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Solvothermal synthesis of nanosized particles of vanadium oxide

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Abstract

The interaction of vanadyl acetate, vanadium(V) oxide, and vanadium(V) isopropylate with capronic acid has afforded a series of nanosized vanadium oxide powders. The products structure has been studied by X-ray diffraction analysis. Both amorphous and crystalline powders of vanadium oxide can be prepared depending on the starting compound, temperature, and the synthesis duration, the V2O3 (karelianite) structure being in all the cases the most thermodynamically stable. Photocatalytic properties of the prepared powders have been studied.

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References

  1. Yu, W.C., Wu, X.D., Si, Z.C., and Weng, D., Appl. Surf. Sci., 2013, vol. 283, p. 209. DOI: 10.1016/j.apsusc.2013.06.083.

    Article  CAS  Google Scholar 

  2. Zhu, J.X., Cao, L.J., Wu, Y.S., Gong, Y.J., Liu, Z., Hoster, H.E., Zhang, Y.H., Zhang, S.T., Yang, S.B., Yan, Q.Y., Ajayan, P.M., and Vajtai, R., Nano Lett., 2013, vol. 13, p. 5408. DOI: 10.1021/nl402969r.

    Article  CAS  Google Scholar 

  3. Kong, F.Y., Li, M., Yao, X.Y., Xu, J.M., Wang, A.D., Liu, Z.P., and Li, G.H., Cryst. Eng. Commun., 2012, vol. 14, p. 3858. DOI: 10.1039/C2CE25199J.

    Article  CAS  Google Scholar 

  4. Yu, M.L., Liu, X.Q., Wang, Y., Zheng, Y.B., Zhang, J.W., Li, M.Y., Lan, W., and Su, Q., Appl. Surf. Sci., 2012, vol. 258, p. 9554. DOI: 10.1016/j.apsusc.2012.05.120.

    Article  CAS  Google Scholar 

  5. Vinogradova, O.P., Sidorov, A.I., Klimov, V.A., Shadrin, E.B., Nashchekin, A.V., Khanin, S.D., and Lyubimov, V.Yu., Phys. Solid State, 2008, vol. 50, p. 1227. DOI: 10.1134/S1063783408070068.

    Article  CAS  Google Scholar 

  6. Manning, T.D., Parkin, I.P., Pemble, M.E., Sheel, D., and Vernardou, D., Chem. Mater., 2004, vol. 16, p. 744. DOI: 10.1021/cm034905y.

    Article  CAS  Google Scholar 

  7. Mori, K., J. Soc. Powder Technol. Japan, 2004, vol. 41, p. 750.

    CAS  Google Scholar 

  8. Zdravkov, A., Kudryashova, Ju., Kanaev, A., Povolotskiy, A., Volkova, A., Golikova, E., and Khimich, N., Mater. Chem. Phys., 2015, vol. 160, p. 73. DOI: 10.1016/j.matchemphys., 2015.04.008.

    Article  CAS  Google Scholar 

  9. Choudary, B.M., Lakshmi Kantam, M., Neeraja, V., Tapasree Bandyopadhyay, and Narsi Reddy, P., J. Mol. Catal. (A), 1998, vol. 140, p. 25. DOI: 10.1016/S1381-1169(98)00214-3.

    Article  Google Scholar 

  10. Magomedov, G.K.-I., Morozova, L.V., Kusainova, K.M., Blokhina, E.I., Medvedeva, A.V., and Beletskaya, I.P., Zh. Obshch. Khim., 1989, vol. 59, no. 8, p. 1777.

    CAS  Google Scholar 

  11. Theobald, F.G., J. Solid State Chem., 1976, vol. 17, p. 431. DOI: 10.1016/S0022-4596(76)80013-8.

    Article  CAS  Google Scholar 

  12. Rice, C.E. and Robinson, W.R., J. Solid State Chem., 1977, vol. 21, p. 145. DOI: 10.1016/0022-4596(77)90154-2.

    Article  CAS  Google Scholar 

  13. Slotvinskii-Sidak, N.P., Vanadii v prirode i v tekhnike (Vanadium in Nature and in Technology), Moscow: Nauka, 1979.

    Google Scholar 

  14. Hetch, H., Jander, G., and Schlapmann, H., Z. Anorg. Allgem. Chem., 1947, vol. 254, p. 255. DOI: 10.1002/zaac.,19472540501.

    Article  Google Scholar 

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Authors and Affiliations

  1. Institute of Silicates Chemistry, Russian Academy of Sciences, St. Petersburg, Russia

    A. V. Zdravkov & L. A. Koptelova

  2. St. Petersburg State Technological University of Plant Polymers, St. Petersburg, Russia

    M. A. Gorbunova & N. N. Khimich

  3. Kirov Military Medical Academy, ul. Akademika Lebedeva 6/Zh, St. Petersburg, 194044, Russia

    N. N. Khimich

Authors
  1. A. V. Zdravkov
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  2. M. A. Gorbunova
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  3. L. A. Koptelova
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  4. N. N. Khimich
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Corresponding author

Correspondence to N. N. Khimich.

Additional information

Original Russian Text © A.V. Zdravkov, M.A. Gorbunova, L.A. Koptelova, N.N. Khimich, 2016, published in Zhurnal Obshchei Khimii, 2016, Vol. 86, No. 2, pp. 191–195.

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Zdravkov, A.V., Gorbunova, M.A., Koptelova, L.A. et al. Solvothermal synthesis of nanosized particles of vanadium oxide. Russ J Gen Chem 86, 219–223 (2016). https://doi.org/10.1134/S1070363216020031

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  • DOI: https://doi.org/10.1134/S1070363216020031

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