Abstract
Precipitation behavior of P550 steel for non-magnetic drill collars was investigated by microstructure characterization as well as thermodynamic calculation. The results demonstrate that the main precipitate formed at 650–900 °C was cellular Cr2N, and its precipitation depended heavily on the aging temperature. The most sensitive precipitation temperature of cellular Cr2N was 750 °C. At 750 °C, the cellular Cr2N exhibited fast-slow precipitation kinetics with the aging time prolonging. The initial precipitation of cellular Cr2N was governed by the short-range intergranular diffusion of Cr. During long-term aging, its growth was controlled by the long-range bulk diffusion of Cr. In addition, cellular Cr2N induced the precipitation of σ phase ahead of the cell after long period of aging. Increasing the nitrogen content resulted in the increment of both the nucleation site and the driving force for the cellular Cr2N, which jointly promoted its precipitation.
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Acknowledgements
This research was sponsored by the National Natural Science Foundation of China (Grant Nos. U1960203 and 51774074), Shanxi Municipal Major Science & Technology Project (Grant No. 20181101014), Fundamental Research Funds for the Central Universities (Grant Nos. N172512033 and N2024005-4), Talent Project of Revitalizing Liaoning (XLYC1902046) and State Key Laboratory of Metal Material for Marine Equipment and Application (Grant No. HG-SKL (2019) 13).
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Xu, Lw., Zheng, Hb., Li, Hb. et al. Precipitation behavior of P550 steel for non-magnetic drill collars during isothermal aging at 650–900 °C. J. Iron Steel Res. Int. 29, 636–646 (2022). https://doi.org/10.1007/s42243-021-00566-6
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DOI: https://doi.org/10.1007/s42243-021-00566-6