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Corrosion resistance of Cr2O3 coating formed by in-situ oxidation on 2205 duplex stainless steel in different pH solutions

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摘要

以2205双相不锈钢为基体材料, 采用原位氧化的方法制备了厚度为734 nm的Cr2O3涂层, 研究了溶液PH值对2205双相不锈钢基体和涂层样品微观形貌和耐蚀性的影响, 其中设定腐蚀环境为3 wt.% NaCl, 0.1 mol KOH和0.5 mol H2SO4溶液。采用扫描电子显微镜, 掠入射X射线衍射仪和辉光放电光谱分别对待测样品的微观结构, 相组成和深度方向元素分布进行表征。结果表明涂层沉积致密且沿深度方向均匀分布, 涂层由Cr2O3和MnCr2O4尖晶石相组成。采用电化学方法对涂层样品和基体的耐蚀性进行评价, 结果表明2205双相不锈钢基体在碱性溶液中具有较好的耐蚀性, 而对于涂层样品在酸性溶液抗腐蚀性能较好。由于涂层的存在, 在不同PH值溶液中基体和涂层样品的腐蚀机理不同, 从而导致相同PH溶液下样品的抗腐蚀性能存在较大差异。

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Acknowledgements

This work was financially supported by the Innovation Capability Support Program of Shaanxi (No. 2019TD-038 and 2020KJXX-063).

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Author notes

  1. Rui Cai, Wei-Jing Wang and Ning Zhao have contributed equally to this work.

Authors and Affiliations

  1. School of Chemical Engineering and Technology, Xi’an Jiaotong University, Xi’an, 710049, China

    Rui Cai, Hai-Jun Hu & Guang-Xu Cheng

  2. State Key Laboratory for Performance and Structure Safety of Petroleum Tubular Goods and Equipment Materials, CNPC Tubular Goods Research Institute, Xi’an, 710077, China

    Rui Cai

  3. GRIMAT Engineering Institute Co., Ltd, Beijing, 101407, China

    Wei-Jing Wang & Qing-He Yu

  4. Youke Publishing Co., Ltd, China GRINM Group Co., Ltd., Beijing, 100088, China

    Ning Zhao

  5. Petrochina Jidong Oilfield Company, Tangshan, 063004, China

    Fa-Yong Wang

  6. Shinda (Tangshan) Creative Oil & Gas Equipment Co., Ltd., Tangshan, 063000, China

    Jian-Liang Duan

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  1. Rui Cai
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Correspondence to Rui Cai, Qing-He Yu or Guang-Xu Cheng.

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Cai, R., Wang, WJ., Zhao, N. et al. Corrosion resistance of Cr2O3 coating formed by in-situ oxidation on 2205 duplex stainless steel in different pH solutions. Rare Met. 42, 2189–2196 (2023). https://doi.org/10.1007/s12598-022-02248-y

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