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Evolution of volatile compounds, aroma attributes, and sensory perception in bottle-aged red wines and their correlation

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Abstract

This study aimed to investigate the evolution of volatile compounds, odor activity value-based aroma notes, and sensory perception in Cabernet Sauvignon (Vitis vinifera L. cv.) dry red wines during an 18-month bottle-aging period, and further to assess the correlation between them. The wines were sealed with six types of stoppers, including natural cork, agglomerated cork, technical cork, and three types of polymer synthetic plugs, to provide different oxygen environments during wine development. Results showed that volatile compounds in all of the wine samples exhibited three evolution trends during the bottle-aging process. Most of the volatiles followed the second evolution trend in which their concentration increased within the first 3–9 months of bottle aging, and subsequently declined. The wines bottle-aged within 9 months possessed obvious aroma characteristics, which resulted from the abundant volatile compounds in this period, in particular, the presence of esters and alcohols. The 15-month bottle-aged wines showed the highest sensory quality evolution, suggesting that this might be related to a good balance of various aroma attributes. Partial least squares regression analysis revealed that wine aroma could develop toward good perception with the increase in ethyl octanoate, 1-octen-3-ol, and ethyl dodecanoate. However, the increase in (Z)-3-hexen-1-ol, 2-methoxy-phenol, decanal, isobutyric acid, octanoic acid, and isoamyl acetate resulted in a negative sensory feature of wine aroma.

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References

  1. Godden P, Lattey K, Francis L, Gishen M, Cowey G, Holdstock M, Robishon E, Waters E, Skouroumounis G, Sefton M, Capone D, Kwiatkowski M, Field J, Coulter A, D’Costa N, Bramley B (2005) Towards offering wine to the consumer in optimal condition-the wine, the closures and other packaging variables: a review of AWRI research examining the changes that occur in wine after bottling Wine. Aust NZ Wine Ind J 20:20–30

    Google Scholar 

  2. Silva MA, Julien M, Jourdes M, Teissedre PL (2011) Impact of closures on wine post-bottling development: a review. Eur Food Res Technol 233(6):905–914

    Article  CAS  Google Scholar 

  3. Ugliano M (2013) Oxygen contribution to wine aroma evolution during bottle aging. J Agric Food Chem 61:6125–6136

    Article  CAS  Google Scholar 

  4. Ugliano M, Kwiatkowski MJ, Travis B, Francis IL, Waters EJ, Herderich MJ, Pretorius IS (2009) Post-bottling management of oxygen to reduce off-flavour formation and optimize wine style. Aust NZ Wine Ind J 24(5):24–28

    Google Scholar 

  5. Lopes P, Silva MA, Pons A (2009) Impact of oxygen dissolved at bottling and transmitted through closures on the composition and sensory properties of a Sauvignon blanc wine during bottle storage. J Agric Food Chem 57(21):10261–10270

    Article  CAS  Google Scholar 

  6. Caillé S, Samson A, Wirth J, Diéval JB, Vidal S, Cheynier V (2010) Sensory characteristics changes of red Grenache wines submitted to different oxygen exposures pre and post bottling. Anal Chim Acta 660(1–2):35–42

    Article  Google Scholar 

  7. Wirth J, Morel-Salmi C, Souquet JM, Dieval JB, Aagaard O, Vidal S, Flucranda H, Cheynier V (2010) The impact of oxygen exposure before and after bottling on the polyphenolic composition of red wines. Food Chem 123(1):107–116

    Article  CAS  Google Scholar 

  8. Ugliano M, Kwiatkowski M, Vidal S, Capone D, Siebert T, Dieval JB, Aagaard O, Waters EJ (2011) Evolution of 3-mercaptohexanol, hydrogen sulfide, and methyl mercaptan during bottle storage of Sauvignon blanc wines. Effect of glutathione, copper, oxygen exposure, and closure-derived oxygen. J Agric Food Chem 59(6):2564–2572

    Article  CAS  Google Scholar 

  9. Ugliano M, Dieval JB, Siebert TE, Kwiatkowski M, Aagaard O, Vidal S, Waters EJ (2012) Oxygen consumption and development of volatile sulfur compounds during bottle aging of two Shiraz wines. Influence of pre-and post bottling controlled oxygen exposure. J Agric Food Chem 60(35):8561–8570

    Article  CAS  Google Scholar 

  10. Wildenradt HL, Singleton VL (1974) The production of aldehydes as a result of oxidation of polyphenolic compounds and its relation to wine aging. Am J Enol Viticult 25(2):119–126

    CAS  Google Scholar 

  11. Saucier C, Guerra C, Pianet I, Laguerre M, Glories Y (1997) +-Catechin-acetaldehyde condensation products in relation to wine-ageing. Phytochemistry 46(2):229–234

    Article  CAS  Google Scholar 

  12. Escribano-Bailón T, Álvarez-García M, Rivas-Gonzalo JC, Heredia FJ, Santos-Buelga C (2001) Color and stability of pigments derived from the acetaldehyde-mediated condensation between malvidin 3-O-glucoside and +-catechin. J Agric Food Chem 49(3):1213–1217

    Article  Google Scholar 

  13. Mateus N, Carvalho E, Carvalho AR, Melo A, González-Paramás AM, Santos-Buelga C, Silva AMS, de Freitas V (2003) Isolation and structural characterization of new acylated anthocyanin–vinyl–flavanol pigments occurring in aging red wines. J Agric Food Chem 51(1):277–282

    Article  CAS  Google Scholar 

  14. Godden P, Francis L, Field J, Gishen M, Coulter A, Valente P, Høj P, Robinson E (2001) Wine bottle closures: physical characteristics and effect on composition and sensory properties of a Semillon wine 1. Performance up to 20 months post-bottling. Aust J Grape Wine Res 7(2):64–105

    Article  CAS  Google Scholar 

  15. Skouroumounis GK, Kwiatkowski MJ, Francis IL, Oakey H, Capone DL, Duncan B, Sefton MA, Waters EJ (2005) The impact of closure type and storage conditions on the composition, colour and flavour properties of a Riesling and a wooded Chardonnay wine during five years’ storage. Aust J Grape Wine Res 11(3):369–377

    Article  CAS  Google Scholar 

  16. Kwiatkowski MJ, Skouroumounis GK, Lattey KA, Waters EJ (2007) The impact of closures, including screw cap with three different headspace volumes, on the composition, colour and sensory properties of a Cabernet Sauvignon wine during two years’ storage. Aust J Grape Wine Res 13(2):81–94

    Article  CAS  Google Scholar 

  17. Escudero A, Asensio E, Cacho J, Ferreira V (2002) Sensory and chemical changes of young white wines stored under oxygen. An assessment of the role played by aldehydes and some other important odorants. Food Chem 77(3):325–331

    Article  CAS  Google Scholar 

  18. Lopes P, Saucier C, Teissedre PL, Glories Y (2006) Impact of storage position on oxygen ingress through different closures into wine bottles. J Agric Food Chem 54(18):6741–6746

    Article  CAS  Google Scholar 

  19. Lopes P, Saucier C, Teissedre PL, Glories Y (2007) Main routes of oxygen ingress through different closures into wine bottles. J Agric Food Chem 55(13):5167–5170

    Article  CAS  Google Scholar 

  20. Silva A, Lambri M, Faveri MDD (2003) Evaluation of the performances of synthetic and cork stoppers up to 24 months post-bottling. Eur Food Res Technol 216(6):529–534

    CAS  Google Scholar 

  21. Marin AB, Jorgensen EM, Kennedy JA, Ferrier J (2007) Effects of bottle closure type on consumer perceptions of wine quality. Am J Enol Viticult 58(2):182–191

    Google Scholar 

  22. Gao Y, Tian Y, Liu D, Li Z, Zhan XX, Li JM, Huang JH, Wang J, Pan QH (2015) Evolution of phenolic compounds and sensory in bottled red wines and their co-development. Food Chem 172:565–574

    Article  CAS  Google Scholar 

  23. Cai J, Zhu BQ, Wang YH, Lu L, Lan YB, Reeves MJ, Duan CQ (2014) Influence of pre-fermentation cold maceration treatment on aroma compounds of Cabernet Sauvignon wines fermented in different industrial scale fermenters. Food Chem 154:217–229

    Article  CAS  Google Scholar 

  24. Xia J, Sinelnikov IV, Han B, Wishart DS (2015) MetaboAnalyst 30—making metabolomics more meaningful. Nucleic Acids Res. doi:10.1093/nar/gkv380

    Google Scholar 

  25. Escudero A, Hernández-Orte P, Cacho J, Ferreira V (2000) Clues about the role of methional as character impact odorant of some oxidized wines. J Agric Food Chem 48(9):4268–4272

    Article  CAS  Google Scholar 

  26. Culleré L, Cacho J, Ferreira V (2007) An assessment of the role played by some oxidation-related aldehydes in wine aroma. J Agric Food Chem 55(3):876–881

    Article  Google Scholar 

  27. Fedrizzi B, Zapparoli G, Finato F, Tosi E, Turri A, Azzolini M, Versini G (2011) Model aging and oxidation effects on varietal, fermentative, and sulfur compounds in a dry botrytized red wine. J Agric Food Chem 59(5):1804–1813

    Article  CAS  Google Scholar 

  28. Ugliano M, Siebert T, Mercurio M, Capone D, Henschke PA (2008) Volatile and color composition of young and model-aged Shiraz wines as affected by di-ammonium phosphate supplementation before alcoholic fermentation. J Agric Food Chem 56:9175–9182

    Article  CAS  Google Scholar 

  29. Moio L, Ugliano M, Genovese A, Gambuti A, Pessina R, Piombino P (2004) Effect of antioxidant protection of must on volatile compounds and aroma shelf life of Falanghina Vitis vinifera L. wine. J Agric Food Chem 52:891–897

    Article  CAS  Google Scholar 

  30. Dimkou E, Ugliano M, Dieval JB, Vidal S, Aagaard O, Rauhut D, Jung R (2011) Impact of headspace oxygen and closure on sulfur dioxide, color, and hydrogen sulfide levels in a Riesling wine. Am J Enol Viticult 62(3):261–269

    Article  Google Scholar 

  31. Capone S, Tufariello M, Siciliano P (2013) Analytical characterisation of Negroamaro red wines by “Aroma Wheels”. Food Chem 141:2906–2915

    Article  CAS  Google Scholar 

  32. Sánchez-Palomo E, Alonso-Villegas R, Viñas MG (2015) Characterisation of free and glycosidically bound aroma compounds of La Mancha Verdejo white wines. Food Chem 173:1195–1202

    Article  Google Scholar 

  33. Ferreira V, López R, Cacho JF (2000) Quantitative determination of the odorants of young red wines from different grape varieties. J Sci Food Agric 80(11):1659–1667

    Article  CAS  Google Scholar 

  34. Gil M, Cabellos JM, Arroyo T, Prodanov M (2006) Characterization of the volatile fraction of young wines from the denomination of origin “Vinos de Madrid”Spain. Anal Chim Acta 563:145–153

    Article  CAS  Google Scholar 

  35. Gómez-Míguez MJ, Cacho JF, Ferreira V, Vicario IM, Heredia FJ (2007) Volatile components of Zalema white wines. Food Chem 100(4):1464–1473

    Article  Google Scholar 

  36. Romano P, Suzzi G, Domizio P, Fatichenti F (1997) Secondary products formation as a tool for discriminating non-Saccharomyces wine strains. Anton Leeuw Int J G 71(3):239–242

    Article  CAS  Google Scholar 

  37. Styger G, Prior B, Bauer FF (2011) Wine flavor and aroma. J Ind Microbiol Biotechnol 38(9):1145–1159

    Article  CAS  Google Scholar 

  38. Francis IL, Newton JL (2005) Determining wine aroma from compositional data Microbial modulation of wine aroma and flavour. Aust J Grape Wine Res 11(2):114–126

    Article  CAS  Google Scholar 

  39. Pineau B, Barbe JC, Van Leeuwen C, Dubourdieu D (2007) Which impact for β-damascenone on red wines aroma? J Agric Food Chem 55(10):4103–4108

    Article  CAS  Google Scholar 

  40. Robinson AL, Ebeler SE, Heymann H, Boss PK, Solomon PS, Trengove RD (2009) Interactions between wine volatile compounds and grape and wine matrix components influence aroma compound headspace partitioning. J Agric Food Chem 57(21):10313–10322

    Article  CAS  Google Scholar 

  41. Sáenz-Navajas MP, Campo E, Culleré L, Fernández-Zurbano P, Valentin D, Ferreira V (2010) Effects of the nonvolatile matrix on the aroma perception of wine. J Agric Food Chem 58(9):5574–5585

    Article  Google Scholar 

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Acknowledgments

This work was financially supported by the project of China Agriculture Research System (CARS-30).

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Correspondence to Qiu-Hong Pan.

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Liu, D., Xing, RR., Li, Z. et al. Evolution of volatile compounds, aroma attributes, and sensory perception in bottle-aged red wines and their correlation. Eur Food Res Technol 242, 1937–1948 (2016). https://doi.org/10.1007/s00217-016-2693-1

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