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EBSD Evaluation of Al- TiAl3 Composites Manufactured Through CRB-Annealing-ARB and CRB-ARB-Annealing Methods

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Abstract

In this study, Al-TiAl3 nanocomposites were produced by applying annealing treatment (AT) before and after the accumulative roll bonding (ARB). First, the sandwich of two Al sheets containing pure Ti powder was subjected to cold roll bonding (CRB) and then underwent AT-ARB and ARB-AT processes. Annealing conditions were used to form the intermetallic compound at 590 °C for 2 h, and the ARB process was performed for a maximum of five cycles. The chemical and microstructural revolutions were evaluated using field emission scanning electron microscopy (FESEM) equipped with an elemental analyzer (EDS) and electron backscatter diffraction (EBSD) analysis. The results showed that through annealing after CRB, TiAl3 intermetallic compound was formed in the Al matrix, and then, the obtained Al-TiAl3 composite was subjected to the ARB process. Finally, a composite containing a uniform distribution of TiAl3 particles of larger than 200 nm in the Al matrix was obtained. Microstructural changes showed that with an increase in strain due to the development of continuous recrystallization, a structure containing grains smaller than 500 nm was obtained. The microstructural evaluation of the ARB-AT composite showed that the grain size of Al and particle size of TiAl3, in this case, were in micrometer and larger.

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Authors and Affiliations

  1. Department of Materials Engineering, Isfahan University of Technology, 84156-83111, Isfahan, Iran

    Zohreh Yazdani, Mohammad Reza Toroghinejad & Hossein Edris

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  1. Zohreh Yazdani
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  2. Mohammad Reza Toroghinejad
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Correspondence to Zohreh Yazdani.

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Mohammad Reza Toroghinejad and Hossein Edris are Co-authors.

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Yazdani, Z., Toroghinejad, M.R. & Edris, H. EBSD Evaluation of Al- TiAl3 Composites Manufactured Through CRB-Annealing-ARB and CRB-ARB-Annealing Methods. Trans Indian Inst Met 75, 113–131 (2022). https://doi.org/10.1007/s12666-021-02408-1

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