Abstract
The influences of selective laser melting (SLM) processing and post-processing on microstructure, crystallographic texture and defect characteristic, as well as the tensile property and anisotropy of SLM-produced Ti6Al4V alloys, were extensively studied. The results showed that the microstructure and the defects including micropore, keyhole and lack of fusion (LOF) can be controlled through the optimization of SLM processing and post-processing procedures. Mechanical tests demonstrated that the tensile properties were dependent mostly on the features of α phase/colony which could result in two types of fracture modes. The laminar heat-affected zone (HAZ) and LOF caused by SLM processing should be responsible for the anisotropy in strength and ductility, respectively. However, the presence of columnar grain structure, inherited weak texture, micropore and keyhole has limited effect on the tensile behaviors. The anisotropy can be alleviated through coarsening α phase, forming α colony and controlling defects such as the laminar HAZ and LOF with various process parameters and heat treatment procedures.
Similar content being viewed by others
References
A. Busachi, J. Erkoyuncu, P. Colegrove, F. Martina, C. Watts, and R. Drake, A Review of Additive Manufacturing Technology and Cost Estimation Techniques for the Defence Sector, CIRP J. Manuf. Sci. Technol., 2017, 19, p 117–128.
B. Baufeld, O. Van der Biest and R. Gault, Additive Manufacturing of Ti-6Al-4V Components by Shaped Metal Deposition: Microstructure and Mechanical Properties, Mat. Des., 2010, 31, p S106–S111.
A. Riemer, S. Leuders, M. Thöne, H.A. Richard, T. Tröster, and T. Niendorf, On the Fatigue Crack Growth Behavior in 316L Stainless Steel Manufactured by Selective Laser Melting, Eng. Fract. Mech., 2014, 120, p 15–25.
K. Rajaguru, T. Karthikeyan, and V. Vijayan, Additive Manufacturing - State of Art, Mater. Today Proc., 2019, 21, p 628–633. (In press)
J.P. Kruth, G. Levy, F. Klocke, and T.H.C. Childs, Consolidation Phenomena in Laser and Powder-Bed Based Layered Manufacturing, CIRP Ann. - Manuf. Technol., 2007, 56, p 730–759.
S. Bodziak, K.S. Al-Rubaie, L.V.O.D. Valentina, F.H. Lafratta, E.C. Santos, and A.M. Zanatta, Precipitation in 300 Grade Maraging Steel Built by Selective Laser Melting: Aging at 510 °C for 2 h, Mater. Charact., 2019, 151, p 73–83.
H. Shipley, D. McDonnell, M. Culleton, R. Coull, R. Lupoi, G. O’Donnell, and D. Trimble, Optimisation of Process Parameters to Address Fundamental Challenges during SELECTIVE Laser Melting of Ti-6Al-4V: A Review, Int. J. Mach. Tools Manuf., 2018, 128, p 1–20.
C.N. Chi, M. Savalani, and H.C. Man, Fabrication of Magnesium Using Selective Laser Melting Technique, Rapid Prototyp. J., 2011, 17, p 479–490.
J.F. Sun, Y.Q. Yang, and D. Wang, Mechanical Properties of Ti6Al4V Octahedral Porous Material Unit Formed by Selective Laser Melting, Adv. Mech. Eng., 2012, 4, p 742–760.
Z.Y. Xie, Y. Dai, X.Q. Ou, S. Ni, and M. Song, Effects of Selective Laser Melting Build Orientations on the Microstructure and Tensile Performance of Ti-6Al-4V Alloy, Mater. Sci. Eng. A., 2020, 776, p 139001.
A. Khorasani, I. Gibson, M. Goldberg, and G. Littlefair, Production of Ti-6Al-4V Acetabular Shell using Selective Laser Melting: Possible Limitations in Fabrication, Rapid. Prototyp. J., 2017, 23, p 110–121.
E.O. Olakanmi, R.F. Cochrane, and K.W. Dalgarno, A Review on selective Laser Sintering/Melting (SLS/SLM) of Aluminium Alloy Powders: Processing, Microstructure, and Properties, Prog. Mater. Sci., 2015, 74, p 401–477.
M. Peters, J. Kumpfert, C.H. Ward, and C. Leyens, Titanium Alloys for Aerospace Applications, Adv. Eng. Mater., 2003, 5, p 419–427.
K.S. Al-Rubaie, S. Melotti, A. Rabelo, and J.M. Paiva, Machinability of SLM-Produced Ti6Al4V Titanium Alloy Parts, J. Manuf. Processes., 2020, 57, p 768–786.
P. Ponnusamy, B. Sharma, S.H. Masood, R.A. Rahman Rashid, R. Rashid, S. Palanisamy, and D. Ruan, A Study of Tensile Behavior of SLM Processed 17–4 PH Stainless Steel, Mater. Today Proc., 2021, 45, p 4531–4534.
R. Mertens, B. Vrancken, N. Holmstock, Y. Kinds, J.P. Kruth, and J. Van Humbeeck, Influence of Powder Bed Preheating on Microstructure and Mechanical Properties of H13 Tool Steel SLM Parts, Phys. Proc., 2016, 83, p 882–890.
K. Kempen, B. Vrancken, S. Buls, L. Thijs, J. Van Humbeeck, and J.P. Kruth, Selective Laser Melting of Crack-Free High Density M2 High Speed Steel Parts by Baseplate Preheating, J. Manuf. Sci. Eng., 2014, 136, p 061026–061036.
X. Tang, S. Zhang, C.H. Zhang, J. Chen, J.B. Zhang, and Y. Liu, Optimization of Laser Energy Density and Scanning Strategy on the Forming Quality of 24CrNiMo Low Alloy Steel Manufactured by SLM, Mater. Charact., 2020, 170, p 110718.
M. Ghayoor, K. Lee, Y.J. He, C.H. Chang, B.K. Paul, and S. Pasebani, Selective Laser Melting of 304L Stainless Steel: Role of Volumetric Energy Density on the Microstructure, Texture and Mechanical Properties, Addit. Manuf., 2020, 32, p 101011.
K.S. Al-Rubaie, S. Melotti, A. Rabelo, J.M. Paiva, M.A. Elbestawi, and S.C. Veldhuis, Machinability of SLM-Produced Ti6Al4V Titanium Alloy Parts, J. Manuf. Processes., 2020, 57, p 768–786.
J. Han, J. Yang, H. Yu, J. Yin, M. Gao, Z. Wang, and X. Zeng, Microstructure and Mechanical Property of Selective Laser Melted Ti6Al4V Dependence on Laser Energy Density, Rapid Prototyp. J., 2017, 23, p 1–21.
M. Tang, P.C. Pistorius, and J.L. Beuth, Prediction of Lack-of-Fusion Porosity for Powder Bed Fusion, Addit. Manuf., 2017, 14, p 39–48.
T. Vilaro, C. Colin, and J.D. Bartout, As-Fabricated and Heat-Treated Microstructures of the Ti-6Al-4V Alloy Processed by Selective Laser Melting, Metall. Mater. Trans. A., 2011, 42, p 3190–3199.
D. Greitemeier, F. Palm, F. Syassen, and T. Melz, Fatigue Performance of Additive Manufactured TiAl6V4 Using Electron and Laser Beam Melting, Int. J. Fatigue., 2017, 94, p 211–217.
S. Palanivel, A.K. Dutt, E.J. Faierson, and R.S. Mishra, Spatially Dependent Properties in a Laser Additive Manufactured Ti-6Al-4V Component, Mater. Sci. Eng. A., 2016, 654, p 39–52.
M. Simonelli, Y.Y. Tse, and C. Tuck, Effect of the Build Orientation on the Mechanical Properties and Fracture Modes of SLM Ti-6Al-4V, Mater. Sci. Eng. A., 2014, 616, p 1–11.
A.M. Khorasani, I. Gibson, A. Ghaderi, and M.I. Mohammed, Investigation on the Effect of Heat Treatment and Process Parameters on the Tensile Behaviour of SLM Ti-6Al-4V Parts, Int. J. Adv. Manuf. Technol., 2019, 101, p 3183–3197.
C. Qiu, N.J.E. Adkins, and M.M. Attallah, Microstructure and Tensile Properties of Selectively Laser-Melted and of HIPed Laser-Melted Ti-6Al-4V, Mater. Sci. Eng. A., 2013, 578, p 230–239.
T. Etter, K. Kunze, F. Geiger, and H. Meidani, Reduction in Mechanical Anisotropy Through High Temperature Heat Treatment of Hastelloy X Processed by Selective Laser Melting (SLM), IOP Conf. Ser. Mater. Sci. Eng., 2015, 82, p 1–4.
J. Mezzetta, J.P. Choi, J. Milligan, J. Danovitch, N. Chekir, A. Bois-Brochu, Y.F. Zhao, and M. Brochu, Microstructure-Properties Relationships of Ti-6Al-4V Parts Fabricated by Selective Laser Melting, Int. J. Precis. Eng. Manuf. Green Technol., 2018, 5, p 605–612.
G.E. Bean, T.D. McLouth, D.B. Witkin, S.D. Sitzman, P.M. Adams, and R.J. Zaldivar, Build Orientation Effects on Texture and Mechanical Properties of Selective Laser Melting Inconel 718, J. Mater. Eng. Perform., 2019, 28, p 1942–1949.
M. Simonelli, Y.Y. Tse, and C. Tuck, On the Texture Formation of Selective Laser Melted Ti-6Al-4V, Metall. Mater. Trans. A., 2014, 45, p 2863–2872.
M.R. Daymond, R.A. Holt, S. Cai, P. Mosbrucker, and S.C. Vogel, Texture Inheritance and Variant Selection Through an hcp-bcc-hcp Phase Transformation, Acta Mater., 2010, 58, p 4053–4066.
B.B. He, W.H. Wu, L. Zhang, L. Lu, Q.Y. Yang, Q.L. Long, and K. Chang, Microstructural Characteristic and Mechanical Property of Ti6Al4V Alloy Fabricated by Selective Laser Melting, Vacuum, 2018, 150, p 79–83.
P. Krakhmalev, G. Fredriksson, I. Yadroitsava, N. Kazantseva, A.D. Plessis, and I. Yadroitsev, Deformation Behavior and Microstructure of Ti6Al4V Manufactured by SLM, Phys. Proc., 2016, 83, p 778–788.
B. Vrancken, L. Thijs, J.P. Kruth, and J.V. Humbeeck, Heat treatment of Ti6Al4V produced by Selective Laser Melting: Microstructure and mechanical properties, J. Alloys Compd., 2012, 541, p 177–185.
Y. Yang, Y.J. Liu, J. Chen, H.L. Wang, Z.Q. Zhang, Y.J. Lu, S.Q. Wu, and J.X. Lina, Crystallographic Features of α Variants and β Phase for Ti-6Al-4V Alloy Fabricated by Selective Laser Melting, Mater. Sci. Eng. A., 2017, 707, p 548–558.
L.E. Murr, S.A. Quinones, S.M. Gaytan, M.I. Lopez, A. Rodela, E.Y. Martinez, D.H. Hernandez, E. Martinez, F. Medina, and R.B. Wicker, Microstructure and Mechanical Behavior of Ti-6Al-4V Produced by Rapid-Layer Manufacturing for Biomedical Applications, J. Mech. Behav. Biomed. Mater., 2009, 2, p 20–32.
H. Attar, M. Calin, L. Zhang, S. Scudino, and J. Eckert, Manufacture by Selective Laser Melting and Mechanical Behavior of Commercially Pure Titanium, Mater. Sci. Eng. A., 2014, 593, p 170–177.
B.V. Hooreweder, D. Moens, R. Boonen, J.P. Kruth, and P. Sas, Analysis of Fracture Toughness and Crack Propagation of Ti6Al4V Produced by Selective Laser Melting, Adv. Eng. Mater., 2012, 14, p 92–97.
S.C. Wang, M. Aindow, and M.J. Starink, Effect of Self-accommodation on α/α Boundary Populations in Pure Titanium, Acta Mater., 2003, 51, p 2485–2503.
B. Zhou, J. Zhou, H. Li, and F. Lin, A study of the Microstructures and Mechanical Properties of Ti6Al4V Fabricated by SLM Under Vacuum, Mater. Sci. Eng. A., 2018, 724, p 1–10.
K.F. Walker, Q. Liu, and M. Brandt, Evaluation of Fatigue Crack Propagation Behavior in Ti-6Al-4V Manufactured by Selective Laser Melting, Int. J. Fatigue., 2017, 104, p 302–308.
C. Zhao, N.D. Parab, X.X. Li, K. Fezzaa, W.D. Tan, A.D. Rollett, and T. Sun, Critical Instability at Moving Keyhole Tip Generates Porosity in Laser Melting, Science, 2020, 370, p 1080–1086.
D.D. Gu, W. Meiners, K. Wissenbach, and R. Poprawe, Laser Additive Manufacturing of Metallic Components: Materials, Processes and Mechanisms, Int. Mater. Rev., 2012, 57, p 133–164.
S.A. Khairallah, A.T. Anderson, A. Rubenchik, and W.E. King, Laser Powder-Bed Fusion Additive Manufacturing: Physics of Complex Melt Flow and Forming Mechanisms of Pores, Spatter, and Denudation Zones, Acta Mater., 2016, 108, p 36–45.
I. Maskery, N.T. Aboulkhair, M.R. Corfield, C. Tuck, A.T. Clare, R.K. Leach, R.D. Wildman, I.A. Ashcroft, and R.J.M. Hague, Quantification and Characterisation of Porosity in Selectively Laser Melted Al-Si10-Mg Using X-ray Computed Tomography, Mater. Charact., 2016, 111, p 193–204.
S. Bo, S. Dong, B. Zhang, H. Liao, and C. Coddet, Effects of Processing Parameters on Microstructure and Mechanical Property of Selective Laser Melted Ti6Al4V, Mater. Des., 2012, 35, p 120–125.
D. Banerjee and J. Williams, Perspectives on Titanium Science and Technology, Acta Mater., 2013, 61, p 844–879.
G. Lütjering, Property Optimization Through Microstructural Control in Titanium and Aluminum Alloys, Mater. Sci. Eng. A, 1999, 243, p 117–126.
E. Chlebus, B. Kuźnicka, T. Kurzynowski, and B. Dybała, Microstructure and Mechanical Behaviour of Ti-6Al-7Nb Alloy Produced by Selective Laser Melting, Mater. Charact., 2011, 62, p 488–495.
T. Sercombe, N. Jones, R. Day, and A. Kop, Heat Treatment of Ti-6Al-7Nb Components Produced by Selective Laser Melting, Rapid Prototyp. J., 2008, 14, p 300–304.
Acknowledgment
The authors wish to thank for the contributions of BLT Company China and HFYC (Zhenjiang) Additive Manufacturing Co., Ltd (AEAM) in manufacturing of designated alloys and providing heat treatment services.
Funding
This work is supported by the financial support from AECC Science and Technology Innovation Platform Program (CXPT-2018-42) and National Natural Science Foundation of China (Grant No. 51875541).
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
Conflict of interest
The authors declare that they have no financial and personal relationships with other people or organizations that can inappropriately influence our work, and there is no professional or other personal interest of any nature or kind in any product, service and/or company that could be construed as influencing the position presented in, or the review of, the manuscript entitled.
Consent for Publication
Written informed consent for publication was obtained from all participants.
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Gao, X., Tao, C., Wu, S. et al. Influence of Modified Microstructures and Characterized Defects on Tensile Properties and Anisotropy of Selective Laser Melting-Produced Ti6Al4V Alloys. J. of Materi Eng and Perform 31, 7705–7718 (2022). https://doi.org/10.1007/s11665-022-06745-0
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-022-06745-0