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Synthesis and properties of copolyimides based on ternary dianhydrides and dibasic diamines

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Abstract

A series of copolyimides were prepared by thermal imidization of polyamide acids derived from 3,3′,4,4′-biphenyltetracarboxylic dianhydride, 2,3′,3,4′-biphenyltetracarboxylic dianhydride, pyromellitic dianhydride, p-phenylenediamine and 4,4′-oxydialinine commonly used for the production of commercial polyimides. The flexible copolyimide films characterized by ultra-low coefficient of thermal expansion were obtained and characterized by FTIR, WAXD, TG, DMA, TMA, FE-SEM and tensile properties measurement. The results showed that three copolyimides remained semi-crystalline and exhibited high glass transition temperature, high thermal stability, and great ultimate strength.

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Authors and Affiliations

  1. School of Chemical Engineering, Nanjing University of Science and Technology, Nanjing, 210094, China

    Yonglin Lei

  2. Research Center of Laser Fusion, Chinese Academy of Engineering Physics, Mianyang, 621900, China

    Yonglin Lei & Yongjian Tang

  3. Engineering Research Center of Biomass Materials, Ministry of Education, School of Materials Science and Engineering, Southwest University of Science and Technology, Mianyang, 621010, China

    Yonglin Lei & Jichuan Huo

  4. Xian Modern Chemistry Research Institute, Xian, 710065, China

    Yuanjie Shu

Authors
  1. Yonglin Lei
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  2. Yuanjie Shu
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  3. Yongjian Tang
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  4. Jichuan Huo
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Correspondence to Yonglin Lei.

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Lei, Y., Shu, Y., Tang, Y. et al. Synthesis and properties of copolyimides based on ternary dianhydrides and dibasic diamines. Polym. Sci. Ser. B 57, 576–583 (2015). https://doi.org/10.1134/S1560090415070027

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  • DOI: https://doi.org/10.1134/S1560090415070027

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