Abstract
Refractory high-entropy alloys (RHEAs) are new types of material that have been developed for high-temperature applications. RHEAs should have enhanced high-temperature strength while maintaining a sufficient level of room-temperature toughness. The phase evolution of novel MoNbSiTiW RHEAs was investigated after mechanical alloying (MA) for 35 h. X-ray diffraction (XRD) was used to analyze the phase evolution, and analysis of particle morphologies was done using a scanning electron microscope (SEM) equipped with energy dispersive spectroscopy (EDS). XRD results indicate that NbMoSiTiW RHEAs with up to 10 h of mechanical alloying have a stable solid solution phase with body centered cubic (BCC) structure. Further milling of NbMoSiTiW RHEAs promotes the evolution of intermetallic compounds until 35 h of mechanical alloying. The Williamson-Hall process was incorporated for crystalline size and lattice strain measurement and the results show that, after 35 h of mechanical alloying, the crystalline size decreased from 298 nm to 25 nm, and an enhancement in lattice strain was observed from 0.1% to 0.65%.
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Acknowledgements
The authors would like to thank the All-India Council for Technical Education (referred to as AICTE, New Delhi), India, for funding the present work under the Research Promotion scheme (RPS) project no: 8-98/FDC/RPS (POLICY -1)/2019-20.
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Prakash, O., Chandrakar, R., Chandraker, S. et al. Phase Evolution of Novel MoNbSiTiW Refractory High-Entropy Alloy Prepared by Mechanical Alloying. JOM 74, 3329–3333 (2022). https://doi.org/10.1007/s11837-022-05417-7
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DOI: https://doi.org/10.1007/s11837-022-05417-7