Abstract
The formation of carbon nanoparticles with ordered structure under nanosecond-duration pulsed laser irradiation of the carbon black samples has been studied. Electron microscopic images of the original and irradiated samples have been obtained and analyzed using the Digital Micrograph software package (Gatan). The length and curvature of graphene layers in high- and low-dispersive carbon black samples have been calculated. The distance between graphene layers (d 002) has been measured. It was shown that the distance d 002 decreases with an increase in the irradiation energy density.
This is a preview of subscription content, log in via an institution to check access.
Similar content being viewed by others
References
J.-N. Rouzaud and C. Clinard, “Quantitative high-resolution transmission electron microscopy: a promising tool for carbon materials characterization,” Fuel Processing Technol. 77–78, 229–235 (2002).
M. Endos, T. Furuta, F. Minoura, and C. Kim, “Visualized observation of pores in activated carbon fibers by HRTEM and combined image processor,” Supramolec. Sci. 5, 261–266 (1998).
Sharma Atul, Takashi Kyotani, and Tomita Akira, “Comparison of structural parameters of PF carbon from XRD and HRTEM techniques,” Carbon 38, 1977–1984 (2000).
K. Yehliu, R. L. Vander Wal, and A. L. Boehman, “Development of an HRTEM image analysis method to quantify carbon nanostructure,” Combust. Flame 158, 1837–1851 (2011).
A. Sharma, T. Kyotani, and A. Tomita, “A new quantitative approach for microstructural analysis of coal char using HRTEM images,” Fuel 78, 1203–1212 (1999).
Yang Jun-he, Cheng Shu-hui, Wang Xia, Zhang Zhuo, Liu Xiao-rong, and Tang Guo-hua, “Trans. quantitative analysis of microstructure of carbon materials by HRTEM,” Nonferr. Met. SOCC. China 16, 796–803 (2006).
J. O. Müller, D. S. Su, U. Wild, and R. Schloegl, “Bulk and surface structural investigations of diesel engine soot and carbon black,” Phys. Chem. Chem. Phys. 9, 4018–4025 (2007).
V. I. Ivanovskii, Technical Carbon. Processes and Apparatuses (OJSC Tekhuglerod, Omsk, 2004), p. 228 [in Russian].
W. Zhu, D. E. Miser, W. G. Chan, and M. R. Hajaligol, “HRTEM investigation of some commercially available furnace carbon blacks,” Carbon 42, 1841–1845 (2004).
H.-S. Shim, R. H. Hurt, and N. Y. C. Yang, “A methodology for analysis of 002 lattice fringe images and its application to combustion-derived carbons,” Carbon 38, 29–45 (2000).
K. Oshida, T. Nakazawa, T. Miyazaki, and M. Endo, “Application of image processing techniques for analysis of nano- and micro-spaces in carbon materials,” Synth. Met. 125, 223–230 (2002).
L. R. Vander Wal and Y. C. Mun, “Pulsed laser heating of soot: morphological changes,” Carbon 37, 231–239 (1999).
H. Bladh, J. Johnsson, and P.-E. Bengtsson, “On the dependence of the laser-induced incandescence (LII) signal on soot volume fraction for variations in particle size,” Appl. Phys. B 90(1), 109–125 (2008).
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text © M.V. Trenikhin, O.V. Protasova, G.M. Seropyan, A.E. Zemtsov, V.A. Drozdov, 2014, published in Rossiiskie Nanotekhnologii, 2014, Vol. 9, Nos. 7–8.
Rights and permissions
About this article
Cite this article
Trenikhin, M.V., Protasova, O.V., Seropyan, G.M. et al. Transmission electron microscopy study of the graphene layer transformation of carbon black under laser irradiation. Nanotechnol Russia 9, 461–465 (2014). https://doi.org/10.1134/S1995078014040193
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1995078014040193