Abstract
The separation ability of surface layers of nickel dimethylglyoximate and acetylacetonate bonded to Silochrom S-80 silica gel was studied. The selectivity of separation was estimated for different classes of organic compounds. It was demonstrated that the studied sorbents are promising for the separation of complex mixtures of high-boiling aromatic compounds and oxygen-containing compounds.
Similar content being viewed by others
REFERENCES
Wasiak, W., J. Chromatogr., 1993, vol. 653, p. 63.
Wasiak, W. and Rykowska, I., Anal. Chim. Acta, 1999, vol. 378, p. 101.
Khuhawar, M.Y., Memon, A.A., and Bhanger, M.I., J. Chromatogr., 1996, vol. 723, p. 313.
Slizhov, Yu.G., Berezkin, V.G., Gavrilenko, M.A., et al., Izv. Vyssh. Uchebn. Zaved., Khim. Khim. Tekhnol., 1999, vol. 42, no. 5, p. 72.
Slizhov, Yu.G., Gavrilenko, M.A., Arkhipova, I.M., and Kuryaeva, T.T., in Khimiki TGU na poroge tret'ego tysyacheletiya: Voprosy khimii i khimicheskogo materialovedeniya (Chemists of Tomsk State University on the Threshold of the Third Millennium: Problems of Chemistry and Chemical Material Science), Tomsk: Tomsk State University, 1998, p. 131.
Grushka, E., Bonded Stationary Phases in Chromatography, Science, 1974.
Sorbenty na osnove silikagelya v radiokhimii (Sorbents Based on Silica Gel in Radiochemistry), Laskorin, B.M., Ed., Moscow: Atomizdat, 1977.
Wasiak, W., J. Chromatogr., 1995, vol. 690, p. 93.
Nawrocki, J. and Buszewski, B., J. Chromatogr., 1988, vol. 449, p. 1.
Modifitsirovannye kremnezemy v sorbtsii, katalize i khromatografii (Modified Silica in Sorption, Catalysis, and Chromatography), Lisichkin, G.V, Ed., Moscow: Khimiya, 1986.
Pomogailo, A.D. and Ufland, E.I., Zh. Vses. Khim. Obshch. Im. Mendeleeva, 1995, vol. 40, nos. 4-5, p. 55.
Stary, I, The Solvent Extraction of Metal Chelates, Oxford: Pergamon, 1964. Translated under the title Ekstraktsiya khelatov, Moscow: Mir, 1966.
Slizhov, Yu.G., Gavrilenko, M.A., and Borbolin, A.A., Zh. Fiz. Khim., 1999, vol. 73, no. 11, p. 2032.
Gregg, S.J. and Sing, K.S.W., Adsorption, Surface Area, and Porosity, New York: Academic, 1982. Translated under the title Adsorbtsiya, udel'naya poverkhnost', poristost', Moscow: Mir, 1984.
Aivazov, B.V., Praktikum po khimii poverkhnostnykh yavlenii i sorbtsii (Laboratory Manual on Chemistry of Surface Effects and Sorption), Moscow: Vysshaya Shkola, 1973.
Lukas, J., J. Chromatogr., 1980, vol. 190, p. 13.
Vigdergauz, M.S., Raschety v gazovoi khromatografii (Calculations in Gas Chromatography), Moscow: Khimiya, 1978.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Slizhov, Y.G., Gavrilenko, M.A. Gas-Chromatographic Properties of Silochrom with a Surface Layer of Nickel Dimethylglyoximate and Acetylacetonate Complexes. Journal of Analytical Chemistry 56, 538–541 (2001). https://doi.org/10.1023/A:1016628610463
Issue Date:
DOI: https://doi.org/10.1023/A:1016628610463