Skip to main content
Log in

Determination of mixing time by colourimetric diagnosis—Application to a new mixing system

  • Original
  • Published:
Experiments in Fluids Aims and scope Submit manuscript

Abstract

A method for determining mixing times in a transparent stirred vessel for highly viscous fluids has been developed. The method involves a chemical decolourization with two acid-base indicators and a colourimetric diagnosis of digital images, deduced from a video captured during the mixing process. The advantages of the method developed are:(1) there is no disturbance of the fluid flow, and (2) measuring and determination of the degree of homogeneity is relatively effortless and cheap since it requires only a standard colour camera and commercial software for digital image analysis. This paper describes protocols for carrying this method out. In addition, examples of experimental results obtained for a standard impeller (of the helical ribbon agitator type) and a new piece of mixing equipment are given and discussed.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8

Similar content being viewed by others

References

  • Brito-de la Fuente E, Leuliet JC, Choplin L, Tanguy PA (1990) Mixing and circulation times in rheologically complex fluids. AIChE Symposium Series 121:76–96

    Google Scholar 

  • Carreau PJ, Patterson I, Yap CY (1976) Mixing of viscoelastic fluids with helical-ribbon agitators, part I: mixing time and flow patterns. Can J Chem Eng 54:135–142

    CAS  Google Scholar 

  • Coyle CK, Hirschland HE, Michel BJ, Oldshue JY (1970) Mixing in viscous liquids. AIChE J 16(6):903–906

    Google Scholar 

  • Delaplace G, Dieulot JY, Leuliet JC, Brienne JP (1999) Détermination expérimentale et prédiction des temps de circulation et de mélange pour un système d’agitation hélicoïdal. Can J Chem Eng 77:447–457

    CAS  Google Scholar 

  • Delaplace G, Leuliet J-C, Relandeau V (2000) Circulation and mixing times for helical ribbon impellers, review and experiments. Exp Fluids 28:170–182

    Article  Google Scholar 

  • Dieulot JY, Delaplace G, Guerin R, Brienne JP, Leuliet JC (2002) Laminar mixing performances of a stirred tank equipped with helical ribbon agitator subjected to steady and unsteady rotational speed. Trans IchemE 80(A):335–344

    Article  CAS  Google Scholar 

  • Gray JB (1963) Batch mixing of viscous liquids. Chem Eng Progress 59(3):55–59

    CAS  Google Scholar 

  • Havas G, Sawinsky J, Deak A (1978) Investigation of the homogenization efficiency of the screw agitator, helical ribbon agitator, gate type anchor impeller and the multi-paddle agitator in the mixing of high-viscosity newtonian liquids. Periodica Polytechnica Chem Eng 22:317–330

    CAS  Google Scholar 

  • Hiby JW (1981) Definition and measurement of the degree of mixing in liquid mixtures. Int Chem Eng 21(2):197–204

    Google Scholar 

  • Ho F, Kwong A (1973) A guide to designing. Chem Eng 95–104

  • Hoogendoorn CJ, Den Hartog AP (1967) Model studies on mixers in the viscous flow region. Chem Eng Sci 22:1689–1699

    Article  CAS  Google Scholar 

  • Käppel M (1979) Development and application of a method for measuring the mixture quality of miscible liquids, part I: state of research and theoretical principles. Int Chem Eng 19(2):196–215

    Google Scholar 

  • Melton LA, Lipp CW, Spradling RW, Paulson KA (2002) DISMT-Determination of mixing time through color changes. Chem Eng Comm 189(3):322–338

    Article  CAS  Google Scholar 

  • Nagata S, Yanagimoto M, Yokoyama T (1956) Studies on the mixing of high viscous liquids. Memoirs of the faculty of engineering, Kyoto University, 18:444–460

    Google Scholar 

  • Patterson WI, Carreau PJ, Yap CY (1979) Mixing with helical ribbon agitators, part II: newtonian fluids. AIChE J 25(3):508–516

    CAS  Google Scholar 

  • Takahashi K, Takata Y, Yokota T, Konno H (1985) Mixing of two miscible highly viscous newtonian liquids in a helical ribbon agitator. J Chem Eng Japan 18(2):159–162

    CAS  Google Scholar 

  • Takahashi K, Yokota T, Furukawa T, Harada K (1994) Mixing of highly viscous newtonian liquid in a helical ribbon agitated vessel at various liquid depths. J Chem Eng Japan 27(2):244–247

    CAS  Google Scholar 

  • Zlokarnick M (1967) Eignung von Rührern zum Homogenisieren von Flussigkeitsgemischen. Chem Ing Techn 39:539–548

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to G. Delaplace.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Delaplace, G., Bouvier, L., Moreau, A. et al. Determination of mixing time by colourimetric diagnosis—Application to a new mixing system. Exp Fluids 36, 437–443 (2004). https://doi.org/10.1007/s00348-003-0741-7

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s00348-003-0741-7

Keywords

Navigation