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Green Synthesis of Zinc Oxide Nanoparticles Using Leaves Extract of Mariposa Christia vespertilionis and its Potential as Anode Materials in Sodium-Ion Batteries (SIBs)

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Abstract

Zinc oxide nanoparticles (ZnO-NPs) is one of the promising material as anode in sodium ion batteries (SIBs). However, due to the large mass and radius of Na-ions, designing electrode materials with high cycling efficiency remains a challenge. One of the attributions is from morphology of ZnO-NPs which can be altered during synthesis process. This study employs Mariposa Christia vespertilionis (MCV) leaves extract to produce ZnO-NP using green synthesis route. This method is safe and cost effective alternative to replace the common chemical methods. Phytochemical test of MCV contains phenols, flavonoids and alkaloids. The formation of ZnO-NPs after calcination at 700, 800 and 900 °C was confirmed via X-ray diffraction and Fourier-transforms infrared spectroscopy analysis. Scanning electron microscope images how irregular shape and agglomerated ZnO-NPs. The average particle sizes of ZnO-NPs range from 38 to 65 nm obtained from high-resolution transmission electron microscope. Nitrogen gas adsorption analysis revealed the pore size and pore volume decreased with the increasing calcination temperatures. The ZnO-NPs calcined at 700 °C exhibits the highest initial discharge capacity of 591 mAh g−1 at 0.1 C up to 100 cycles and better rate capability and could be further exploited as anode materials in SIBs.

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Acknowledgements

The authors would like to thank the research fund University Malaysia Terengganu (UMT), Talent and Publication Enhancement Research Grant (TAPE-RG Vot: 55259), Faculty of Science and Marine Environment, and Institute of Marine Biotechnology for the facilities provided throughout this study. The authors would also like to thank the Centre for Functional Materials and Nanotechnology, Institute of Science, Universiti Teknologi MARA, Shah Alam, Malaysia for their support in completing this work.

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Authors and Affiliations

  1. Faculty of Science and Marine Environment, Universiti Malaysia Terengganu, 21030, Kuala Nerus, Terengganu, Malaysia

    Nurul Atikah Idris, Hanis Mohd Yusoff, Nurhanna Badar & Chia Poh Wai

  2. Advance Nano Materials (AnoMa) Research Group, Faculty of Science and Marine Environment, Universiti Malaysia Terengganu, 21030, Kuala Nerus, Terengganu, Malaysia

    Hanis Mohd Yusoff & Nurhanna Badar

  3. Energy Storage Research Group, Faculty of Ocean Engineering Technology and Informatics, Universiti Malaysia Terengganu, 21030, Kuala Nerus, Terengganu, Malaysia

    Nurul Hayati Idris, Sarah Umeera Muhamad & Nor Fazila Mahamad Yusoff

  4. Centre for Functional Materials and Nanotechnology, Institute of Science, Universiti Teknologi MARA, 40450, Shah Alam, Malaysia

    Kelimah Elong

  5. School of Chemistry and Environment, Faculty of Applied Sciences, Universiti Teknologi MARA, 40450, Shah Alam, Malaysia

    Kelimah Elong

Authors
  1. Nurul Atikah Idris
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  2. Hanis Mohd Yusoff
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  3. Nurul Hayati Idris
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  4. Nurhanna Badar
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  5. Kelimah Elong
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  6. Sarah Umeera Muhamad
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  7. Nor Fazila Mahamad Yusoff
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  8. Chia Poh Wai
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Corresponding author

Correspondence to Hanis Mohd Yusoff.

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Idris, N.A., Yusoff, H.M., Idris, N.H. et al. Green Synthesis of Zinc Oxide Nanoparticles Using Leaves Extract of Mariposa Christia vespertilionis and its Potential as Anode Materials in Sodium-Ion Batteries (SIBs). Arab J Sci Eng 49, 623–635 (2024). https://doi.org/10.1007/s13369-023-08300-y

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