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Effect of Temperature on Thermal Treatment of Silica Coated Magnetic Nanoparticles

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Abstract

In the quest for developing a catalyst with as many desired characteristics, a facile synthetic route was designed for the preparation of mesoporous silica coated magnetic nanoparticles(MSMNP) employing a colloid mill reactor. The composite particles were characterized by the techniques, such as nitrogen adsorption-desorption isotherms, scanning electron microscopy(SEM), transmission electron microscopy(TEM), X-ray diffraction patterns (XRD), thermo-gravimetric analysis(TGA), Fourier transform infrared spectroscopy(FTIR) and vibrating sample magnetometer(VSM), etc. The analysis showed that the resulted MSMNP composites were composed of silica shell layers with open pores connecting channels and NiFe2O4 with spinel structure, so the thermal treatment temperature did not show significant effect on pore textural properties, and its specific surface areas were in the range of 443–474 m2/g, while pore volume of about 0.8 cm3/g with an average pore size of around 9.5 nm. The composites with super paramagnetic nature were encapsulated entirely with amorphous silica layers contributing to optimum porosity and abundant surface hydroxyl groups.

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References

  1. Polshettiwar V., Luque R., Fihri A., Zhu H. B., Bouhrara M., Bas-set J. M., Chem. Rev. 2011 111, 3036

    Article  CAS  PubMed  Google Scholar 

  2. Gawande M. B., Monga Y., Zboril R., Sharma R. K., Coordin. Chem. Rev., 2015 288, 118

    Article  CAS  Google Scholar 

  3. Nie J., He B., Cheng Y. M., Yin W., Hou C. J., Hou D. Q., Qian L. L., Qin Y. A., Fa H. B., Chem. Res. Chinese Universities, 2017 33(6), 951

    Article  CAS  Google Scholar 

  4. Chng L. L., Erathodiyil N., Ying J. Y., Acc. Chem. Res. 2013 46, 1825

    Article  CAS  PubMed  Google Scholar 

  5. Neyts E. C., Ostrikov K., Sunkara M. K., Bogaerts A., Chem. Rev., 2015 115, 13408

    Article  CAS  PubMed  Google Scholar 

  6. Sharma R. K., Yadav M., Monga Y., Gaur R., Adholeya A., Zboril R., Varma R. S., Gawande M. B., ACS Sustain. Chem. Eng., 2016 4, 1123

    Article  CAS  Google Scholar 

  7. Gill C. S., Price B. A., Jones C. W., J. Catalysis, 2007 251, 145

    Article  CAS  Google Scholar 

  8. Stoeber W., Fink A., Bohn E., J. Colloid Interf. Sci., 1968 26, 62

    Article  CAS  Google Scholar 

  9. Montañopriede J. L., Coelho J. P., Guerreromartínez A., Rodríguez O. P., Pal U., J. Phys. Chem. C, 2017 121, 9543

    Article  CAS  Google Scholar 

  10. Ow H., Larson D. R., Srivastava M., Baird B. A., Webb W. W., Wiesner U., Nano Lett., 2005 5, 113

    Article  CAS  PubMed  Google Scholar 

  11. Yu S. Y., Zhang H. J., Yu J. B., Wang C., Sun L. N., Shi W. D., Langmuir, 2007 3, 7836

    Article  CAS  Google Scholar 

  12. Christy R., Vestal Z., Zhang J., Nano Lett., 2003 3, 1739

    Article  CAS  Google Scholar 

  13. Leng Y. H., Sato K., Shi Y. G., Li J. G., Ishigaki T., Yoshida T., Kamiya H., J. Phys. Chem. C, 2009 113, 16681

    Article  CAS  Google Scholar 

  14. Christy R., Vestal Z., Zhang J., Nano Lett., 2003 3, 1739

    Article  CAS  Google Scholar 

  15. Qu H., Tong S., Song K. J., Ma H., Bao G., Pincus S., Zhou W. L., Connor C., Langmuir, 2013 29, 10573

    Article  CAS  PubMed  PubMed Central  Google Scholar 

  16. Zhao W. R., Gu J. L., Zhang L. X., Chen H. R., Shi J. L., J. Am. Chem. Soc., 2005 127, 8916

    Article  CAS  PubMed  Google Scholar 

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Authors and Affiliations

  1. National Demonstration Center for Experimental Chemical Engineering Comprehensive Education, School of Chemical Engineering and Technology, North University of China, Taiyuan, 030051, P. R. China

    Yu Li, Penghong Zhang, Huipeng Zhao, Xiaoqiang Du, Junping Li & Laishuan Liu

Authors
  1. Yu Li
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  2. Penghong Zhang
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  3. Huipeng Zhao
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  4. Xiaoqiang Du
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  5. Junping Li
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  6. Laishuan Liu
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Corresponding author

Correspondence to Yu Li.

Additional information

Supported by the Major Program of Science and Technology of Shanxi Province, China(No.20111101013).

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Li, Y., Zhang, P., Zhao, H. et al. Effect of Temperature on Thermal Treatment of Silica Coated Magnetic Nanoparticles. Chem. Res. Chin. Univ. 34, 857–861 (2018). https://doi.org/10.1007/s40242-018-7431-8

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  • DOI: https://doi.org/10.1007/s40242-018-7431-8

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