIB SEM, called the TriBeam, has become one of the only 3D serial sectioning methods available that can gather millimeter-scaled multimodal datasets at sub-\(\mu \)m voxel resolutions; these length scales are critical for many materials problems. Multimodal chemical, crystallographic, and morphological information can be gathered rapidly on a layer-by-layer basis and reconstructed in 3D. Large (gigabyte to terabyte scale) 3D datasets have been generated for a broad array of materials systems, including metallic alloys, ceramics, biomaterials, polymer- and ceramic-matrix composites, and semiconductors. The research tasks performed have resulted in a completely new design, operating with a dual-wavelength femtosecond-pulsed laser on a plasma focused ion beam (PFIB) platform.

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Acknowledgements

Sandia National Laboratories is a multimission laboratory managed and operated by National Technology and Engineering Solutions of Sandia, LLC, a wholly owned subsidiary of Honeywell International, Inc., for the US Department of Energy’s National Nuclear Security Administration under Contract DE-NA-0003525. M.P.E., T.M.P., and J.L. gratefully acknowledge the support of ONR Grant N00014-18-1-2794.

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Authors and Affiliations

  1. Materials Department, University of California Santa Barbara, Santa Barbara, California, 93106, USA

    McLean P. Echlin, Andrew T. Polonsky, James Lamb & Tresa M. Pollock

  2. Materials Mechanics and Tribology Department, Sandia National Laboratories, Albuquerque, New Mexico, 87185, USA

    Andrew T. Polonsky

  3. Thermo Fisher Scientific, 5651GG, Eindhoven, The Netherlands

    Remco Geurts

  4. Thermo Fisher Scientific, Hillsboro, Oregon, 97124, USA

    Steven J. Randolph & Aurélien Botman

  5. Oak Ridge National Laboratory, Center for Nanophase Materials Sciences, Oak Ridge, Tennessee, 37831, USA

    Steven J. Randolph

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Echlin, M.P., Polonsky, A.T., Lamb, J. et al. Recent Developments in Femtosecond Laser-Enabled TriBeam Systems. JOM 73, 4258–4269 (2021). https://doi.org/10.1007/s11837-021-04919-0

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