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Crystal Structure of A Molecular Complex Compound of Antimony(III) Fluoride with L-Leucine

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Abstract

Single crystal X-ray diffraction analysis is used to determine the crystal structure of a newly synthesized molecular complex compound of antimony(III) fluoride with L-leucine of the composition SbF3(C6H13NO2) (orthohombic crystal system: a = 5.7948(8) Å, b = 6.2433(9) Å, c = 28.594(4) Å, Z = 4, P212121 space group). The structure consists of SbF3 molecules and L-leucine bound into polymer chains by bidentate bridging carboxyl groups of amino acid molecules. Weak Sb…F(1)b bonds combine the adjacent chains into polymer ribbons organized by N-H…. F and N-H…. O hydrogen bonds into a framework.

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Authors and Affiliations

  1. Institute of Chemistry, Far East Division, Russian Academy of Sciences, Vladivostok, Russia

    A. A. Udovenko, N. V. Makarenko, R. L. Davidovich, L. A. Zemnukhova & E. V. Kovaleva

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  1. A. A. Udovenko
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  2. N. V. Makarenko
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  3. R. L. Davidovich
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  4. L. A. Zemnukhova
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  5. E. V. Kovaleva
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Correspondence to A. A. Udovenko.

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Original Russian Text Copyright © 2010 by A. A. Udovenko, N. V. Makarenko, R. L. Davidovich, L. A. Zemnukhova, and E. V. Kovaleva

Translated from Zhurnal Strukturnoi Khimii, Vol. 51, No. 4, pp. 792–795, July–August, 2010.

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Udovenko, A.A., Makarenko, N.V., Davidovich, R.L. et al. Crystal Structure of A Molecular Complex Compound of Antimony(III) Fluoride with L-Leucine. J Struct Chem 51, 765–768 (2010). https://doi.org/10.1007/s10947-010-0113-0

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  • DOI: https://doi.org/10.1007/s10947-010-0113-0

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