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Metal–Organic Framework-Derived Hierarchical Cu9S5/C Nanocomposite Fibers for Enhanced Electromagnetic Wave Absorption

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Abstract

Refining the electromagnetic wave absorption characteristics of traditional metal–organic framework (MOF)-derived carbon composites remains a challenge because of their discontinuous conductive path. To overcome this limitation, in this work, MOF-derived hierarchical Cu9S5/C nanocomposite fibers are fabricated by electrospinning and subsequent carbonization-sulfurization process. Morphological analyses show that MOF-derived octahedral Cu9S5/C particles are evenly monodispersed inside carbonaceous fibers. This configuration creates a unique hierarchical structure, ranging from Cu9S5 particle embedding, MOF-derived skeleton, to a three-dimensional network. The optimized composite fibers (Cu9S5/C-40) exhibit extraordinary electromagnetic wave absorption performance at a low mass fraction (20 wt%): the minimum reflection loss value reaches − 69.6 dB, and the maximum effective absorption bandwidth achieves 5.81 GHz with an extremely thin thickness of only 1.83 mm. Systematic investigations demonstrate that constructing the three-dimensional conductive network to connect MOF derivatives is crucial for activating performance enhancement. The unique nano-micro hierarchical structure synergized with elaborate-configured components endows the materials with optimal impedance matching and amplifies the loss capacity of each part. This work provides a reliable example and theoretical guidance for fabricating new-generation high-efficiency MOF-derived fibrous electromagnetic wave absorbers.

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Acknowledgements

This work was supported by the Natural Science Foundation of Shandong Province (ZR2021ME194, 2022TSGC2448, 2023TSGC0545), and the key research and development program of Shandong Province(2021ZLGX01).

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Authors and Affiliations

  1. Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials Ministry of Education, Shandong University, Jinan, 250061, People’s Republic of China

    Simeng Wu, Chengjuan Wang, Yunxiang Tang, Jiangyiming Jiang, Haotian Jiang, Xiaodan Xu, Bowen Cui, Yanyan Jiang & Yanxiang Wang

  2. Carbon Fiber Engineering Research Center, School of Materials Science and Engineering, Shandong University, Jinan, 250061, People’s Republic of China

    Simeng Wu, Chengjuan Wang, Haotian Jiang, Xiaodan Xu, Bowen Cui & Yanxiang Wang

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  1. Simeng Wu
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Wu, S., Wang, C., Tang, Y. et al. Metal–Organic Framework-Derived Hierarchical Cu9S5/C Nanocomposite Fibers for Enhanced Electromagnetic Wave Absorption. Adv. Fiber Mater. 6, 430–443 (2024). https://doi.org/10.1007/s42765-023-00362-9

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