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Cyanoacetylene and Its Derivatives: XXVII. 5,5-Dialkyl-4-azido-2,5-dihydrofuran-2-imine

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Abstract

The reaction of 3-azido-4-hydroxy-2-alkynenitriles with hydrogen chloride is accompanied by intramolecular ring closure with formation of 5,5-dialkyl-4-azido-2,5-dihydrofuran-2-imine hydrochlorides which can be converted into the corresponding free bases by the action of potassium carbonate in ethanol.

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Authors and Affiliations

  1. Siberian Division, Russian Academy of Sciences, Irkutsk Institute of Chemistry, ul. Favorskogo 1, Irkutsk, 664033, Russia

    A. G. Mal'kina, R. N. Kudyakova & B. A. Trofimov

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  1. A. G. Mal'kina
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  2. R. N. Kudyakova
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  3. B. A. Trofimov
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Mal'kina, A.G., Kudyakova, R.N. & Trofimov, B.A. Cyanoacetylene and Its Derivatives: XXVII. 5,5-Dialkyl-4-azido-2,5-dihydrofuran-2-imine. Russian Journal of Organic Chemistry 37, 700–703 (2001). https://doi.org/10.1023/A:1012456002746

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  • DOI: https://doi.org/10.1023/A:1012456002746

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