Abstract
Products of tetramethyllead dealkylation with bromine in the temperature interval from −20 to 20°C were analyzed by X-ray diffraction, IR spectroscopy, and spectrophotometry. Specific features of their thermal behavior were studied by differential thermal analysis and mass spectrometry.
Similar content being viewed by others
References
Izotopy: svoistva, poluchenie, primenenie (Isotopes: Properties, Production, Use), Baranov, V.Yu., Ed., Moscow: Fizmatlit, 2005, vol. 2
Application of Stable Lead Isotope Pb-208 in Nuclear Power Engineering and Its Acquisition Techniques, Khorasanov, G.L., Ed., New York: Nova Science, 2013.
Bokhan, P.A., Buchanov, V.V., Zakrevskii, D.E., et al., Alternat. Energet. Ekol., 2007, vol. 47, no. 3, pp. 92–105.
Shmelev, A.N., Kulikov, G.G., Apse, V.A., et al., Sci. Technol. Nucl. Install., 2011, ID 252903, pp. 1–12.
Smirnov, A.Yu., Borisevich, V.D., and Sulaberidze, G.A., Theor. Found. Chem. Eng., 2012, vol. 46, no. 4, pp. 373–378.
Clouston, J.G. and Cook, C.L., Trans. Faraday Soc., 1958, vol. 54, pp. 1001–1007.
Simons, J.H., McNamee, R.W., and Hurd, C., J. Phys. Chem., 1932, vol. 36, pp. 939–948.
Kocheshkov, K.A., Zemlyanskii, N.N., Sheverdina, N.I., and Panov, E.M., Metody elementoorganicheskoi khimii. Germanii, olovo, svinets (Methods of Organometallic Chemistry. Germanium, Tin, and Lead), Moscow: Nauka, 1968.
Akimov, D.V., Andrienko, O.S., Egorov, N.B., et al., Alternat. Energet. Ekol., 2013, no. 4-1, pp. 36–40.
Schmidt, U. and Huber, F., Anal. Chim. Acta, 1978, vol. 98, pp. 147–149.
Clark, R.J.H., Davies, A.G., and Puddephatt, R.J., J. Am. Chem. Soc., 1968, vol. 90, no. 25, pp. 6923–6927.
Quinn, E.I., Dibeler, V.H., and Mohler, F.L., J. Res. NBS, 1956, vol. 57, no. 1, pp. 41–43.
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text © N.B. Egorov, 2014, published in Zhurnal Prikladnoi Khimii, 2014, Vol. 87, No. 5, pp. 636–641.
Rights and permissions
About this article
Cite this article
Egorov, N.B. Products of tetramethyllead dealkylation with bromine. Russ J Appl Chem 87, 624–628 (2014). https://doi.org/10.1134/S1070427214050152
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1070427214050152