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Superplastic Properties of AZ31 and AZ31-1.0Y-1.3Sr Alloy Produced by Twin-Roll Casting and Sequential Hot Rolling

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Abstract

Superplastic mechanical properties of the AZ31 and AZ31-1.0Y-1.3Sr magnesium alloy sheets produced by twin-roll casting and sequential hot rolling (TRC) were investigated. The AZ31-1.0Y-1.3Sr alloy sheets with the thickness of 1 mm were prepared by twin-roll casting process, which exhibited finer equiaxed grain structure. Uniaxial tensile testing and gas blow forming on AZ31 and AZ31-1.0Y-1.3Sr magnesium alloy sheets were carried out. Results show that the superplastic mechanical properties of AZ31-1.0Y-1.3Sr alloys are better than those of AZ31 alloys at 400 °C and the strain rate of 7 × 10−4/s. The addition of Y and Sr elements is helpful to improve the formability of AZ31 alloy. Grain boundary sliding plays a dominant role in superplastic forming.

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References

  1. H. Friedrich and S. Schumann, Research for a “New Age of Magnesium” in the Automotive Industry, J. Mater. Process. Technol., 2001, 117, p 276

    Article  Google Scholar 

  2. D.H. Ping, K. Hono, and J.F. Nie, Atom Probe Characterization of Plate-like Precipitates in a Mg-RE-Zn-Zr Casting Alloy, Scr. Mater., 2003, 48, p 1017–1022

    Article  Google Scholar 

  3. X. Huang, K. Suzuki, and N. Saito, Textures and Stretch Formability of Mg-6Al-1Zn Magnesium Alloy Sheets Rolled at High Temperatures up to 793K, Scr. Mater., 2009, 60, p 651–654

    Article  Google Scholar 

  4. H. Zhou, G.M. Cheng, X.L. Ma, W.Z. Xu, S.N. Mathaudhu, Q.D. Wang, and Y.T. Zhu, Effect of Ag on Interfacial Segregation in Mg-Gd-Y-(Ag)-Zr Alloy, Acta Mater., 2015, 95, p 20–29

    Article  Google Scholar 

  5. H. Yang, L. Huang, and M. Zhan, Coupled Thermo-Mechanical FE Simulation of the Hot Splitting Spinning Process of Magnesium Alloy AZ31, Comput. Mater. Sci., 2010, 47, p 857–866

    Article  Google Scholar 

  6. F.K. Farha and M.K. Khraisheh, Mechanical Characteristics of Superplastic Deformation of AZ31 Magnesium Alloy, J. Mater. Eng. Perform., 2007, 16, p 192–199

    Article  Google Scholar 

  7. H. Watanabe, H. Tsutsui, T. Mukai, K. Ishikawa, Y. Okanda, M. Kouzu, and K. Higashi, Superplastic Behavior in Commercial Wrought Magnesium Alloys, Mater. Sci. Forum., 2000, 350, p 171–176

    Article  Google Scholar 

  8. A.W. Morsy, K. Manabe, and H. Nishimura, Superplastic Forming of AZ31 Magnesium Alloy Sheet into a Rectangular Pan, Mater. Trans., 2002, 43, p 2443–2448

    Article  Google Scholar 

  9. Y.D. Yu, P. Jiang, J. Feng, and G.J. Wang, Properties and Microstructures Analysis of ZK60 Alloy Superplastic Sheet, J. Harbin Inst. Technol., 2011, 18, p 33–37

    Google Scholar 

  10. K.H. Kim and B.C. Suh, Microstructure and Texture Evolution of Mg Alloys During Twin-Roll Casting and Subsequent Hot Rolling, Scr. Mater., 2010, 63, p 716–720

    Article  Google Scholar 

  11. R.Q. Li, D.Q. Fang, J. An, Y. Lu, Z.Y. Cao, and Y.B. Liu, Comparative Studies on the Microstructure Evolution and Fracture Behavior Between Hot-Rolled and As-Cast Mg96ZnY3 Alloys, Mater. Charact., 2009, 60, p 470–475

    Article  Google Scholar 

  12. Y. Zhang, X.Q. Zeng, L.F. Liu, C. Lu, H.T. Zhou, Q. Li, and Y.P. Zhu, Effects of Yttrium on Microstructure and Mechanical Properties of Hot-extruded Mg-Zn-Y-Zr Alloys, Mater. Sci. Eng. A, 2004, 373, p 320–327

    Article  Google Scholar 

  13. D.H. Bae, S.H. Kim, W.T. Kim, and D.H. Kim, High Strength Mg-Zn-Y alloy Containing Quasicrystalline Particles, Mater. Trans., 2001, 42, p 2144–2147

    Article  Google Scholar 

  14. D. Xu, E.H. Han, L. Liu, and Y. Xu, Influence of Higher Zn/Y Ratio on the Microstructure and Mechanical Properties of Mg-Zn-Y-Zr Alloys, Metall. Mater. Trans. A, 2009, 40, p 1727–1740

    Article  Google Scholar 

  15. N. Kashefi and R. Mahmudi, The Microstructure and Impression Creep Behavior of Cast AZ80 Magnesium Alloy with Yttrium Additions, Mater. Design, 2012, 39, p 200–210

    Article  Google Scholar 

  16. H. Zhou, Q.D. Wang, and J. Chen, Microstructure and Mechanical Properties of Extruded Mg-8.5Gd-2.3Y-1.8Ag-0.4Zr Alloy, Trans. Nonferr. Metal. Soc., 2012, 22, p 1891–1895 (in Chinese)

    Article  Google Scholar 

  17. Y.D. Yu, Y.Q. Wang, K. Lin, and P. Jiang. Investigation of Gas Blow Forming Properties of AZ31+Y+Sr Magnesium Alloy Sheet, 2011 the 6th International Forum on Strategic Technology, Harbin, Aug 22-24, 2011, p 32–35.

  18. X.H. Chen and R. Xiao, Research Status on AZ Alloy, Metall. Mater. Trans. A, 2012, 41, p 14–18

    Google Scholar 

  19. S. Lee, S.H. Lee, and D.H. Kim, Effect of Y, Sr and Nd Additions on the Microstructure and Microfracture Mechanism of Squeeze-Cast AZ91-X Magnesium Alloys, Metall. Mater. Trans. A, 1998, 29, p 1221–1235

    Article  Google Scholar 

  20. D.G. Zhi, Fine Grain Superplastic and Heat Treatment, J. Heat Treat. Met, 1995, 10, p 45–46 (in Chinese)

    Google Scholar 

  21. H. Zhou, Q.D. Wang, B. Ye, and W. Guo, Hot Deformation and Processing Maps of As-Extruded Mg-9.8Gd-2.7Y-0.4Zr Mg Alloy, Mater. Sci. Eng. A, 2013, 576, p 101–107

    Article  Google Scholar 

  22. H. Zhou, W.Z. Xu, W.W. Jian, G.M. Cheng, X.L. Ma, W. Guo, S.N. Mathaudhu, Q.D. Wang, and Y.T. Zhu, A New Metastable Precipitate Phase in Mg-Gd-Y-Zr Alloy, Philos. Mag., 2014, 94, p 2403–2409

    Article  Google Scholar 

  23. S.C. Wu, Metallic Superplastic Deformation Theory, National Defence Industry Press, Beijing, 1997, p 34–104 (in Chinese)

    Google Scholar 

  24. Y.S. Li, D.Q. Dong, and Z.P. Wu, Research Status and Application Prospects of Rare Earth in Magnesium Alloys, J. Funct. Mater., 2006, 34, p 5001–5007 (in Chinese)

    Google Scholar 

  25. D.F. Zhang, S. Xia, F.S. Pan, L.Y. Jiang, G.S. Hu, and D.L. Yu, Research Status of Effect of Rare Earth Element on Mechanical Properties of Magnesium Alloys, J. Funct. Mater., 2014, 45, p p5001–5007 (in Chinese)

    Google Scholar 

  26. Y.D. Yu, P. Jiang, C.X. Li, and K. Lin, Microstructures and Mechanical Properties of AZ31+Sr+Y Magnesium Alloy Sheets Produced by Twin-Roll Casting and Sequential Hot Rolling, Adv. Mater. Res., 2013, 765–767, p 783–786

    Google Scholar 

  27. F.G. Qi and D.F. Zhang, Effect of Y Addition on Microstructure and Mechanical Properties of Mg-Zn-Mn Alloy, Trans. Nonferr. Metal. Soc., 2014, 24, p 1352–1364

    Article  Google Scholar 

  28. M.B. Yang and F.S. Pan, Effect of Strontium and Yttrium on Microstructure Refinement of Mg-3AL-1Zn Magnesium Alloy, China Foundry, 2009, 58, p 476–481 (in Chinese)

    Google Scholar 

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Acknowledgments

The authors gratefully acknowledge the financial support by the HarBin Science and Technology Burean (NO. 2014RFQXJ102), The School Youth Foundation of Heilongjiang Institute of Technology (NO. 2014QJ09), National Natural Science Foundation of China (NO. 51404082).

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Correspondence to Yandong Yu.

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Ning, H., Yu, Y., Lin, K. et al. Superplastic Properties of AZ31 and AZ31-1.0Y-1.3Sr Alloy Produced by Twin-Roll Casting and Sequential Hot Rolling. J. of Materi Eng and Perform 25, 635–641 (2016). https://doi.org/10.1007/s11665-015-1857-7

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  • DOI: https://doi.org/10.1007/s11665-015-1857-7

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