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Chemical synthesis and granulometric composition of CaZr0.9Y0.1O3–δ powders

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Abstract

CaZr0.9Y0.1O3–δ powders were synthesized by chemical solution methods: modified Pechini method and from solutions of inorganic salts in water and ethanol. The structure crystallizes into the orthorhombic type upon annealing at 1000°C for powders prepared by the Pechini method and from solution of salts in water. It was shown that CaZr0.9Y0.1O3–δ powders synthesized by various methods have different dispersities. The results obtained in a study of the granulometric composition by the sedimentation method and microscopic analysis enable fabrication of dense and mechanically strong electrolyte films and ceramics.

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Authors and Affiliations

  1. Institute of High-Temperature Electrochemistry, Ural Branch, Russian Academy of Sciences, ul. Akademicheskaya 20, Yekaterinburg, 620137, Russia

    A. Sh. Khaliullina, V. M. Kuimov, S. A. Belyakov & L. A. Dunyushkina

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  1. A. Sh. Khaliullina
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  2. V. M. Kuimov
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  3. S. A. Belyakov
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  4. L. A. Dunyushkina
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Correspondence to A. Sh. Khaliullina.

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Original Russian Text © A.Sh. Khaliullina, V.M. Kuimov, S.A. Belyakov, L.A. Dunyushkina, 2017, published in Zhurnal Prikladnoi Khimii, 2017, Vol. 90, No. 3, pp. 279−285.

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Khaliullina, A.S., Kuimov, V.M., Belyakov, S.A. et al. Chemical synthesis and granulometric composition of CaZr0.9Y0.1O3–δ powders. Russ J Appl Chem 90, 342–348 (2017). https://doi.org/10.1134/S107042721703003X

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  • DOI: https://doi.org/10.1134/S107042721703003X

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