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Influence of Scanning Rotation on Nanoscale Artificial Strain in Open-Loop Atomic Force Microscopy

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Abstract

For nanoscale metrology using atomic force microscopy (AFM), it is essential to know the baseline error induced by the AFM scanning process. A systematic study has been performed using digital image correlation (DIC) to quantify the influence of scanning rotation angle on the artificial strain (error) in an open loop AFM. It is found that significant artificial strain has been induced by the scanning rotation angle, demonstrating that highly accurate metrology can only be performed in an open loop AFM when the scan angle is held constant during imaging.

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References

  1. Troyan VI, Pushkin MA, Tronin VN, Borman VD, Krasovskii PA (2008) Metrology and standards in nanotechnology. Meas Tech 51:992–997

    Article  Google Scholar 

  2. Tong W, Hector LG, Weiland H (1997) In-situ surface characterization of a binary aluminum alloy during tensile deformation. Scripta Mater 36:1339–1344

    Article  Google Scholar 

  3. Cretegny L, Saxena A (2001) AFM Characterization of the evolution of surface deformation during fatigue in polycrystalline copper. Acta Mater 49:3755–3765

    Article  Google Scholar 

  4. Chandrasekaran D, Nygards M (2003) A study of the surface deformation behavior at grain boundaries in an ultra-low-carbon steel. Acta Mater 51:5375–5384

    Article  Google Scholar 

  5. Bobji MS, Bhushan B (2003) A technique to measure Poisson’s ratio of ultrathin polymeric films using atomic force microscopy. Rev Sci Instrum 74:1043–1047

    Article  Google Scholar 

  6. Dasari A, Rohrmann J, Misra RDK (2003) Atomic force microscopy assessment of mechanically induced scratch damage in polypropylenses and ethylene-propylene di-block copolymers. Mater Sci Eng A 354:67–81

    Article  Google Scholar 

  7. Chasiotis I, Fillmore HL, Gillies GT (2003) Atomic force microscopy measurement of cytostructural elements involved in the nanodynamics of tumor cell invasion. Nanotechnol 14:557–561

    Article  Google Scholar 

  8. Chasiotis I, Knauss WG (2002) A new microtensile tester for the study of MEMS materials with the aid of atomic force microscopy. Exp Mech 42:51–57

    Article  Google Scholar 

  9. Cho SW, Chasiotis I, Friedman TA, Sullivan J (2005) Young’s modulus, Poisson’s ratio and failure properties of tetrahedral amorphous diamond-like carbon for MEMS devices. J Micromech Microeng 15:728–735

    Article  Google Scholar 

  10. Cho SW, Cardenas-Garcia JF, Chasiotis I (2005) Measurement of nanodisplacements and elastic properties of MEMS via the microscopic hole method. Sens Actuat A Phys 120:163–171

    Article  Google Scholar 

  11. Cho SW, Chasiotis I (2007) Elastic properties and representative volume element of polycrystalline silicon for MEMS, Exp. Mech 47:37–49

    Google Scholar 

  12. Vogel D, Kuhnert R, Dost M, Michel B (2002) Determination of packaging material properties utilizing image correlation techniques. J Electr Pack 124:345–351

    Article  Google Scholar 

  13. Li XD, Xu WJ, Sutton MA, Mello M (2006) Nanoscale deformation and cracking studies of advanced metal evaporated magnetic tapes using atomic force microscopy and digital image correlation techniques. Mater Sci Technol 22:835–844

    Article  Google Scholar 

  14. Li XD, Xu WJ, Sutton MA, Mello M (2007) In situ nanoscale in-plane deformation studies of ultrathin polymeric films during tensile deformation using atomic force microscopy and digital image correlation techniques. IEEE Trans Nanotechnol 6:4–12

    Article  Google Scholar 

  15. Xu ZH, Sutton MA, Li XD (2008) Mapping nanoscale wear field by combined atomic force microscopy and digital image correlation techniques. Acta Mater 56:6304–6309

    Article  Google Scholar 

  16. Peters WH, Ranson WR (1982) Digital imaging techniques in experimental stress analysis. Opt Eng 21:427–432

    Google Scholar 

  17. McNeill SR, Sutton MA, Wolters WJ, Peters WH (1983) Determination of displacements using an improving digital correlation method. Image Vis Comput 1:1333–1339

    Google Scholar 

  18. Sutton MA, Cheng M, Peters WH, Chao YJ, McNeill SR (1986) Application of an optimized digital correlation method to planar deformation analysis. Image Vis Comput 4:143–153

    Article  Google Scholar 

  19. Bruck HA, McNeill SR, Sutton MA, Peters WH (1989) Digital image correlation using Newton-Raphson method of partial differential correction. Exp Mech 29:262–267

    Article  Google Scholar 

  20. Vendroux G, Knauss WG (1998) Submicron deformation field measurements: part 2. Improved digital image correlation. Exp Mech 38:86–91

    Article  Google Scholar 

  21. Jin H, Bruck HA (2005) A new method for characterizing nonlinearity in scanning probe microscopes using digital image correlation. Nanotechnol 16:1849–1855

    Article  Google Scholar 

  22. Sun Y, Pang JHL (2006) AFM image reconstruction for deformation measurements by digital image correlation. Nanotechnol 17:933–939

    Article  Google Scholar 

  23. Xu ZH, Li XD, Sutton MA, Li N (2008) Drift and spatial distortion elimination in atomic force microscopy images by the digital image correlation technique. J Strain Anal Eng Design 43:729–743

    Article  Google Scholar 

  24. Digital Instruments Veeco Metrology Group (2000) Nanoscope Command Reference Manual, Version 5.12, Revision B, 004-122-000.

  25. Chasiotis I (2008) Chapter 17: atomic force microscopy in solid mechanics. In: Sharp WN Jr (ed), Handbook for experimental solid mechanics. Springer, p 409–443

  26. Marinello F, Bariani P, Carmignato S, Savio E (2009) Geometrical modeling of scanning probe microscopes and characterization of errors. Meas Sci Technol 20:084013

    Article  Google Scholar 

Download references

Acknowledgements

This work was supported by the National Science Foundation (CMMI-0653651, CMMI-0968843, and CMMI-824728) and the University of South Carolina NanoCenter.

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Correspondence to Xiaodong Li.

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Xu, ZH., Jin, H., Lu, WY. et al. Influence of Scanning Rotation on Nanoscale Artificial Strain in Open-Loop Atomic Force Microscopy. Exp Mech 51, 619–624 (2011). https://doi.org/10.1007/s11340-010-9442-3

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  • DOI: https://doi.org/10.1007/s11340-010-9442-3

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