Abstract
Semi-solid powder rolling (SSPR) is a novel strip manufacturing process, which combines powder rolling with semi-solid rolling in one step. Based on the features of SSPR, powders were heated to the semi-solid temperature range and then rolled. Therefore, oxides will form during heating and rolling. The oxidation behavior of 7050 aluminum during SSPR was analyzed and the quantity, distribution and morphology of oxides are discussed. The effects of quantity, distribution and morphology of the oxides on the microhardness of strips under different conditions were studied. The results showed that the main factor influencing the quantity of oxides is the heating temperature. The mechanism of oxidation during SSPR was found to be diffusion controlled. In the heating stage, surface oxide films hinder the diffusion. In the rolling stage, surface oxide layers were broken and so the oxidation of aluminum alloy mainly took place in the rolling stage. The formed oxides are Al2O3 with a little of MgO showing an irregular morphology with a size of 2–3 µm. High bonding quality between the oxide particles and the matrix, as well as an uniform distribution of the oxides, leads to a higher microhardness of the SSPR-ed strips. But, the bonding quality between the oxide particles and the matrix is poor under conditions of low liquid fraction and some oxides distribute non-uniformly around the grain boundaries.
Similar content being viewed by others
References
Y. Z. Liu, X. Luo and Z. L. Li, The Journal of Materials Processing Technology 214, 2014 (165).
Y. J. Lang, Y. H. Cai, H. Cui and J. S. Zhang, Materials & Design 32, 2011 (4241).
C. G. Kang, J. H. Yoon and Y. H. Seo, The Journal of Materials Processing Technology 66, 1997 (30).
W. Y. Kim, C. G. Kang and B. M. Kim, The Journal of Materials Processing Technology 191, 2007 (372).
W. G. Cho and C. G. Kang, The Journal of Materials Processing Technology 105, 2000 (269).
M. Suery and M. C. Flemings, Metallurgical and Materials Transactions A 13, 1982 (1809).
Y. F. Wu and G.-Y. Kim, Powder Technology 214, 2011 (252).
Y. F. Wu, G.-Y. Kim, I. E. Anderson, et al., Acta Materialia 58, 2010 (4398).
Y. F. Wu, G.-Y. Kim and A. M. Russel, Materials Science and Engineering 538, 2012 (164).
Y. F. Wu and G.-Y. Kim, The Journal of Materials Processing Technology 211, 2011 (1341).
Y.F. Wu, Fabrication of metal matrix composite by semisolid powder processing. 2011, Ph.D Thesis, Iowa State University, IA.
R. F. Smart and E. C. Ellwood, Nature. 181, 1958 (833).
R. Q. Guo, P. K. Rohatgi and D. Nath, The Journal of Materials Science 32, 1997 (3971).
M. Zabihi, M. R. Toroghinejad and A. Shafyei, Materials Science and Engineering 560, 2013 (567).
H. Asteman, W. Hartnagel and D. Jakobi, Oxidation of Metals 80, 2013 (3).
F. Velasco, S. Guzman, C. Moral and A. Bautista, Oxidation of Metals 80, 2013 (403).
J. F. Perez and D. G. Morris, Scripta Materialia 31, 1994 (231).
H. Liu, X. Zeng and E. J. Lavernia, Scripta Materialia 29, 1993 (1341).
S. Hasani, M. Panjepour and M. Shamanian, Oxidation of Metals 78, 2012 (179).
W. D. Cai, J. Smugeresky and E. J. Lavernia, Materials Science and Engineering 241, 1998 (60).
D. R. Lide, The CRC Chemistry and Physics Handbook, (CRC Press, Ann Arbor, 1995).
A. D. Mcleod and C. M. Gabryel, Metallurgical and Materials Transactions A 23, 1992 (1279).
R. N. Lumley, T. B. Sercombe and G. B. Schaffer, Metallurgical and Materials Transactions A 30A, 1999 (457).
R. M. Wang, M. K. Surappa, C. H. Tao, et al., Materials Science and Engineering 254, 1998 (219).
X. Luo, Y. Z. Liu, C. X. Gu and Z. L. Li, Powder Technology 261, 2014 (161).
J.-P. Delplanque, E. J. Lavernia and R. H. Range, Journal of Heat Transfer 122, 2000 (126).
S. K. Vajpai, R. K. Dube and S. Sangal, Materials Science and Engineering 529, 2011 (378).
J. D. Robson, Materials Science and Engineering 382, 2004 (112).
K. Shen, J. L. Chen and Z. M. Yin, The Transactions of Nonferrous Metals Society of China 19, 2009 (1405).
J. Buha, R. N. Lumley and A. G. Crosky, Materials Science and Engineering 492, 2008 (1).
D. Dumont, A. Deschamps and Y. Brechet, Materials Science and Engineering 356, 2003 (32).
Acknowledgments
The authors gratefully acknowledge the financial supports from Fundamental Research Funds for the Central Universities (Grant No. 2011ZZ0010) and Science and Technology Innovation Project of Guangdong Provincial Department of Education (2013KJCX0014).
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Luo, X., Liu, Y. & Jia, H. The Oxidation Behaviors of 7,050 Aluminum Strips During Semi-solid Powder Rolling and Mechanical Properties of Strips. Oxid Met 83, 55–70 (2015). https://doi.org/10.1007/s11085-014-9499-y
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11085-014-9499-y