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A device for the preliminary separation of ions for mass spectrometry analysis

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Abstract

A device for the preliminary separation of ions based on an ion mobility increment spectrometer with cylindrical geometry of its electrodes is described. The device is operated in tandem with an atmospheric-pressure ionization mass spectrometer. The use of the spectrometer in the preliminary separation of ions of the target substance from ions of the chemical noise is illustrated by investigating the vapor above a water solution of acrylamide (CH2=CH-CO-NH2) with a concentration of 1.4 × 10−5 mol/L. The resolution of the device is rather low, R ∼ 10–20; nevertheless, thanks to its simplicity and availability, the device may find application to routine chemical analysis and in portable instruments.

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Authors and Affiliations

  1. Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, pr. Akademika Lavrent’eva 3, Novosibirsk, 630090, Russia

    Yu. N. Kolomiets, V. V. Pervukhin & D. G. Sheven

Authors
  1. Yu. N. Kolomiets
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  2. V. V. Pervukhin
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  3. D. G. Sheven
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Corresponding author

Correspondence to V. V. Pervukhin.

Additional information

Original Russian Text © Yu.N. Kolomiets, V.V. Pervukhin, D.G. Sheven, 2012, published in Pribory i Tekhnika Eksperimenta, 2012, No. 2, pp. 104–107.

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Kolomiets, Y.N., Pervukhin, V.V. & Sheven, D.G. A device for the preliminary separation of ions for mass spectrometry analysis. Instrum Exp Tech 55, 244–247 (2012). https://doi.org/10.1134/S0020441212010290

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  • DOI: https://doi.org/10.1134/S0020441212010290

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