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Variation in Mechanical Properties and Heterogeneity in Microstructure of High-Strength Ferritic Steel During Mill Trial

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Abstract

HS600 and HS800 are two new generation, high-strength advanced ferritic steels that find widespread application in automobiles. During commercial production of the same grades with different thicknesses, it has been found that mechanical properties like tensile strength and stretchability varied widely and became inconsistent. In the current endeavor, two different thicknesses have been chosen from a mill trial sample of HS600 and HS800. An in-depth structural characterization was carried out for all four alloys to explain the variation in their respective mechanical and shear punch properties. The carbon content was smaller and Ti + Mo quantity was higher in case of HS800 with respect to HS600. The microstructure of both steels consisted of the dispersion of (Ti,Mo)C in a ferrite matrix. The grain size of HS800 was little larger than HS600 due to an increased coiling temperature (CT) of the former in comparison to the latter. It was found that in case of same grade of steel with a different thickness, a variation in microstructure occurred due to change in strain, CT, and cooling rate. The strength and stretch formability of these two alloys were predominantly governed by a microalloyed carbide. In this respect, carbides with a size range above 5 nm were responsible for loosing coherency with ferrite matrix. In case of HS600, both ≤5 and >5-nm size (Ti,Mo)C precipitates shared a nearly equal fraction of microalloyed precipitates. However, for HS800, >5-nm size (Ti,Mo)C carbide was substantially higher than ≤5-nm size alloy carbides. The ultimate tensile strength and yield strength of HS800 was superior to that of HS600 owing to a higher quantity of microalloyed carbide with a decreased column width and interparticle distance. A higher degree of in-coherency of HS800 made the alloy prone to crack formation with low stretchability.

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Notes

  1. Qualitative and quantitative microstructural analysis consisting of grain size, phase fraction, aspect ratio and other geometrical quantities.

References

  1. H.W. Yen, C.Y. Chen, C.Y. Huang, and J.R. Yang: The 3 rd Int. Conf. on Adv. Struct. Steels, Gyeongju, Korea, 2006, pp. 400–405.

  2. W.B. Lee, S.G. Hong, C.G. Park, and S.H. Park: Metall. Mater. Trans. A, 2002, vol. 33A, pp. 1689–98.

    Article  Google Scholar 

  3. T. Gladman: The Physical Metallurgy of Microalloyed Steels, The Institute of Materials, Maney Publishing, London, June 1997, pp. 54–81.

  4. Y. Funakawa, T. Shiozaki, K. Tomita, T. Yamamoto, and E. Maeda: ISIJ Int., 2004, vol. 44, pp. 1945–51.

    Article  Google Scholar 

  5. H.J. Kestenbach: Mater. Sci. Technol., 1997, vol.13, pp. 731–39.

    Article  Google Scholar 

  6. K. Seto, Y. Funakawa, and S. Kaneko: JFE Tech. Rep., 2007, no. 10, pp. 19–25

  7. C.Y. Chen, H.W. Yen, F.H. Kao, W.C. Li, C.Y. Huang, J.R. Yang, and S.H. Wang: Mater. Sci. Eng. A, 2009, vol. 499, pp. 162–66.

    Article  Google Scholar 

  8. J. Calvo, I.H. Jung, A.M. Elwazri, D. Bai, and S. Yue: Mater. Sci. Eng. A, 2009, vol. 520, pp. 90–96.

    Article  Google Scholar 

  9. X. Mao, X. Huo, X. Sun, and Y. Chai: J. Mater. Proc. Technol., 2010, vol. 210, pp. 1660–66.

    Article  Google Scholar 

  10. H.W. Yen, P.Y. Chen, C.Y. Huang, and J.R. Yang: Acta Mater., 2011, vol. 59, pp. 6264–74.

    Article  Google Scholar 

  11. J.-G. Cao, J. Zhang, N. Kong, and K.-F. Mi: Finite Element Analysis, ed. David Moratal, 2010, http://www.intechopen.com/books/finite-element-analysis/-finite-element-analysis-of-strip-and-rolling-mills.

  12. P.J. Hurley and P.D. Hodgson: Mater. Sci. Eng. A, 2001, vol. 302, pp. 206–14.

    Article  Google Scholar 

  13. G. Jha, S. Das, S. Sinha, A. Lodh, and A. Haldar: Mater. Sci. Eng. A, 2013, vol. 561, pp. 394–402.

    Article  Google Scholar 

  14. Y. Kim, K. Im, Y.M. Cheong, and S.B. Ahn: J. Nucl. Mater., 2005, vol. 346, pp. 120–30.

    Article  Google Scholar 

  15. S.S. Campos, E.V. Morales, and H.J. Kestenbach: Mater. Charact., 2004, vol. 52, pp. 379–84.

    Article  Google Scholar 

  16. G.E. Lucas, J.W. Sheckherd, G.R. Odett, and S. Panchanadeeswaran: J. Nucl. Mater., 1984, vol. 122, pp. 429–34.

    Article  Google Scholar 

  17. S. Acharya and K.K. Roy: Mater. Sci. Eng. A, 2013, vol. 565, pp. 405–13.

    Article  Google Scholar 

  18. I.B. Timokhina, P.D. Hodgson, S.P. Ringer, R.K. Zheng, and E.V. Pereloma: Scripta Mater., 2007, vol. 56, pp. 601–604.

    Article  Google Scholar 

  19. M.B. Toloczko, M.L. Hamilton, and G.E. Lucas: J. Nucl. Mater., 2000, vols. 283–287, pp. 987–91

    Article  Google Scholar 

  20. T. Shimidzu, Y. Funakawa, and S. Kaneko: JFE Technical Report No. 4, 2004, pp. 25–31.

  21. Y.F. Shen, C.M. Wang, and X. Sun: Mater. Sci. Eng. A, 2011, vol. A528, pp. 8150–56.

    Article  Google Scholar 

  22. C.Y. Chen and J.R. Yang: National Taiwan University, Taipei, Taiwan, unpublished research, 2007, p. 13.

  23. P.J. Hurley and P.D. Hodgson: Mater. Sci. Technol., 2001, vol. 17, pp. 1360–67.

    Article  Google Scholar 

  24. M.R. Hickson, P.J. Hurley, R.K. Gibbs, G.L. Kelly, and P.D. Hodgson: Metall. Mater. Trans. A, 2002, vol. 33A, pp. 1019–26.

    Article  Google Scholar 

  25. H. Xinlai, S. Chengjia, H. Huaxin, and G. Aimin: The Development of 600–800 MPa Grade High Strength Low Carbon Bainitic Steel, http://www.metal.citic.com/iwcm/UserFiles/img/cd/2005-HSLA-NB/HSLA-031.pdf.

  26. H.W. Yen, C.Y. Huang, and J.R. Yang: Scripta Mater., 2009, vol. 61, pp. 616–19.

    Article  Google Scholar 

  27. J.S. Park, Y.S. Ha, S.J. Lee, and Y.K. Lee: Metall. Mater. Trans. A, 2009, vol. 40A, pp. 560–68.

    Article  Google Scholar 

  28. S.G. Hong, K.B. Kang, and C.J. Park: Scripta Mater., 2002, vol. 46, pp. 163–68.

    Article  Google Scholar 

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Acknowledgments

The authors are indebted to Director, CSIR–NML, and Dr. T. Venugopalan_CTO-TSL for their kind interest during the study as well as for giving permission to publish the work. The authors are grateful to Tata Steel Limited, Jamshedpur, India, for providing raw materials and partial financial support to carry out the investigation.

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Correspondence to M. Ghosh.

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Manuscript submitted July 12, 2013.

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Ghosh, M., Barat, K., Das, S.K. et al. Variation in Mechanical Properties and Heterogeneity in Microstructure of High-Strength Ferritic Steel During Mill Trial. Metall Mater Trans A 45, 2719–2731 (2014). https://doi.org/10.1007/s11661-014-2226-0

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