Abstract
In this study, the formation of the silicon coating on the AISI D2 steel with the pack siliconizing method has been investigated. To do so, different times (2, 3, 4 h) and temperatures (650, 800, 950 °C) for heat treating, and Si (8, 10 and 12 wt%) with the same percentage of NH4Cl and NaF (0.5 + 0.5 wt%), and balances Al2O3 halide activator were used. For characterization of coating, SEM (thickness, EDX), XRD, and micro-hardness were used. Based on the experimental results, by increasing time, temperature, and silicon percentage, thickness of the coating, and micro-hardness and percentage of the silicon with the EDX are increased. To run optimization, a Central Composite design, CCD, was used to find the best combination of parameters. Eventually, the optimal combination of parameters was introduced then verified. According to optimization, 4 h holing time, 11.744 Si percentage and 950 degree Celsius are the best combination of process parameters.
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Kumar A, Kaur M, Singh S, Joseph A, Jhala G, Bhandari S (2018) High-temperature tribological studies of plasma-nitrided tool steels. Surf Eng 34(8):620–633
Gobbi SJ, Gobbi VJ, Reinke G, Muterlle PV, Rosa DM (2019) Ultra-low-temperature process effects on microscale abrasion of tool steel AISI D2. Mater Sci Technol 35(11):1355–1364
A.M. Khan, M. Jamil, A. Ul Haq, S. Hussain, L. Meng, and N. He, Sustainable machining. Modeling and optimization of temperature and surface roughness in the milling of AISI D2 steel, Ind Lubr Tribol, 2019, 71(2), p 267–277
Bombač D, Terčelj M, Kugler G, Peruš I (2018) Amelioration of surface cracking during hot rolling of AISI D2 tool steel. Mater Sci Technol 34(14):1723–1736
Yapici A, Aydin SE, Koc V, Kanca E, Yildiz M (2019) Wear behavior of Borided AISI D2 steel under linear reciprocating sliding conditions. Prot Met Phys Chem Surf 55(2):341–351
Sadeghi B, Shamanian M, Ashrafizadeh F, Cavaliere P, Rizzo A (2018) Wear behavior of Al-based Nanocomposites reinforced with bimodal micro- and Nano-sized Al2O3 particles produced by spark plasma sintering. Mater Perf Charact 7(1):327–350
Keddam M, Kulka M (2018) Simulation of the growth kinetics of FeB and Fe2B layers on AISI D2 steel by the integral method. Phys Met Metallogr 119(9):842–851
Xiang J, Xie F, Wu X, Yu Y (2019) Microstructure and tribological properties of Si-Y/Al two-step deposition coating prepared on Ti2AlNb based alloy by halide activated pack cementation technique. Tribol Int 136:45–57
Tian J, Yu WH, Tian W, Zhao J, Li YQ, Liu YZ (2015) Effects of Y-Ce on wear behaviours of silicide coatings. Surf Eng 31(4):289–294
Lu XJ, Xiang ZD (2017) A novel single-step surface-treatment process for forming Cr-nitride coatings on steels. Met Trans A48:580–583
Sun J, Li T, Zhang G-P, Fu Q-G (2019) Different oxidation protection mechanisms of HAPC silicide coating on niobium alloy over a large temperature range. J Alloys Compd 790:1014–1022
Byeong WL (2018) Effect of diffusion coatings on the high temperature properties of nickel-chromium-superalloys. Int J Mod Phys B 32:1840056
Chaia N, Portebois L, Mathieu S, David N, Vilasi M (2017) On the interdiffusion in multilayered silicide coatings for the vanadium-based alloy V-4Cr-4Ti. J Nucl Mater 484:148–156
Li X, Hu G, Tian J, Tian W, Xie W, Li X (2018) Wear resistance enhancement of Ti-6Al-4V alloy by applying Zr-modified silicide coatings. J Mater Eng Perform 27:1073–1082
Xue J, Tao G, Tang C, Xu N, Li F, Yin C (2020) Effect of siliconizing with molten salt on the wear resistance and corrosion resistance of AISI 302 stainless steel. Surf Coat Technol 382:125217
Tang C-b, Wen F-r, Chen H-x, Liu J-j, Tao G-y, Xu N-j, Xue J-q (2019) Corrosion characteristics of Fe3Si intermetallic coatings prepared by molten salt infiltration in sulfuric acid solution. J Alloys Compd 778:972–981
Semboshi S, Kimura S, Iwase A, Ohtsu N (2014) Surface hardening of age-hardenable cu–Ti dilute alloys by plasma nitriding. Surf Coat Technol 258:691–698
Ikeda J, Semboshi S, Iwase A, Gao W, Sugawara A (2015) Precipitation behavior and properties of cu-Ti alloys with added nitrogen. Metall Mater Trans 56(3):297–302
Ueyama D, Semboshi S, Saitoh Y, Ishikawa N, Nishida K, Soneda N, Hori F, Iwase A (2014) Hardening induced by energetic electron beam for Cu–Ti alloys, Japan. J Appl Phys 53(5S1):05FC04
Perepezko JH, Sossaman TA, Taylor M (2017) Environmentally resistant Mo-Si-B-based coatings. J Therm Spray Technol 26(5):929–940
Hosseinzadeh M, Mouziraji MG (2016) An analysis of tube drawing process used to produce squared sections from round tubes through FE simulation and response surface methodology. Int J Adv Manuf Technol 87(5–8):2179–2194
Ghasempour-Mouziraji M, Ghorbani-Menghari H, Hosseinzade M, Karami JS, Wei D (2018). Enhancing mechanical property of Al7075 by using elliptical cross-sectioned spiral Equal-Channel extrusion: experimental, numerical and optimization approach. Int J Adv Technol 9(205)
Naghibi HD, Shakeri M, Hosseinzadeh M (2016) Neural network and genetic algorithm based modeling and optimization of tensile properties in FSW of AA 5052 to AISI 304 dissimilar joints. Trans Indian Inst Metals 69(4):891–900
Jafari M, Lotfi M, Ghaseminejad P, Roodi M, Teimouri R (2015) Numerical control and optimization of springback in L-bending of magnesium alloy through FE analysis and artificial intelligence. Trans Indian Inst Metals 68(5):969–979
Design-Expert software v8 user’s guide. Technical manual. Minneapolis (MN): Stat-Ease Inc.; 2010
Li X, Guo X, Qiao Y (2016) Friction and wear behaviors of Nb-Ti-Si-Cr based ultrahigh temperature alloy and its Zr-Y jointly modified silicide coatings. Trans Nonferrous Met Soc China 26:1892–1901
Tian J, Yu W-H, Tian W, Zhao J, Li Y-Q, Liu Y-Z (2015) Effects of Y–Ce on wear behaviours of silicide coatings. Surf Eng 31(4):289–294
Xiao J, Huang Y, Zhou Q, Wang J, He X (2019) Room temperature nanoindentation creep of nitrocarburised AISI 4140 steel. Surf Eng 35(8):719–727
Fazel ZA, Elmkhah H, Nouri M, Fattah-alhosseini A (2019) Effect of compound layer on the corrosion behavior of plasma nitrided AISI H13 tool steel. Mater Res Expr 6(5):056412
Ebrahimzadeh I, Ashrafizadeh F (2014) High temperature wear and frictional properties of duplex-treated tool steel sliding against a two phase brass. Ceram Int 40(10):16429–16439
Haftlang F, Habibolahzadeh A, Heydarzadeh Sohi M (2014) Duplex treatment of AISI 1045 steel by plasma nitriding and aluminizing. Vacuum 107:155–158
Mouri L, Mabille I, Fiaud C, Amouroux J, Catillon G, Gras R (2001) Study of corrosion resistance and surface properties of carbon steel after a duplex plasma treatment. Thin Solid Films 389(1):153–160
Asempah I, Xu J, Yu L, Ju H, Wu F, Luo H (2019) Microstructure, mechanical and tribological properties of magnetron sputtered Ti-B-N films. Surf Eng 35(8):701–709
Stathokostopoulos D, Chaliampalias D, Pliatsikas N, Kassavetis S, Pavlidou E, Patsalas P, Logothetidis S, Chrissafis K, Vourlias G (2018) Ti and nitride surface modification of copper by pack cementation. Surf Eng 34(3):243–250
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Najafizadeh, M., Ghasempour-Mouziraji, M. Multi-Objective Optimization of Process Parameters in Pack Siliconizing on AISI D2 Steel. Silicon 13, 2233–2242 (2021). https://doi.org/10.1007/s12633-020-00735-4
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DOI: https://doi.org/10.1007/s12633-020-00735-4