Abstract
The hot deformation behavior of X45CrSi93 valve steel was investigated by a series of compression and tensile tests by means of the Gleeble-1500 simulator and microstructural analyses. The experimental results show that the flow stress decreases with the increasing temperature between 850 and 900 °C followed by an abnormal increase with the increasing temperature between 900 and 1000 °C under the compressive conditions. A normal decrease of the flow stress is continued with the increasing temperature above 1000 °C. Meantime, the tensile specimen conducted at 1000 °C shows double necking effect. Further microstructural analyses show that the phase transition from α-ferrite to austenite and the solution strengthening caused by carbide dissolution are the main reasons for abnormal variation of flow stress for X45CrSi93. The negative temperature gradient in the tensile specimen results in the symmetrical microstructure and then the double necking phenomenon.
Similar content being viewed by others
REFERENCES
T.Y. Qin: Development status of property and application for engine valve steel. Shanghai Met. 02, 50 (2011).
M. Atapour and F. Ashrafizadeh: Cyclic oxidation behavior of plasma nitrided valve steel. Phys. Procedia 32, 853 (2012).
H. Berns, C. Escher, and W.D. Streich: Martensitic high nitrogen steel for applications at elevated temperature. Mater. Sci. Forum 318, 443 (1999).
Z. Grzesik, G. Smola, K. Adamaszek, Z. Jurasz, and S. Mrowec: High temperature corrosion of valve steels in combustion gases of petrol containing ethanol addition. Corros. Sci. 77, 369 (2013).
A. Ramalho, P. Kapsa, G. Bouvard, J.C. Abry, T. Yoshida, and M. Charpentier: Effect of temperatures up to 400 °C on the impact-sliding of valve-seat contacts. Wear 267 (5), 777 (2009).
H.J.C. Voorwald, R.C. Coisse, and M.O.H. Cioffi: Fatigue strength of X45CrSi93 stainless steel applied as internal combustion engine valves. Procedia Eng. 10, 1256 (2011).
M. Azadi, M. Roozban, and A. Mafi: Failure analysis of an intake valve in a gasoline engine. J. Eng. Res. 26, 03 (2012).
Y. Hu, M.J. Xu, C.F. Gan, Z. Guo, and M. Huang: Failure analysis of the fracture on valve steel X45CrSi93. CISC Technol. 51 (4), 14 (2008).
Y.C. Lin, M.S. Chen, and J. Zhong: Effect of temperature and strain rate on the compressive deformation behavior of 42CrMo steel. J. Mater. Process. Technol. 205 (1), 308 (2008).
M.Y. Zheng, Z.R. Zhang, L.L. Song, and D.Q. Mo: High temperature compression behavior of 21-4N valve steel in hot-working process. Mater. Heat Treat. 02, 46 (2012).
A. Momeni and K. Dehghani: Characterization of hot deformation behavior of 410 martensitic stainless steel using constitutive equations and processing maps. J. Mater. Process. Technol. 527 (21), 5467 (2010).
Y. Han, D. Zou, Z. Chen, G.W. Fan, and W. Zhang: Investigation on hot deformation behavior of 00Cr23Ni4N duplex stainless steel under medium–high strain rates. Mater. Charact. 62 (2), 198 (2011).
H. Farnoush, A. Momeni, K. Dehghani, J.A. Mohandesi, and H. Keshmiri: Hot deformation characteristics of 2205 duplex stainless steel based on the behavior of constituent phases. Mater. Des. 31 (1), 220 (2010).
D.Y. Cai, L.Y. Xiong, W.C. Liu, G.D. Sun, and M. Yao: Characterization of hot deformation behavior of a Ni-base superalloy using processing map. Mater. Des. 30 (3), 921 (2009).
S.I. Oh, S.L. Semiatin, and J.J. Jonas: An analysis of the isothermal hot compression test. Metall. Trans. A 23 (3), 963 (1992).
J. Wu: Duplex Stainless Steel (Metallurgical Industry Press, Beijing, 2000); pp. 17–18.
Y.N. Yu: Fundamentals of Materials Science, 1st ed. (Higher Education Press, Beijing, 2006); pp. 387–391, 453–454.
G.L. Chen, X.S. Xie, and R.C. Ye: Superalloys (Metallurgical Industry Press, Beijing, 1988); pp. 5–6.
R.Z. Zhu and Y.X. Lu: Heat-Resistant Steel and Superalloy (Chemical Industry Press, Beijing, 1995); pp. 151.
A. Chiba and M.S. Kim: Suzuki segregation and dislocation locking in supersaturated Co-Ni-based alloy. Mater. Trans. 42 (10), 2112 (2001).
ACKNOWLEDGMENTS
The authors would like to thank for the financial support from MCC Capital Engineering & Research Incorporation Limited and the facilities provided by materials experimental test center in School of Materials Science and Engineering, University of Science and Technology Beijing.
Author information
Authors and Affiliations
Corresponding author
Additional information
Contributing Editor: Jürgen Eckert
Rights and permissions
About this article
Cite this article
Wu, Y., Zhang, M. & Xu, X. Investigations on hot deformation behaviors and abnormal variation mechanisms of flow stress at elevated temperature for X45CrSi93 valve steel. Journal of Materials Research 30, 1715–1726 (2015). https://doi.org/10.1557/jmr.2015.98
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1557/jmr.2015.98