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Mn-Fe Layered Double Hydroxide Modified Cellulose-Based Membrane for Sustainable Anionic Pollutant Removal

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Abstract

This study aimed to investigate the adsorption of As(V), phosphate, and textile dye Acid Green 25 (AG-25) on layered double hydroxides Mn-Fe_LDH and corresponding membranes (wCell/Mn-Fe_LDH). The wCell membrane, derived from waste tobacco boxes, was formed by cross-linking of epoxy and amino modified cellulose fibers with epoxy modified Mn-Fe_LDH and lysine as cross-linker. Structural and morphological analyses were conducted for Mn-Fe_LDH and wCell/Mn-Fe_LDH. The batch system explored pH, contact time, temperature, and initial concentration effects on wCell/Mn-Fe_LDH adsorption efficiency. Adsorption capacities of 82.71, 106.9, and 130.3 mg g−1 were achieved for As(V), phosphate, and AG-25, respectively, indicating effective anionic species removal. Kinetic analysis suggested intraparticle diffusion as the rate-limiting step. Thermodynamic parameters and ionic strength effects indicated a physisorption mechanism for AG-25 and surface complexation for As(V) and phosphate. Biodegradation experiments after five adsorption/desorption cycles revealed the membrane’s decomposition, with phosphate’s strong bonding releasing essential elements valuable for soil fertilization. Effluent wastewater treatment demonstrated low environmental impact through the formation of insoluble As(V) salts and photocatalytic dye degradation.

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Acknowledgements

This work was supported by the Ministry of Science, Technological Development and Innovations of the Republic of Serbia (Contract Grants No. 451-03-47/2023-01/200135, 451-03-47/2023-01/200017, and 451-03-47/2023-01/200326).

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Authors and Affiliations

  1. University of Belgrade, Faculty of Technology and Metallurgy, Department of Organic Chemistry, Karnegijeva 4, 11000, Belgrade, Serbia

    Muna Abdualatif Abduarahman & Aleksandar Marinković

  2. Department of Biology, Faculty of Science, University of Sabratha, Sabratha, Libya

    Muna Abdualatif Abduarahman

  3. University of Belgrade, Department of Chemical Dynamics and Permanent Education, “VINČA” Institute of Nuclear Sciences - National Institute of the Republic of Serbia, Mike Petrovića Alasa 12-14, Belgrade, 11351, Serbia

    Marija M. Vuksanović, Adela Egelja & Andrija Savić

  4. University of Belgrade, Institute of Chemistry, Technology and Metallurgy - National Institute of the Republic of Serbia, Department of Ecology and TechnoEconomics, Njegoševa 12, Belgrade, 11000, Serbia

    Milena Milošević

  5. University of Defence, Military Academy, Veljka Lukića Kurjaka 33, Belgrade, 11000, Serbia

    Zlate Veličković

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Contributions

M. A. A.: Conceptualization, Investigation, Data curation, Writing—original draft preparation; M. M. V.: Investigation, Formal analysis, Writing—reviewing and editing; M. M.: Investigation, Visualization, Formal analysis, Writing—reviewing and editing; A. E.: Investigation, Formal analysis; A. S.: Investigation Validation, Data Curation; Z. V.: Investigation, Data Curation; A. M.: Conceptualization, Resources, Validation, Supervision.

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Abduarahman, M.A., Vuksanović, M.M., Milošević, M. et al. Mn-Fe Layered Double Hydroxide Modified Cellulose-Based Membrane for Sustainable Anionic Pollutant Removal. J Polym Environ (2024). https://doi.org/10.1007/s10924-024-03192-x

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