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Adsorption of Cationic Dye onto ZSM-5 Zeolite-Based Bio Membrane: Characterizations, Kinetics and Adsorption Isotherm

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Abstract

In this study, we report polyvinyl alcohol/carboxymethyl cellulose/gelatin/ZSM-5 zeolite (PVA/CMC/GEL/ZSM-5) membrane for cationic dye (rhodamine B, Rh B) removal from aqueous solution. The prepared membrane was characterized using different techniques such as Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), scanning electron microscopy (SEM), optical microscopy (OM), universal testing machine (UTM) and water contact angle respectively. XRD, FT-IR and SEM analysis indicates successful incorporation of zeolite into PVA/CMC/GEL membrane. The improved hydrophobicity of the zeolite loaded membrane was confirmed by contact angle analysis. The Rh B removal efficiency of zeolite loaded PVA/CMC/GEL membrane was investigated through batch adsorption technique. The effect of different parameters such as initial dye concentration, zeolite dosage, contact time, temperature and pH on the adsorption was examined. Rh B dye adsorption onto the membrane followed Freundlich isotherm model. The kinetic studies revealed that Rh B dye adsorption on the membrane could be explained using pseudo-second-order model. Finally, the recyclability test revealed that the membrane exhibits good recycle efficiency and is stable after six recycle.

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Acknowledgements

Authors gratefully thanks the Centre of Innovation in Design and Engineering for Manufacturing (CoI- DEM), KMUTNB, Thailand for characterization facilities to carry out this study. The study was financially supported by the King Mongkut's University of Technology North Bangkok (KMUTNB), Thailand through the Post-Doctoral Program (Grant Nos. KMUTNB-64-Post-03 and KMUTNB-63-Post-03 to SR)

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Authors and Affiliations

  1. Materials and Production Engineering, The Sirindhorn International Thai-German Graduate School of Engineering (TGGS), King Mongkut’s University of Technology North Bangkok, Bangkok, 10800, Thailand

    Sabarish Radoor, Aswathy Jayakumar, Debabrata Nandi & Suchart Siengchin

  2. Government Women’s Polytechnic College, Calicut, Kerala, India

    Jasila Karayil

  3. Department of Science, Faculty of Science & Technology, Alliance University, Chandapura-Anekal Main Road, Bengaluru, Karnataka, 562106, India

    Jyotishkumar Parameswaranpillai

  4. Department of Polymer-Nano Science and Technology, Jeonbuk National University, 567 Baekje-daero, Deokjin-gu, Jeonju-si, 54896, Korea

    Jaewoo Lee

  5. Department of Bionanotechnology and Bioconvergence Engineering, Jeonbuk National University, 567 Baekje-daero, Deokjin-gu, Jeonju-si, 54896, Korea

    Jaewoo Lee

  6. AMC Engineering College, Bannerghatta Main Road, Bengaluru, Karnataka, 560083, India

    Jyothi Mannekote Shivanna

  7. Department of Industrial Biotechnology, Government College of Technology, Coimbature, 641027, India

    Rajarathinam Nithya

  8. Institute of Plant and Wood Chemistry, Technische Universität Dresden, Pienner Str. 19, 01737, Tharandt, Germany

    Suchart Siengchin

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  1. Sabarish Radoor
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Radoor, S., Karayil, J., Jayakumar, A. et al. Adsorption of Cationic Dye onto ZSM-5 Zeolite-Based Bio Membrane: Characterizations, Kinetics and Adsorption Isotherm. J Polym Environ 30, 3279–3292 (2022). https://doi.org/10.1007/s10924-022-02421-5

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