Skip to main content

Advertisement

Log in

Effect of Tempering on the Microstructure and Tensile Properties of a Martensitic Medium-Mn Lightweight Steel

  • Published:
Metallurgical and Materials Transactions A Aims and scope Submit manuscript

Abstract

In the present study a Fe-8.8Mn-5.1Al-0.31C (wt pct) medium-Mn lightweight steel with martensitic matrix was newly designed, and the effect of tempering on its microstructure and tensile properties was investigated. When the medium-Mn lightweight steel specimen was quenched from annealing temperature of 1373 K (1100 °C), it revealed a triple-phase microstructure consisting of 64.6 pct fresh martensite, 20.2 pct ferrite, and 15.2 pct retained austenite. Tempering the as-quenched specimen at temperatures less than 573 K (300 °C) induced the precipitation of thin cementite or κ-carbide platelets in tempered martensite. With the increasing tempering temperature, the type of precipitate changed from cementite to κ-carbide, and thickening of platelets with the longer interspacing was observed by means of transmission electron microscopy and atom probe tomography. While the as-quenched specimen revealed high strain-hardening rate (SHR) and poor elongation (< 2 pct), tempered specimens exhibited moderate SHR and improved elongation (> 16.8 pct) mainly due to gradual transformation-induced plasticity in retained austenite stabilized by tempering. In particular, the 373 K (100 °C)-tempered specimen with tempered martensite embedded with thin cementite platelets revealed ultrahigh strengths (yield strength of 945 MPa and ultimate tensile strength of ~ 1.56 GPa) with moderate elongation of ~ 16.8 pct.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9

Similar content being viewed by others

Data Availability

The authors confirm that the data supporting the findings of this study are available within the article and its supplementary materials.

References

  1. 1.B.C. De Cooman: Curr. Opin. Solid State Mater. Sci., 2004, vol. 8, pp. 285-303.

    Article  Google Scholar 

  2. 2.G.K. Tirumalasetty, M.A. Van Huis, C. Kwakernaak, J. Sietsma, W.G. Sloof, H.W. Zandbergen: Acta Mater. 2012, vol. 60, pp. 1311-1321.

    Article  Google Scholar 

  3. 3.P.J. Gibbs, E. De Moor, M.J. Merwin, B. Clausen, J.G. Speer, D.K. Matlock: Metall. Mater. Trans. A, 2011, vol. 42, pp. 3691-3702.

    Article  Google Scholar 

  4. 4.G.-H. Kang, S. Duan, S.-J. Kim, W. Bleck: Metall. Mater. Trans. A, 2016, vol. 47, pp. 1918-1921.

    Article  Google Scholar 

  5. 5.O. Bouaziz, S. Allain, C.P. Scott, P. Cugy, D. Baribier: Curr. Opin. Solid State Mater. Sci., 2011, vol. 15, pp. 141-168.

    Article  Google Scholar 

  6. 6.I. Gutierrez-Urrutia, D. Raabe: Acta Mater., 2011, vol. 59, pp. 6449-6462.

    Article  Google Scholar 

  7. 7.G. Frommeyer, U. Brüx: Steel Res. Int., 2006, vol. 77, pp. 627-633.

    Article  Google Scholar 

  8. 8.K.-T. Park, K.G. Jin, S.H. Han, S.W. Hwang: Mater. Sci. Eng. A, 2010, vol. 483, pp. 184-187.

    Google Scholar 

  9. 9.K.-T. Park: Scr. Mater., 2013, vol. 68, pp. 375-379.

    Article  Google Scholar 

  10. 10.K. Choi, C.-H. Seo, H. Lee, S.K. Kim, J.-H. Kwak, K.G. Chin, K.-T. Park, N.J. Kim: Scr. Mater., 2010, vol. 63, pp. 1028-1031.

    Article  Google Scholar 

  11. 11.K.M. Chang, C.G. Chao, T.F. Liu: Scr. Mater., 2010, vol. 63, pp. 162-165.

    Article  Google Scholar 

  12. 12.C.L. Lin, C.G. Chao, H.Y. Bor, T.F. Liu: Mater. Trans. JIM., 2010, vol. 51, pp. 1084-1088.

    Article  Google Scholar 

  13. 13.C.L. Lin, C.G. Chao, J.Y. Juang, J.M. Yang, T.F. Liu: J. Alloys Compd., 2014, vol. 586, pp. 16-20.

    Article  Google Scholar 

  14. 14.I. Gutierres-Urrutia, D. Raabe: Acta Mater., 2012, vol. 60, pp. 5791-5802.

    Article  Google Scholar 

  15. 15.I. Gutierres-Urrutia, D. Raabe: Mater. Sci. Tech., 2014, vol. 30, pp. 1099-1104.

    Article  Google Scholar 

  16. 16.H. Springer, D. Raabe: Acta Mater., 2012, vol. 60, pp. 4950-4959.

    Article  Google Scholar 

  17. 17.I. Gutierres-Urrutia, D. Raabe: Scr. Mater., 2013, vol. 68, pp. 343-347.

    Article  Google Scholar 

  18. E. Welsch, D. Ponge, S.M.H. Haghighat, S. Sandlobes, P. Choi, M. Herbig, S. Zaefferer, D. Raabe: Acta Mater., 2016, vol. 116, pp. 188-199.

    Article  Google Scholar 

  19. 19.Y. Satou, M. Kamiya, R. Umino, I. Ohnuma, K. Ishida: ISIJ Int., 2010, vol. 50, pp. 893-899.

    Article  Google Scholar 

  20. 20.S.H. Kim, H. Kim, N.J. Kim: Nature, 2015, vol. 518, pp. 77-88.

    Article  Google Scholar 

  21. 21.S.-Y. Shin, H. Lee, S.-Y. Han, C.-H. Seo, K. Choi, S. Lee, N.J. Kim, J.-H. Kwak, K.-G. Chin: Metall. Mater. Trans. A, 2010, vol. 41, pp. 138-148.

    Article  Google Scholar 

  22. 22.S.-Y. Han, S.-Y. Shin, H.-J. Lee, B.-J. Lee, S. Lee, N.J. Kim, J.-H. Kwak: Metall. Mater. Trans. A, 2012, vol. 43, pp. 843-853.

    Article  Google Scholar 

  23. 23.S.S. Sohn, B.-J. Lee, J.-H. Kwak, S. Lee: Acta Mater., 2013, vol. 61, pp. 5626-5635.

    Article  Google Scholar 

  24. 24.S.S. Sohn, B.-J. Lee, J.-H. Kwak, S. Lee: Metall. Mater. Trans. A, 2014, vol. 45, pp. 3844-3856.

    Article  Google Scholar 

  25. 25.S.S. Sohn, B.-J. Lee, J.-H. Kwak: Met. Mater. Int., 2015, vol. 21, pp. 43-53.

    Article  Google Scholar 

  26. 26.R.-C. Xu, Y.-L. He, H. Jiang, H. Wang, N.-Q. Zhu, X.-G. Lu, L. Li: J. Iron Steel Res. Int., 2017, vol. 24, pp. 737-742.

    Article  Google Scholar 

  27. 27.H. Song, S.G. Lee, S.S. Sohn, J.-H. Kwak, S. Lee: Metall. Mater. Trans. A, 2016, vol. 47, pp. 5372-5392.

    Article  Google Scholar 

  28. 28.S.S. Sohn, B.-J. Lee, S. Lee, N.J. Kim, J.-H. Kwak: Acta Mater., 2013, vol. 61, pp. 5050-5066.

    Article  Google Scholar 

  29. 29.S.S. Sohn, K. Choi, J.-H. Kwak, N.J. Kim, S. Lee: Acta Mater., 2014, vol. 78, pp. 181-189.

    Article  Google Scholar 

  30. 30.C.-H. Seo, K.H. Kwon, K. Choi, K.-H. Kim, S. Lee, N.J. Kim: Scr. Mater., 2012, vol. 66, pp. 519-522.

    Article  Google Scholar 

  31. 31.S.S. Sohn, H. Song, J.G. Kim, J.-H. Kwak, H.-S. Kim, S. Lee: Metal. Mater. Trans. A, 2016, vol. 47, pp. 706-717.

    Article  Google Scholar 

  32. 32.S.S. Sohn, S. Lee, B.-J. Lee, J.-H. Kwak: JOM, 2014, vol. 66, pp. 1857-1867.

    Article  Google Scholar 

  33. 33.J. Park, M.C. Jo, H.J. Jeong, S.S. Sohn, J.-H. Kwak, H.S. Kim, S. Lee: Sci. Rep., 2017, vol. 7, pp. 15726.

    Article  Google Scholar 

  34. 34.S.S. Sohn, H. Song, J.-H. Kwak, S. Lee: Sci. Rep., 2017, vol. 7, pp. 1927.

    Article  Google Scholar 

  35. 35.H. Song, S.S. Sohn, J.-H. Kwak, B.-J. Lee, S. Lee: Metal. Mater. Trans. A, 2016, vol. 47, pp. 2674-2685.

    Article  Google Scholar 

  36. 36.C.-Y. Lee, J. Jeong, J. Han, S.-J. Lee, S. Lee, Y.-K. Lee: Acta Mater., 2015, vol. 84, pp. 1-8.

    Article  Google Scholar 

  37. 37.J. Jeong, C.-Y. Lee, I.-J. Park, Y.-K. Lee: J. Alloys Compd., 2013, vol. 574, pp. 299-304.

    Article  Google Scholar 

  38. 38.S. Lee, J. Jeong, Y.-K. Lee: J. Alloys Compd., 2015, vol. 648, pp. 149-153.

    Article  Google Scholar 

  39. 39.J. Mahieu, J. Maki, B.C. De Cooman, S. Claessens: Metall. Mater. Trans. A, 2002, vol. 33, pp. 2573-2580.

    Article  Google Scholar 

  40. Thermo-Calc. Database TCFE2000, upgraded by Lee, B.-J. & Sundman, B., Stockholm., KTH, 1999.

  41. 41.K.-G. Chin, H.-J. Lee, J.-H. Kwak, J.-Y. Kang, B.-J. Lee: J. Alloys Compd., 2010, vol. 505, pp. 217-223.

    Article  Google Scholar 

  42. 42.J.E. Jin, Y.-K. Lee: Acta Mater., 2012, vol. 60, pp. 1680-1688.

    Article  Google Scholar 

  43. 43.D. Fahr: Metall. Trans., 1971, vol. 2, pp. 1883-1892.

    Google Scholar 

  44. 44.S.S. Babu, E.D. Specht, S.A. David, E. Karapetrova, P. Zschack, M. Peet, H.K.D.H. Bhadeshia: Metall. Mater. Trans. A, 2005, vol. 36, pp. 2005-3281.

    Google Scholar 

  45. 45.M.A. Maleque, S. Dyuti: Int. J. Mech. Mater. Eng., 2010, vol. 5, pp. 95-100.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Young-Kook Lee.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Manuscript submitted November 21, 2018.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Lee, S., Kang, SH., Nam, JH. et al. Effect of Tempering on the Microstructure and Tensile Properties of a Martensitic Medium-Mn Lightweight Steel. Metall Mater Trans A 50, 2655–2664 (2019). https://doi.org/10.1007/s11661-019-05190-4

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11661-019-05190-4

Navigation