Abstract
Nanosized slightly agglomerated powders of neodymium-activated yttrium aluminum garnet (YAG:Nd) were obtained by a self-propagating high-temperature synthesis method. An increase in content of reducing substituents in metal-organic complexes as compared to oxidizing substituents leads to an increase in average size of the forming grains from 23 to 70 nm; thereupon, a decrease in powder agglomeration degree is observed. Firing of x-ray amorphous powders results in formation of polycrystalline YAG:Nd without forming intermediate phases.
Similar content being viewed by others
References
Li, J.I., Ikegami, T., Lee, J.H., and Mori, T., Low-Temperature Fabrication of Transparent Yttrium Aluminum Garnet (YAG) Ceramics Without Additives, J. Am. Ceram. Soc., 2000, vol. 83, no. 4, pp. 961–963.
Sim, S.-M., Keller, K.A., and Mah, T.-I., Phase Formation in Yttrium Aluminum Garnet Powders Synthesized by Chemical Methods, J. Mater. Sci., 2000, vol. 35, no. 3, pp. 713–717.
Li, J., et al., Nanostructured YAG:Nd Powders Via Gel Combustion: The Influence of Citrate-To-Nitrate Ratio, Ceram. Int., 2008, no. 34, pp. 141–149.
Liu, Y. and Gao, L., Low-Temperature Synthesis of Nanocrystalline Yttrium Aluminum Garnet Powder Using Triethanolamine, J. Am. Ceram. Soc., 2003, vol. 86, no. 10, pp. 1651–1653.
Kakade, M.B., Ramanathan, S., and Ravindran, P.V., Yttrium Aluminum Garnet Powders by Nitrate Decomposition and Nitrate-Urea Solution Combustion Reactions a Comparative Study, J. Alloys Compd., 2003, no. 350, pp. 123–129.
Drobotenko, V.V., RF Patent No. 2118402, Byull. Izobret., No. 24 (1998).
Drobotenko, V.V., Balabanov, S.S., and Storozheva, T.I., Poluchenie gomo- i geterometallicheskikh biyadernykh kompleksov kak prekursorov dlya sozdaniya oksidnykh materialov, Vestn. Nizhegorodskogo Gos. Un-Ta Im. N.I. Lobachevskogo, 2007, no. 6, pp. 72–76.
Veitch, C.D., Synthesis of Polycrystalline Yttrium Iron Garnet and Yttrium Aluminium Garnet from Organic Precursors, J. Mater. Sci., 1991, no. 26, pp. 6527–6532.
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text © S.S. Balabanov, E.M. Gavrishchuk, V.V. Drobotenko, A.M. Kut’in, V.S. Polyakov, T.I. Storozheva, 2009, published in Neorganicheskie Materialy, 2009, Vol. 45, No. 2, pp. 194–198.
Rights and permissions
About this article
Cite this article
Balabanov, S.S., Gavrishchuk, E.M., Drobotenko, V.V. et al. Obtaining nanodisperse powders of neodymium-activated yttrium aluminum garnet by self-propagating high-temperature synthesis method. Inorg Mater 45, 157–161 (2009). https://doi.org/10.1134/S0020168509020095
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S0020168509020095