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Thermal Analysis of Processes at the Solid-Phase Synthesis of Lithium-Titanium Ferrite

  • XVI INTERNATIONAL CONFERENCE ON THERMAL ANALYSIS AND CALORIMETRY IN RUSSIA
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Abstract

In this study, the reactivity of a Fe2O3–Li2CO3–TiO2 mixture with different initial densities was investigated by thermal and kinetic methods to analyze phase formation of lithium titanium ferrite. Test samples were powder with a density of 1 g/cm3 and a compact with a density of 2.6 g/cm3. High-density samples were formed by single-action cold compaction. It is shown that the reaction of solid-phase interaction of lithium-titanium ferrite strongly depends on the degree of compaction. The mass of the powder mixture sample decreases in the temperature range of 500–720°C. In compacts, the reaction of solid-phase interaction starts at lower temperature (∼420°C). In addition, it is shown that in compacted samples, a lithium ferrite spinel phase is formed during heating. The kinetic analysis was used to determine the kinetic model of the synthesis reaction of lithium-titanium ferrite and to calculate the parameters of this process.

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ACKNOWLEDGMENTS

This research was supported by the Russian Science Foundation (grant no. 19-72-10078).

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  1. Tomsk Polytechnic University, 634050, Tomsk, Russia

    E. V. Nikolaev, E. N. Lysenko & A. P. Surzhikov

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  1. E. V. Nikolaev
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  2. E. N. Lysenko
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  3. A. P. Surzhikov
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Correspondence to E. V. Nikolaev.

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Nikolaev, E.V., Lysenko, E.N. & Surzhikov, A.P. Thermal Analysis of Processes at the Solid-Phase Synthesis of Lithium-Titanium Ferrite. Russ. J. Phys. Chem. 95, 882–886 (2021). https://doi.org/10.1134/S0036024421050204

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  • DOI: https://doi.org/10.1134/S0036024421050204

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