The process of formation of surface layer on steel AISI D2 pack siliconized at 650, 800 and 950°C for 2, 3, and 4 h using a powder mixture (in wt.%) of 0.5, 0.75, 1.0 NH4Cl + 12 Si, the remainder Al2O3 is studied. The siliconized layer is analyzed by x-ray diffractometry and electron microscopy, and its microhardness is measured. It is shown that the thickness and the microhardness of the coating increase with the temperature and the treatment time and with the content of the halide activator. The response surface methodology based on the Box–Behnken method is used to optimize the siliconizing process for steel AISI D2.
Similar content being viewed by others
Notes
Here and below in the article the content of the elements is given in wt.%.
References
W. H. Wills, “Practical observations on high-carbon high-chromium tool steels,” Trans. ASM, 23, 469 – 476 (1935).
S. J. Gobbi, V. J. Gobbi, G. Reinke, et al., “Ultra-low-temperature process effects on microscale abrasion of tool steel AISI D2,” Mater. Sci. Technol., 35(11), 1355 – 1364 (2019).
A. M. Khan, M. Jamil, A. Ul Haq, et al., “Sustainable machining. Modeling and optimization of temperature and surface roughness in the milling of AISI D2 steel,” Ind. Lubr. Tribol., 71(2), 267 – 277 (2019).
D. Bombaè, M. Terèelj, G. Kugler, and I. Peruš, “Amelioration of surface cracking during hot rolling of AISI D2 tool steel,” Mater. Sci. Technol., 34(14), 1723 – 1736 (2018).
Y. Sun, J. Dong, P. Zhao, and B. Dou, “Formation and phase transformation of aluminide coating prepared by low-temperature aluminizing process,” Surf. Coat. Technol., 330, 234 – 240 (2017).
H.-L. Kim, I.-S. Park, S.-J. Lee, et al., “Effect of surface pretreatment and pack cementation on bioactivity of titanium dental implant,” Surf. Coat. Technol. B, 259, 178 – 184 (2014).
P. Juzoñ, M. Ziemnicka, S. Chevalier et al., “Improving Fe3Al alloy resistance against high temperature oxidation by pack cementation process,” Appl. Surf. Sci., 253(11), 4928 – 4934 (2007).
J. Xiang, F. Xie, X. Wu, and Y. Yu, “Microstructure and tribological properties of Si-Y_Al two-step deposition coating prepared on Ti2 AlNb based alloy by halide activated pack cementation technique,” Tribol. Int., 136, 45 – 57 (2019).
S. A. Tsipas and E. Gordo, Molybdeno-aluminizing of powder metallurgy and wrought Ti and Ti – 6Al – 4V alloys by pack cementation process,” Mater. Charact., 118, 494 – 504 (2016).
F. Bozza, G. Bolelli, C. Giolli, et al., “Diffusion mechanisms and microstructure development in pack aluminizing of Ni-based alloys,” Surf. Coat. Technol., 239, 147 – 159 (2014).
Z. D. Xiang and P. K. Datta, “Pack aluminisation of low alloy steels at temperatures below 700 °C,” Surf. Coat. Technol., 184(1), 108 – 115 (2004).
Hosseinzadeh, Morteza and Mehran Ghasempour Mouziraji, “An analysis of tube drawing process used to produce squared sections from round tubes through FE simulation and response surface methodology,” Int. J. Adv. Manuf. Technol., 87(5–8), 2179 – 2194 (2016).
Mehdi Salehi, Morteza Hosseinzadeh, and Majid Elyasi, “A study on optimal design of process parameters in tube drawing process of rectangular parts by combining Box–Behnken design of experiment, response surface methodology and artificial bee colony algorithm,” Trans. Indian Inst. Met., 69(6), 1223 – 1235 (2016).
Mirshaban Jafari, Morteza Hosseinzadeh, and Majid Elyasi, “Optimization of tube drawing process through FE analysis, intelligent computation, and experimental verification,” Proc. Inst. Mech. Eng. E, J. Proc. Mech. Eng., 232(1), 94 – 107 (2018).
H. Ghorbani, J. H. Kim, M. Hosseinzadeh, et al. “Manufacturing of bent tubes with non-uniform curvature and cross-section using a novel hydroforming die: experimental, finite element analysis, and optimization,” Int. J. Adv. Manuf. Technol., 107(3–4), 1683 – 1695 (2020).
Author information
Authors and Affiliations
Corresponding author
Additional information
Translated from Metallovedenie i Termicheskaya Obrabotka Metallov, No. 1, pp. 44 – 4, January, 2022.
Rights and permissions
Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
About this article
Cite this article
Najafizadeh, M., Ghasempour-Mouziraji, M. Effect of Pack Siliconizing on Mechanical Properties of a Tool from Steel AISI D2: Experiment and Optimization. Met Sci Heat Treat 64, 45–50 (2022). https://doi.org/10.1007/s11041-022-00757-2
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11041-022-00757-2