Abstract
A method of ceramic-ceramic joining that exploits a thin layer of a transient liquid phase to join alumina to alumina has been developed, and the results of its application to joining alumina are reported. Through the use of microdesigned multilayer Cu/Pt interlayers, transient liquid-phase joining has been achieved at 1150°C, yielding an interlayer that is platinum-rich at temperatures substantially lower than those required for solid-state diffusion bonding with pure platinum interlayers. Flexure tests indicate that ceramic/metal interface strengths exceeding those of the ceramic can be achieved. Post-bonding anneals of 10 h duration in air and gettered argon at 1000 °C had discernibly different effects on room-temperature joint strength. The microstructure and chemistry of fracture surfaces were examined using SEM and EDS in an effort to identify the nature of strength-limiting flaws in both as-bonded and postbonding annealed specimens. Topics requiring further study are identified. Opportunities for extensions of the method to other systems are discussed.
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Shalz, M.L., Dalgleish, B.J., Tomsia, A.P. et al. Ceramic joining. Journal of Materials Science 28, 1673–1684 (1993). https://doi.org/10.1007/BF00363367
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DOI: https://doi.org/10.1007/BF00363367