Abstract
Liquid-metal-mediated recrystallization is a poorly understood facet of liquid metal embrittlement that has never before been the subject of systematic study. In this work, commercially pure Zn sheet with varied grain size and amount of prior deformation is exposed to liquid eutectic Ga-In, and the resulting microstructural evolution is characterized. The penetration rate of the liquid into the grain boundary network is observed to be strongly dependent on grain size, with little or no dependence on prior deformation. However, the extent of recrystallization and the accompanying evolution of crystallographic and morphologic texture is strongly dependent on prior deformation.
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Acknowledgements
The authors thank M.D. Dickey for highly productive discussions throughout this project. This work is partially supported by the National Science Foundation award no. DMR-1842650. This work was performed in part at the Analytical Instrumentation Facility (AIF) at North Carolina State University, which is supported by the State of North Carolina and the National Science Foundation (award no. ECCS-1542015). The AIF is a member of the North Carolina Research Triangle Nanotechnology Network (RTNN), a site in the National Nanotechnology Coordinated Infrastructure (NNCI).
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Norkett, J.E., Miller, V.M. Liquid-Metal-Mediated Recrystallization of Zinc Under Ambient Conditions. JOM 72, 860–867 (2020). https://doi.org/10.1007/s11837-019-03954-2
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DOI: https://doi.org/10.1007/s11837-019-03954-2