Skip to main content
Log in

Degradation and reduction of small punch creep life of service-exposed Super304H steel

  • Published:
Journal of Mechanical Science and Technology Aims and scope Submit manuscript

Abstract

To ensure the safety and structural integrity of a power boiler in thermal power plants, residual life management of superheater tubes at elevated temperature is needed. Over the decades, small punch (SP) creep testing has been widely used as an effective method for measuring creep life and creep properties of the boiler tube materials. In this study, a series of SP creep tests were performed at 650 °C with virgin and service-exposed Super304H stainless steels. The service period was 54750 h and 68550 h, respectively. The residual creep rupture life of the 68550 h serviced Super304H material decreased significantly when it was compared with the virgin and 54750 h serviced materials. Coarsening of the M23C6 precipitates along the grain boundaries made the adjacent region Cr-depleted, which could accelerate the formation of creep cavities at the grain boundaries. These microstructural degradations reduced the creep rupture life of the service-exposed materials. The Larson–Miller curve and the Monkman–Grant relationship were applied to predict the creep rupture life of service-exposed Super304H steels from the measured short creep rupture data.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

Abbreviations

Ā :

Small punch creep coefficient

:

Small punch creep exponent

B :

Monkman Grant constant

C :

Larson Miller constant

LMP :

Larson Miller parameter

P :

Small punch load

t r :

Time to rupture (in hours)

T :

Temperature (in Kelvin)

δ̇min :

Minimum punch-displacement rate

α :

Monkman-Grant exponent for small punch creep

References

  1. F. Masuyama, History of power plants and progress in heat resistant steels, ISIJ International, 41 (6) (2001) 612–615.

    Article  Google Scholar 

  2. M. K. Dash, T. Karthikeyan, R. Mythili, V. D. Vijayanand and S. Saroja, Effect of long-term thermal exposures on microstructure and impression creep in 304HCu grade austenitic stainless steel, Metallurgical and Materials Transactions A, 48 (10) (2017) 4883–4894.

    Article  Google Scholar 

  3. D. B. Park, S. M. Hong, K. H. Lee, M. Y. Huh, J. Y. Suh, S. C. Lee and W. S. Jung, High-temperature creep behavior and microstructural evolution of an 18Cr9Ni3CuNbVN austenitic stainless steel, Materials Characterization, 93 (2014) 52–61.

    Article  Google Scholar 

  4. X. Huang, Q. Zhou, W. Wang, W. S. Li and Y. Gao, Microstructure and property evolutions of a novel Super304H steel during high temperature creeping, Materials at High Temperatures, 35 (5) (2017) 438–450.

    Article  Google Scholar 

  5. S. Bagui, K. Laha, R. Mitra and S. Tarafder, Accelerated creep behavior of Nb and Cu added 18Cr-8Ni austenitic stainless steel, Materials Research Express, 5 (11) (2018) 116515.

    Article  Google Scholar 

  6. H. Tanaka, M. Murata, F. Abe and H. Irie, Microstructural evolution and change in hardness in type 304H stainless steel during long-term creep, Materials Science and Engineering A, 319–319 (2001) 788–791.

    Article  Google Scholar 

  7. V. H. Dao, K. B. Yoon, G. M. Yang and J. S. Oh, Determination of creep constitutive model for 28-48WCo alloy based on experimental creep tests at 817–817 °C, J. of Mechanical Science and Technology, 32 (9) (2018) 4201–4208.

    Article  Google Scholar 

  8. S. Yang, J. Zhou, X. Ling and Z. Yang, Effect of geometric factors and processing parameters on plastic damage of SUS304 stainless steel by small punch test, Materials and Design, 41 (2012) 447–452.

    Article  Google Scholar 

  9. M. P. Manahan, A. S. Argon and O. K. Harling, The development of a miniaturized disk bend test for the determination of postirradiation mechanical properties, J. of Nuclear Materials, 104 (1981) 1545–1550.

    Article  Google Scholar 

  10. T. Izaki, T. Kobayashi, J. Kusumoto and A. Kanaya, A creep life assessment method for boiler pipes using small punch creep test, International J. of Pressure Vessel Piping, 86 (9) (2009) 637–642.

    Article  Google Scholar 

  11. A. Moradi, N. Soltani and H. Nobakhti, Experimental study of remaining creep life of SA-304L stainless steel using small punch creep test, Materials at High Temperatures, 35 (5) (2017) 410–417.

    Article  Google Scholar 

  12. N. C. Z. Htun, T. T. Nguyen, D. Won, M. H. Nguyen and K. B. Yoon, Creep fracture behaviour of SUS304H steel with vanadium addition based on small punch creep testing, Materials at High Temperatures, 34 (1) (2017) 33–40.

    Article  Google Scholar 

  13. N. C. Z. Htun, T. T. Nguyen, K. B. Yoon and J. H Park, Small punch and uniaxial creep fracture behaviours of modified SUS304H steel at various temperatures, Materials at High Temperatures, 35 (4) (2018) 378–386.

    Article  Google Scholar 

  14. S. I. Komazaki, T. Kato, Y. Kohno and H. Tanigawa, Creep property measurements of welded joint of reducedactivation ferritic steel by the small-punch creep test, Materials Science and Engineering A, 510–510 (C) (2009) 229–233.

    Article  Google Scholar 

  15. Y. W. Ma, S. Shim and K. B. Yoon, Assessment of power law creep constants of Gr91 steel using small punch creep tests, Fatigue and Fracture Engineering Materials and Structures, 32 (12) (2009) 951–960.

    Article  Google Scholar 

  16. M. D. Mathew, J. G. Kumar, V. Ganesan and K. Laha, Small punch creep studies for optimization of nitrogen content in 316LN SS for enhanced creep resistance, Metallurgical and Materials Transactions A, 45 (2) (2014) 731–737.

    Article  Google Scholar 

  17. F. D. Persio, G. C. Stratford and R. C. Hurst, Validation of the small punch test as a method for assessing ageing of a V modified low alloy steel, Proc. of the Baltica VI International Conference on Life Management and Maintenance for Power Plants, Helsinki, Finland, 2 (2004) 523–535.

    Google Scholar 

  18. ASTM A213/213M: Standard Specification for Steamless Ferritic and Austenitic Alloy-steel Boiler, Superheater, and Heat-exchanger Tubes, ASTM International (2003).

  19. T. Zhou, R. P. Babu, J. Odqvist, H. Yu and P. Hedström, Quantitative electron microscopy and physically based modeling of Cu precipitation in precipitation-hardening martensitic stainless steel 15-5 PH, Materials and Design, 143 (2018) 141–149.

    Article  Google Scholar 

  20. Q. Xiong, J. D. Robson, L. Chang, J. W. Fellowes and M. C. Smith, Numerical simulation of grain boundary carbides evolution in 316H stainless steel, J. of Nuclear Materials, 508 (2018) 299–309.

    Article  Google Scholar 

  21. M. Hillert, The compound energy formalism, Journal of Alloys and Compounds, 320 (2) (2001) 161–176.

    Article  Google Scholar 

  22. V. Makarevičius, V. Baltušnikas, I. Lukošiūtė, R. Kriūkienė and A. Grybėnas, Transformation kinetic of M23C6 carbide lattice parameters in ferritic-martensitic P91 steel during thermal ageing, Proc. of Metal, Brno, Czech Republic (2015) 2–6.

    Google Scholar 

  23. S. Yamasaki, Modelling precipitation of carbides in martensitic steels, Doctoral Thesis, University of Cambridge, UK (2004).

    Google Scholar 

  24. S. R. Ortner, A stem study of the effect of precipitation on grain boundary chemistry in AISI 304 steel, Acta Metallurgica et Materialia, 39 (3) (1991) 341–350.

    Article  Google Scholar 

  25. X. M. Li, Y. Zou, Z. W. Zhang, Z. D. Zou and B. S. Du, Intergranular corrosion of weld metal of super type 304H steel during 650 °C aging, Corrosion, 68 (2012) 379–387.

    Article  Google Scholar 

  26. K. C. Sahoo, S. Goyal, V. Ganesan, J. Vanaja, G. V. Reddy, P. Padmanabhan and S. K. Laha, Analysis of creep deformation and damage behaviour of 304HCu austenitic stainless steel, Materials at High Temperatures (2019) 1–16.

    Google Scholar 

  27. C. Y. Chi, H. Y. Yu, J. X. Dong, W. Q. Li, S. C. Cheng, Z. D. Liu and X. S. Xie, The precipitation strengthening behavior of Cu-rich phase in Nb contained advanced Fe-Cr-Ni type austenitic heat resistant steel for USC power plant application, Progress in Natural Science: Materials International, 23 (3) (2012) 175–185.

    Article  Google Scholar 

  28. Y. Li, Y. Yang, Y. Wu, L. Wang and X. Liu, Quantitative comparison of three Ni-containing phases to the elevatedtemperature properties of Al-Si piston alloys, Materials Science and Engineering A, 527 (26) (2010) 7132–7137.

    Article  Google Scholar 

  29. S. Yang, X. Ling and Y. Zheng, Creep behaviors evaluation of Incoloy800H by small punch creep test, Materials Science and Engineering A, 685 (2017) 1–6.

    Article  Google Scholar 

  30. A. O. Mariscal, M. L. S. Munoz, Naveena and S. Komazaki, Application of small punch creep testing for evaluation of creep properties of as-received, Materials Science and Engineering A, 709 (2018) 322–329.

    Article  Google Scholar 

Download references

Acknowledgments

This work was supported by a Korea Institute of Energy Technology Evaluation and Planning (KETEP) [grant number 2014 1010101850] funded by the Ministry of Trade, Industry and Energy (MOTIE). This study was also supported by a KETEP [grant number 2016 1110100090] funded by the MOTIE.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Kee Bong Yoon.

Additional information

Recommended by Editor Chongdu Cho

Thi Giang Le received her B.S. in Metallurgical Engineering from Hanoi University of Science and Technology. She received the M.S. in Mechanical Engineering from Chung-Ang University. She is currently a Ph.D. candidate at Chung-Ang University. Her research interest is creep behavior and aging characteristics of high temperature alloy materials.

Kee Bong Yoon received his M.S. in Mechanical Engineering from KAIST and Ph.D. from Georgia Institute of Technology. He is currently a Professor at Chung-Ang University. His research interests are high temperature fracture and risk based management of energy plants. He is extending research to fracture of additive manufactured materials.

Tae Min Jeong received his B.S. and M.S. in Mechanical Engineering from Chung-Ang University. He conducted research on creep behavior and fracture of the high temperature materials. He is also interested in the life and integrity assessment of plant facilities. He is currently working on the team of NAND package front technology of SK Hynix Inc.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Le, T.G., Yoon, K.B. & Jeong, T.M. Degradation and reduction of small punch creep life of service-exposed Super304H steel. J Mech Sci Technol 33, 5243–5250 (2019). https://doi.org/10.1007/s12206-019-1014-6

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s12206-019-1014-6

Keywords

Navigation