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Stereoselective Methods for the Synthesis of 4-Benzoyl-1-benzoylamino-3-(2-chlorophenyl)-2-cyano-1-methylthio-1-butene and Its Structure

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Abstract

Selective methods were developed for the synthesis of 4-benzoyl-1-benzoylamino-3-(2-chlorophenyl)-2-cyano-1-methylthio-1-butene on the basis of the reaction of N-methylmorpholinium and piperidinium 5-benzoyl-4-(2-chlorophenyl)-3-cyano-6-hydroxy-6-phenyl-1,4,5,6-tetrahydropyridine-2-thiolates with methyl iodide. The structure of the product was established by X-ray crystallographic analysis.

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Authors and Affiliations

  1. East-Ukraine State University, Lugansk, 91034, Ukraine

    S. G. Krivokolysko

  2. Institute of Organic Chemistry, National Academy of Sciences of Ukraine, Kiev, 02094, Ukraine

    E. B. Rusanov

  3. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, 117913, Russia

    V. P. Litvinov

Authors
  1. S. G. Krivokolysko
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  2. E. B. Rusanov
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  3. V. P. Litvinov
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Krivokolysko, S.G., Rusanov, E.B. & Litvinov, V.P. Stereoselective Methods for the Synthesis of 4-Benzoyl-1-benzoylamino-3-(2-chlorophenyl)-2-cyano-1-methylthio-1-butene and Its Structure. Chemistry of Heterocyclic Compounds 38, 1205–1209 (2002). https://doi.org/10.1023/A:1021729513180

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  • DOI: https://doi.org/10.1023/A:1021729513180

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