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Effect of Pack Siliconizing on Mechanical Properties of a Tool from Steel AISI D2: Experiment and Optimization

  • THERMOCHEMICAL TREATMENT AND COATINGS
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Metal Science and Heat Treatment Aims and scope

The process of formation of surface layer on steel AISI D2 pack siliconized at 650, 800 and 950°C for 2, 3, and 4 h using a powder mixture (in wt.%) of 0.5, 0.75, 1.0 NH4Cl + 12 Si, the remainder Al2O3 is studied. The siliconized layer is analyzed by x-ray diffractometry and electron microscopy, and its microhardness is measured. It is shown that the thickness and the microhardness of the coating increase with the temperature and the treatment time and with the content of the halide activator. The response surface methodology based on the Box–Behnken method is used to optimize the siliconizing process for steel AISI D2.

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Notes

  1. Here and below in the article the content of the elements is given in wt.%.

References

  1. W. H. Wills, “Practical observations on high-carbon high-chromium tool steels,” Trans. ASM, 23, 469 – 476 (1935).

    Google Scholar 

  2. S. J. Gobbi, V. J. Gobbi, G. Reinke, et al., “Ultra-low-temperature process effects on microscale abrasion of tool steel AISI D2,” Mater. Sci. Technol., 35(11), 1355 – 1364 (2019).

    Article  CAS  Google Scholar 

  3. A. M. Khan, M. Jamil, A. Ul Haq, et al., “Sustainable machining. Modeling and optimization of temperature and surface roughness in the milling of AISI D2 steel,” Ind. Lubr. Tribol., 71(2), 267 – 277 (2019).

    Article  Google Scholar 

  4. D. Bombaè, M. Terèelj, G. Kugler, and I. Peruš, “Amelioration of surface cracking during hot rolling of AISI D2 tool steel,” Mater. Sci. Technol., 34(14), 1723 – 1736 (2018).

    Article  Google Scholar 

  5. Y. Sun, J. Dong, P. Zhao, and B. Dou, “Formation and phase transformation of aluminide coating prepared by low-temperature aluminizing process,” Surf. Coat. Technol., 330, 234 – 240 (2017).

    Article  CAS  Google Scholar 

  6. H.-L. Kim, I.-S. Park, S.-J. Lee, et al., “Effect of surface pretreatment and pack cementation on bioactivity of titanium dental implant,” Surf. Coat. Technol. B, 259, 178 – 184 (2014).

    Article  CAS  Google Scholar 

  7. P. Juzoñ, M. Ziemnicka, S. Chevalier et al., “Improving Fe3Al alloy resistance against high temperature oxidation by pack cementation process,” Appl. Surf. Sci., 253(11), 4928 – 4934 (2007).

    Article  Google Scholar 

  8. J. Xiang, F. Xie, X. Wu, and Y. Yu, “Microstructure and tribological properties of Si-Y_Al two-step deposition coating prepared on Ti2 AlNb based alloy by halide activated pack cementation technique,” Tribol. Int., 136, 45 – 57 (2019).

    Article  CAS  Google Scholar 

  9. S. A. Tsipas and E. Gordo, Molybdeno-aluminizing of powder metallurgy and wrought Ti and Ti – 6Al – 4V alloys by pack cementation process,” Mater. Charact., 118, 494 – 504 (2016).

    Article  CAS  Google Scholar 

  10. F. Bozza, G. Bolelli, C. Giolli, et al., “Diffusion mechanisms and microstructure development in pack aluminizing of Ni-based alloys,” Surf. Coat. Technol., 239, 147 – 159 (2014).

    Article  CAS  Google Scholar 

  11. Z. D. Xiang and P. K. Datta, “Pack aluminisation of low alloy steels at temperatures below 700 °C,” Surf. Coat. Technol., 184(1), 108 – 115 (2004).

    Article  CAS  Google Scholar 

  12. Hosseinzadeh, Morteza and Mehran Ghasempour Mouziraji, “An analysis of tube drawing process used to produce squared sections from round tubes through FE simulation and response surface methodology,” Int. J. Adv. Manuf. Technol., 87(5–8), 2179 – 2194 (2016).

    Article  Google Scholar 

  13. Mehdi Salehi, Morteza Hosseinzadeh, and Majid Elyasi, “A study on optimal design of process parameters in tube drawing process of rectangular parts by combining Box–Behnken design of experiment, response surface methodology and artificial bee colony algorithm,” Trans. Indian Inst. Met., 69(6), 1223 – 1235 (2016).

    Article  CAS  Google Scholar 

  14. Mirshaban Jafari, Morteza Hosseinzadeh, and Majid Elyasi, “Optimization of tube drawing process through FE analysis, intelligent computation, and experimental verification,” Proc. Inst. Mech. Eng. E, J. Proc. Mech. Eng., 232(1), 94 – 107 (2018).

    Article  Google Scholar 

  15. H. Ghorbani, J. H. Kim, M. Hosseinzadeh, et al. “Manufacturing of bent tubes with non-uniform curvature and cross-section using a novel hydroforming die: experimental, finite element analysis, and optimization,” Int. J. Adv. Manuf. Technol., 107(3–4), 1683 – 1695 (2020).

    Article  Google Scholar 

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Correspondence to Mojtaba Najafizadeh.

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Translated from Metallovedenie i Termicheskaya Obrabotka Metallov, No. 1, pp. 44 – 4, January, 2022.

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Najafizadeh, M., Ghasempour-Mouziraji, M. Effect of Pack Siliconizing on Mechanical Properties of a Tool from Steel AISI D2: Experiment and Optimization. Met Sci Heat Treat 64, 45–50 (2022). https://doi.org/10.1007/s11041-022-00757-2

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  • DOI: https://doi.org/10.1007/s11041-022-00757-2

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