Skip to main content
Log in

Preparation and properties of Os–Ir–Al alloy for impregnated tungsten cathodes

  • Published:
Rare Metals Aims and scope Submit manuscript

Abstract

Os–Ir–Al alloy was fabricated by powder metallurgy technique. IrAl and OsIr interalloys were synthesized to reduce the Al evaporation and ensure the composition of the ternary alloy. Analysis on microstructures shows that each component is distributed homogeneously, and the green density reaches 94.9 %. Ba–W cathodes with Os–Ir–Al alloy magnetic sputtered on the tips are prepared and directly current density tests are carried out on these cathodes. It is found that at 1,050 °C, the average zero field emission density of the cathode reaches up to 20 A·cm−2. The improvements of cathodic current density and stability may indicate the prosperous application of Os–Ir–Al alloy on cathode.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4

Similar content being viewed by others

References

  1. Li YT, Zhang HL, Liu PK, Zhang MC. A new dispenser cathode with dual-layer. Appl Surf Sci. 2005;251(1–4):126.

    Article  Google Scholar 

  2. Hill PJ, Cornish LA, Witcomb MJ. Constitution and hardness of the Ir–Al system. J Alloy Compd. 1998;280(1–4):240.

    Article  Google Scholar 

  3. Ode M, Abe T, Murakami H, Yamabe-Mitarai Y, Hara T, Nagashio K, Kocer C, Onodera H. An investigation of the phase diagram of the Ir–Al binary system. Intermetallics. 2008;16(10):1171.

    Article  Google Scholar 

  4. Lu P, Shen CY, Qiu T. Study on microstructure and emission properties of Ba–W cathodes doped with CeO2. Rare Met. 2008;32(1):50.

    Google Scholar 

  5. Isagawa S, Highchi T, Kobayashi K, Miyake S, Ohya K, Youshida M. Application of M-type cathodes to high-power cw klystrons. Appl Surf Sci. 1999;146(1–4):89.

    Article  Google Scholar 

  6. Zhang HL, Liu YW, Zhang MC, Li YT. Emission and surface characteristic of ternary alloy Ir/Re/W-coated impregnated tungsten cathodes. Appl Surf Sci. 2005;251(1–4):130.

    Article  Google Scholar 

  7. Li J, Yu ZQ, Shao WS, Zhang K, Gao YJ. High current density M-type cathode for vacuum electron devices. Appl Surf Sci. 2005;251(1–4):151.

    Article  Google Scholar 

  8. Zhang HW, Shi SM, Bai ZG, Ding YG. The development of cathode technology in Russia. Vac Electron. 2003;72(5):117.

    Google Scholar 

  9. Yin SY, Zhang HL, Wang Y, Zhang MC, Tian H. Progress in large current density M-type cathode. In: The Sixteenth Annual Conference of the Military Microwave Tube Symposium, 2007;8:338.

  10. Yan X, Zhang QY, Lu JH, Zhao W. Recent progress in preparation and application for iridium/oxide films. Rare Met. 2004;28(4):757.

    Google Scholar 

  11. Shen CY, Qiu T, Li XY. Advances in dispenser cathodes materials with high properties. Mater Rev. 2005;19(3):25.

    Google Scholar 

  12. Yamabe-Mitarai Y, Aoki H, Hill P, Harada H. High-temperature mechanical properties of Ir–Al alloys. Scripta Mater. 2003;48(5):565.

    Article  Google Scholar 

  13. Danzaki Y. Quantitative analysis of several kinds of Ir–Al alloys by ICP–OES. Bunseki Kagaku. 2002;51(10):983.

    Article  Google Scholar 

  14. Katrych SO, Petyukh VM, Bondar AA. Phase relations in the Al–Ir–Os system in the range up to 70 at% Al. Powder Metall Met Ceram. 2007;46(7–8):357.

    Article  Google Scholar 

  15. Xiang DD, Ding L. New technologies of sintering W–Ni–Fe heavy alloys. Rare Met. 2013;37(1):155.

    Google Scholar 

  16. Guo ZZ, Sun Y, Duan YH, Peng MJ, Wu DP, Liu GT. Structure and properties of Cu/Mo nanostructure multilayer deposited by magnetron sputtering. Rare Met. 2012;36(1):92.

    Google Scholar 

Download references

Acknowledgments

This work was financially supported by the Special Fund Project for Technology Research and Development of Scientific Research Institute (No. 2012EG115001).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Yang Xia.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Xia, Y., Xie, YF., Jiang, H. et al. Preparation and properties of Os–Ir–Al alloy for impregnated tungsten cathodes. Rare Met. 32, 564–568 (2013). https://doi.org/10.1007/s12598-013-0086-1

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s12598-013-0086-1

Keywords

Navigation