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Pilot scale test of producing nickel concentrate from low-grade saprolitic laterite by direct reduction-magnetic separation

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Abstract

The enrichment of Ni from a low-grade saprolitic laterite ore, which has been pre-treated by high pressure grinding roller(HPGR) to be 74% passing 0.074 mm and contains 0.92% Ni, 18.47% Fe, 10.61% MgO and 42.27% SiO2, was conducted by using pelletizing, rotary kiln reduction and magnetic separation process on a semi industrial scale, and the effects of reduction duration, mass ratio of coal to pellets(C/P), the types of magnetic separator, the sections of grinding-separation and the grinding fineness on the recovery of Ni and Fe were examined. It is shown that nickel concentrate containing 3.13 % Ni and 59.20 % Fe was achieved at recoveries of 84.36 % and 71.51 % for Ni and Fe, respectively under the following conditions: reducing at (1120±40) °C for 120 min, C/P being 1.0, wet grinding of reduced pellets up to 70%–87% passing 0.074 mm and a magnetic field intensity of 238.8 kA/m during the first section of grinding-magnetic separation, and a grinding fineness of 84%–91% passing 0.045 mm and a magnetic intensity of 39.8 kA/m during the second section of grinding-magnetic separation. The enriched Ni containing concentrate has a low content of S and P, and can be used for further processing to produce high-grade ferronickel alloy.

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References

  1. KUCK P H. Nickel [R]. Reston: U.S. Geological Survey, 2012.

    Google Scholar 

  2. GU Yi, XIA Chang-qing, LI Jia, WU An-ru. Effect of nano-size nickel particles on wear resistance and high temperature oxidation resistance of ultrafine ceramic coating [J]. J Cent South Univ Technol, 2004, 11(4): 358–361.

    Article  Google Scholar 

  3. WARNER A E M., DIAZ C M, DALVI A D, MACKEY P J, TARASOV A V. JOM world nonferrous smelter survey, Part III: nickel: Laterite [J]. JOM, 2006, 4: 11–20.

    Article  Google Scholar 

  4. KÖSE C H, TOPKAYA Y A. Hydrometallurgical processing of nontronite type lateritic nickel ores by MHP process [J]. Minerals Engineering, 2011, 24: 396–415.

    Article  Google Scholar 

  5. MCDONALD R G, WHITTINGTON B I. Atmospheric acid leaching of nickel laterites review: Part I. Sulphuric acid technologies [J]. Hydrometallurgy, 2008, 91(1/2/3/4): 35–55.

    Article  Google Scholar 

  6. CONNOR F O’, CHEUNG W H, VALIX M. Reduction roasting of limonite ores: Effect of dehydroxylation [J]. Int J Miner Process, 2006, 80: 88–99.

    Article  Google Scholar 

  7. ISHII K. Development of ferro-nickel smelting from laterite in Japan [J]. Int J Miner Process, 1987, 19: 15–24.

    Article  Google Scholar 

  8. KOTZE I J. Pilot plant production of ferroniekel from niekel oxide ores and dusts in a DC arc furnace [J]. Miner Eng, 2002, 15: 1017–1022.

    Article  Google Scholar 

  9. NORGATE T, JAHANSHAHI S. Assessing the energy and greenhouse gas footprints of nickel laterite processing [J]. Miner Eng, 2011 24(7): 698–707.

    Article  Google Scholar 

  10. FU Fang-ming, HU Qi-yang, LI Xin-hai, WANG Zhi-xing, LI Jin-hui, LI Ling-jun. Thermodynamics and chloridizing roasting conditions of laterite through ammonium chloride [J]. Journal of Central South University (Science and Technology), 2010, 41(6): 2096–2102. (in Chinese)

    Google Scholar 

  11. LI Qi-hou, CUI Yu, ZHU De-qing, ZHU Jing-he, PAN Jian, ZHANG Hong-liang, ZHENG Guo-lin. Study on selective reduction of low-grade nickel laterite ore to produce high nickel concentrate [C]// Robin Batterham. XXV International Mineral Processing Congress Proceedings. Brisbane: AUSIMM, 2010: 1549–1556.

    Google Scholar 

  12. LI Guang-hui, RAO Ming-jun, JIANG Tao, HUANG Qing-qing, SHI Tang-min, ZHANG Yuan-bo. Innovative process for preparing ferronickel materials from laterite ore by reduction roasting-magnetic separation [J]. Trans Nonferrous Met Soc China, 2011, 21(12): 3137–3142. (in Chinese)

    Google Scholar 

  13. ZHU De-qing, ZHENG Guo-lin, PAN Jian, LI Qi-hou, An Yue-ming, WANG Lin. Direct reduction-magnetic separation of low-grade saprolitic laterite to produce nickel concentrate [C]// PRADIP and MISHRA B K. XXVI International Mineral Processing Congress 2012 Proceedings. New Delhi: New Concept Information Systems Pvt. Ltd, 2012: 6242–6249.

    Google Scholar 

  14. ZHU De-qing, PAN Jian, LI Qi-hou, ZHENG Guo-lin, LI Zi-yun. A process for producing high nickel concentrate from low-grade nickel laterite: China patent, CN 102242252 [P]. 2011. (in Chinese)

    Google Scholar 

  15. CHUN Tie-jun. Study on high-efficient enrichment technology and mechanism of low-grade and super-fine hematite [D]. Changsha: Central South University, 2010. (in Chinese)

    Google Scholar 

  16. ZHU De-qing, CUI Yu, VININ K, HAPUGODA S, DOUGLAS J, PAN J, ZHENG Guo-lin. Upgrading low nickel content laterite ores using selective reduction followed by magnetic separation [J]. Int J Miner Process, 2012, 106–109: 1–7.

    Google Scholar 

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Correspondence to De-qing Zhu  (朱德庆).

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Foundation item: Project(NDRC-Hitech Office 2009-606) supported by the National Development and Reform Commission of China; Project(50974135) supported by the National Natural Science Foundation of China

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Zheng, Gl., Zhu, Dq., Pan, J. et al. Pilot scale test of producing nickel concentrate from low-grade saprolitic laterite by direct reduction-magnetic separation. J. Cent. South Univ. 21, 1771–1777 (2014). https://doi.org/10.1007/s11771-014-2123-0

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  • DOI: https://doi.org/10.1007/s11771-014-2123-0

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