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Nickel hexacyanoferrate nanoparticles/nano silver coated multiwalled carbon nanotubes nanocomposite for the detection of hydrogen peroxide

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Abstract

A new nanocomposite was developed by combination of nickel hexacyanoferrate nanoparticles (NiNP) and nano silver coated multiwalled carbon nanotubes (nano Ag-MWNTs). The NiNP/nano Ag-MWNTs nanocomposite was charactered by scanning electron microscopy (SEM). The NiNP/nano Ag-MWNTs nanocomposite modified glassy carbon (GC) electrode was used to investigate the electrochemical reduction of hydrogen peroxide. The results showed that NiNP and nano Ag-MWNTs provided the synergistic effect toward this process. The obtained NiNP/nano Ag-MWNTs/GC electrode showed a wide linear response range of 1 × 10−6 to 1 × 10−4 and 5 × 10−4 to 0.01 M hydrogen peroxide with correlation coefficients of 0.998 and 0.997, fast response time (2 s), and good selectivity toward the electrocatalytic reduction of hydrogen peroxide. The detection limit (S/N = 3) of hydrogen peroxide was 5 × 10−7 M.

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Authors and Affiliations

  1. Department of Chemistry and Chemical Engineering, Jining University, Qufu, 273155, P.R. China

    Xiurong Zhai

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  1. Xiurong Zhai
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Zhai, X. Nickel hexacyanoferrate nanoparticles/nano silver coated multiwalled carbon nanotubes nanocomposite for the detection of hydrogen peroxide. J Anal Chem 68, 307–312 (2013). https://doi.org/10.1134/S1061934813040126

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  • DOI: https://doi.org/10.1134/S1061934813040126

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