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Influence of laser process on the porosity-related defects, microstructure and mechanical properties for selective laser melted AlSi10Mg alloy

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Abstract

Correlations among the laser process, microstructure, porosity-related defects, and mechanical properties for selective laser melted AlSi10Mg alloy were investigated through experiments. A series of samples were produced with various laser parameters, and the porosity-related defects and microstructure were characterized by using X-ray computed tomography and scanning electron microscope. A model is proposed based on the energy density to reflect the evolution of the sample density with changing laser parameters; the optimal energy density level is evident when the sample density reaches 99.5%. Furthermore, the model has good applicability for both the volumetric energy density and deposited energy density parameters. In addition, defect evolution with increasing energy density, namely, the transition from lack of fusion defect domination to pore defect domination, is identified by considering anisotropy and sphericity factors simultaneously. The results also indicate that the porosity and Al-Si eutectic microcell have different effects on the mechanical properties. The negative correlation between the cell size and microhardness is built. The tensile strength highly depends on the porosity while the yield strength is mainly associated with the Al-Si eutectic structure.

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The authors confirm that the data supporting the findings of this study are available within the article and its supplementary materials.

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Notes

  1. The equivalent diameter of a defect is defined as \({D}_{eq}=\sqrt[3]{\frac{6\times {\text{Volume}}}{\pi }}\) [32]

References

  1. Steenhuis H, Fang X, Ulusemre T (2020) Global diffusion of innovation during the fourth industrial revolution: The case of additive manufacturing or 3D printing. Int J Technol Manage 17:2050005. https://doi.org/10.1142/S0219877020500054

    Article  Google Scholar 

  2. Zhang H, Zhu H, Qi T, Hu Z, Zeng X (2016) Selective laser melting of high strength Al–Cu–Mg alloys: Processing, microstructure and mechanical properties. Mater Sci Eng A 656:47–54. https://doi.org/10.1016/j.msea.2015.12.101

    Article  Google Scholar 

  3. Biffi CA, Fiocchi J, Tuissi A (2018) Selective laser melting of AlSi10Mg: Influence of process parameters on Mg2Si precipitation and Si spheroidization. J Alloy Compd 755:100–107. https://doi.org/10.1016/j.jallcom.2018.04.298

    Article  Google Scholar 

  4. Yan C, Hao L, Hussein A, Young P, Huang J, Zhu W (2015) Microstructure and mechanical properties of aluminium alloy cellular lattice structures manufactured by direct metal laser sintering. Mater Sci Eng A 628:238–246. https://doi.org/10.1016/j.msea.2015.01.063

    Article  Google Scholar 

  5. Gu D, Wang H, Dai D, Chang F, Meiners W, Hagedorn Y, Wissenbach L, Kelbassa I, Poprawe R (2015) Densification behavior, microstructure evolution, and wear property of TiC nanoparticle reinforced AlSi10Mg bulk-form nanocomposites prepared by selective laser melting. J Laser Appl 27:S17003. https://doi.org/10.2351/1.4870877

    Article  Google Scholar 

  6. Han Q, Jiao Y (2019) Effect of heat treatment and laser surface remelting on AlSi10Mg alloy fabricated by selective laser melting. Int J Adv Manuf Technol 102:3315–3324. https://doi.org/10.1007/s00170-018-03272-y

    Article  Google Scholar 

  7. Wu H, Ren J, Huang Q, Zai X, Liu L, Chen C, Liu S, Yang X, Li R (2018) Effect of laser parameters on microstructure, metallurgical defects and property of AlSi10Mg printed by selective laser melting. J Micromech Mol Phys 02:1750017. https://doi.org/10.1142/S2424913017500175

    Article  Google Scholar 

  8. Biffi CA, Fiocchi J, Valenza F, Bassani P, Tuissi A (2020) Selective laser melting of NiTi shape memory alloy: Processability, microstructure, and superelasticity. Shape Mem Superelast 6:342–353. https://doi.org/10.1007/s40830-020-00298-8

    Article  Google Scholar 

  9. Trevisan F, Calignano F, Lorusso M, Pakkanen J, Aversa A, Ambrosio E, Lombardi M, Fino P, Manfredi D (2017) On the Selective Laser Melting (SLM) of the AlSi10Mg Alloy: Process, Microstructure, and Mechanical Properties. Mater 10:76. https://doi.org/10.3390/ma10010076

    Article  Google Scholar 

  10. Li Z, Kuai Z, Bai P, Nie Y, Fu G, Liu W, Yang S (2019) Microstructure and tensile properties of AlSi10Mg alloy manufactured by multi-laser beam Selective Laser Melting (SLM). Metal 9:1337. https://doi.org/10.3390/met9121337

    Article  Google Scholar 

  11. Franczyk E, Machno M, Zębala W (2021) Investigation and optimization of the SLM and WEDM processes’ parameters for the AlSi10Mg-sintered part. Mater 14:410. https://doi.org/10.3390/ma14020410

    Article  Google Scholar 

  12. Aboulkhair NT, Everitt NM, Ashcroft I, Tuck C (2014) Reducing porosity in AlSi10Mg parts processed by selective laser melting. Addit Manuf 1–4:77–86. https://doi.org/10.1016/j.addma.2014.08.001

    Article  Google Scholar 

  13. Louvis E, Fox P, Sutcliffe CJ (2011) Selective laser melting of aluminium components. J Mater Process Technol 211:275–284. https://doi.org/10.1016/j.jmatprotec.2010.09.019

    Article  Google Scholar 

  14. Kempen K, Thijs L, Van J, Humbeeck KJP (2015) Processing AlSi10Mg by selective laser melting: parameter optimisation and material characterization. Mater Sci Technol 31:917–923. https://doi.org/10.1179/1743284714Y.0000000702

    Article  Google Scholar 

  15. Wei P, Wei Z, Chen Z, Du J, He Y, Li J, Zhou Y (2017) The AlSi10Mg samples produced by selective laser melting: single track, densification, microstructure and mechanical behavior. Appl Surf Sci 408:38–50. https://doi.org/10.1016/j.apsusc.2017.02.215

    Article  Google Scholar 

  16. Rao H, Giet S, Yang K, Wu X, Davies CHJ (2016) The influence of processing parameters on aluminium alloy A357 manufactured by Selective Laser Melting. Mater Des 109:334–346. https://doi.org/10.1016/j.matdes.2016.07.009

    Article  Google Scholar 

  17. Xiong ZH, Liu SL, Li SF, Shi Y, Yang YF, Misra RDK (2019) Role of melt pool boundary condition in determining the mechanical properties of selective laser melting AlSi10Mg alloy. Mater Sci Eng A 740–741:148–156. https://doi.org/10.1016/j.msea.2018.10.083

    Article  Google Scholar 

  18. Wang L, Wang S, Hong X (2018) Pulsed SLM-manufactured AlSi10Mg alloy: Mechanical properties and microstructural effects of designed laser energy densities. J Manuf Process 35:492–499. https://doi.org/10.1016/j.jmapro.2018.09.007

    Article  Google Scholar 

  19. Read N, Wang W, Essa K, Attallah MM (2015) Selective laser melting of AlSi10Mg alloy: Process optimisation and mechanical properties development. Mater Des 65:417–424. https://doi.org/10.1016/j.matdes.2014.09.044

    Article  Google Scholar 

  20. Suzuki A, Nishida R, Takata N, Kobashi M, Kato M (2019) Design of laser parameters for selectively laser melted maraging steel based on deposited energy density. Addit Manuf 28:160–168. https://doi.org/10.1016/j.addma.2019.04.018

    Article  Google Scholar 

  21. Weingarten C, Buchbinder D, Pirch N, Meiners W, Wissenbach K, Poprawe R (2015) Formation and reduction of hydrogen porosity during selective laser melting of AlSi10Mg. J Mater Process Technol 221:112–120. https://doi.org/10.1016/j.jmatprotec.2015.02.013

    Article  Google Scholar 

  22. Bauereiß A, Scharowsky T, Körner C (2014) Defect generation and propagation mechanism during additive manufacturing by selective beam melting. J Mater Process Technol 214:2522–2528. https://doi.org/10.1016/j.jmatprotec.2014.05.002

    Article  Google Scholar 

  23. Gong H, Rafi K, Gu H, Starr T, Stucker B (2014) Analysis of defect generation in Ti–6Al–4V parts made using powder bed fusion additive manufacturing processes. Addit Manuf 1–4:87–98. https://doi.org/10.1016/j.addma.2014.08.002

    Article  Google Scholar 

  24. Leung CLA, Marussi S, Atwood RC, Towrie M, Withers PJ, Lee PD (2018) In situ X-ray imaging of defect and molten pool dynamics in laser additive manufacturing. Nat Commum 9:1355. https://doi.org/10.1038/s41467-018-03734-7

    Article  Google Scholar 

  25. Sanaei N, Fatemi A (2021) Defects in additive manufactured metals and their effect on fatigue performance: A state-of-the-art review. Prog Mater Sci 117:100724. https://doi.org/10.1016/j.pmatsci.2020.100724

    Article  Google Scholar 

  26. Wu SC, Xiao TQ, Withers PJ (2017) The imaging of failure in structural materials by synchrotron radiation X-ray microtomography. Eng Fract Mech 182:127–156. https://doi.org/10.1016/j.engfracmech.2017.07.027

    Article  Google Scholar 

  27. Maskery I, Aboulkhair NT, Corfield MR, Tuck C, Clare AT, Leach RK, Wildman RD, Ashcroft IA, Hague RJM (2016) Quantification and characterisation of porosity in selectively laser melted Al–Si10–Mg using X-ray computed tomography. Mater Charact 111:193–204. https://doi.org/10.1016/j.matchar.2015.12.001

    Article  Google Scholar 

  28. Romano S, Abel A, Gumpinger J, Brandão AD, Beretta S (2019) Quality control of AlSi10Mg produced by SLM: Metallography versus CT scans for critical defect size assessment. Addit Manuf 28:394–405. https://doi.org/10.1016/j.addma.2019.05.017

    Article  Google Scholar 

  29. Wang P, Zhou H, Zhang L, Chen H, Zhu X, Lei H, Fang D (2020) In situ X-ray micro-computed tomography study of the damage evolution of prefabricated through-holes in SLM-Printed AlSi10Mg alloy under tension. J Alloy Compd 821:153576. https://doi.org/10.1016/j.jallcom.2019.153576

    Article  Google Scholar 

  30. Cunningham R, Narra SP, Ozturk T, Beuth J, Rollett AD (2016) Evaluating the effect of processing parameters on porosity in electron beam melted Ti–6Al–4V via synchrotron X-ray microtomography. JOM 68:765–771. https://doi.org/10.1007/s11837-015-1802-0

    Article  Google Scholar 

  31. Cunningham R, Narra SP, Montgomery C, Beuth J, Rollett AD (2017) Synchrotron-based X-ray microtomography characterization of the effect of processing variables on porosity formation in laser power-bed additive manufacturing of Ti–6Al–4V. JOM 69:479–484. https://doi.org/10.1007/s11837-016-2234-1

    Article  Google Scholar 

  32. Tammas-Williams S, Zhao H, Léonard F, Derguti F, Todd I, Prangnell PB (2015) XCT analysis of the influence of melt strategies on defect population in Ti–6Al–4V components manufactured by Selective Electron Beam Melting. Mater Charact 102:47–61. https://doi.org/10.1016/j.matchar.2015.02.008

    Article  Google Scholar 

  33. Kasperovich G, Hausmann J (2015) Improvement of fatigue resistance and ductility of TiAl6V4 processed by selective laser melting. J Mater Process Technol 220:202–214. https://doi.org/10.1016/j.jmatprotec.2015.01.025

    Article  Google Scholar 

  34. Zhou X, Dai N, Chu M, Wang L, Li D, Zhou L, Cheng X (2020) X-ray CT analysis of the influence of process on defect in Ti–6Al–4V parts produced with Selective Laser Melting technology. Int J Adv Manuf Technol 106:3–14. https://doi.org/10.1007/s00170-019-04347-0

    Article  Google Scholar 

  35. Kang N, Coddet P, Liao H, Baur T, Coddet C (2016) Wear behavior and microstructure of hypereutectic Al-Si alloys prepared by selective laser melting. Appl Surf Sci 378:142–149. https://doi.org/10.1016/j.apsusc.2016.03.221

    Article  Google Scholar 

  36. Maire E, Withers PJ (2014) Quantitative X-ray tomography. Int Mater Rev 59:1–43. https://doi.org/10.1179/1743280413Y.0000000023

    Article  Google Scholar 

  37. Spierings AB, Schneider M, Eggenberger R (2011) Comparison of density measurement techniques for additive manufactured metallic parts. Rapid Prototyp J 17:380–386. https://doi.org/10.1108/13552541111156504

    Article  Google Scholar 

  38. Thijs L, Kempen K, Kruth J, Van Humbeeck J (2013) Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder. Acta Mater 61:1809–1819. https://doi.org/10.1016/j.actamat.2012.11.052

    Article  Google Scholar 

  39. Asgari H, Baxter C, Hosseinkhani K, Mohammadi M (2017) On microstructure and mechanical properties of additively manufactured AlSi10Mg_200C using recycled powder. Mater Sci Eng A 707:148–158. https://doi.org/10.1016/j.msea.2017.09.041

    Article  Google Scholar 

  40. Sanaei N, Fatemi A, Phan N (2019) Defect characteristics and analysis of their variability in metal L-PBF additive manufacturing. Mater Des 182:108091. https://doi.org/10.1016/j.matdes.2019.108091

    Article  Google Scholar 

  41. Zhang M, Sun C, Zhang X, Goh PC, Wei J, Hardacre D, Li H (2017) Fatigue and fracture behaviour of laser powder bed fusion stainless steel 316L: Influence of processing parameters. Mater Sci Eng A 703:251–261. https://doi.org/10.1016/j.msea.2017.07.071

    Article  Google Scholar 

  42. Krner C, Attar E, Heinl P (2011) Mesoscopic simulation of selective beam melting processes. J Mater Process Technol 211:978–987. https://doi.org/10.1016/j.jmatprotec.2010.12.016

    Article  Google Scholar 

  43. Brandl E, Heckenberger U, Holzinger V, Buchbinder D (2012) Additive manufactured AlSi10Mg samples using Selective Laser Melting (SLM): microstructure, high cycle fatigue, and fracture behavior. Mater Des 34:159–169. https://doi.org/10.1016/j.matdes.2011.07.067

    Article  Google Scholar 

  44. Hansen BL, Carpenter JS, Sintay SD, Bronkhorst CA, Mccabe RJ, Mayeur JR, Mourad HM, Beyerlein IJ, Mara NA, Chen SR (2013) Modeling the texture evolution of Cu/Nb layered composites during rolling. Int J Plast 49:71–84. https://doi.org/10.1016/j.ijplas.2013.03.001

    Article  Google Scholar 

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Acknowledgements

The authors would like to acknowledge the support of University Research Program of Ford Motor Company and The National Natural Science Foundation of China [grant number 52090042].

Funding

This work is supported by University Research Program of Ford Motor Company and The National Natural Science Foundation of China [grant number 52090042].

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All authors contributed to the study conception and design. Material preparation, data collection, and analysis were performed by Zhenxuan Luo, Weiqin Tang, and Dayong Li; the manuscript was written by Zhenxuan Luo; others helped perform the analysis with constructive discussions.

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Correspondence to Weiqin Tang.

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Luo, Z., Tang, W., Li, D. et al. Influence of laser process on the porosity-related defects, microstructure and mechanical properties for selective laser melted AlSi10Mg alloy. Int J Adv Manuf Technol 124, 281–296 (2023). https://doi.org/10.1007/s00170-022-10523-6

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