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Multiscale Characterization of Microstructure in Near-Surface Regions of a 16MnCr5 Gear Wheel After Cyclic Loading

  • 3D Nanoscale Characterization of Metals, Minerals, and Materials
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Abstract

The dependence of the microstructure on the degree of deformation in near-surface regions of a 16MnCr5 gear wheel after 2.1 × 106 loading cycles has been investigated by x-ray diffraction analysis, transmission electron microscopy, and atom probe tomography. Retained austenite and large martensite plates, along with elongated lamella-like cementite, were present in a less deformed region. Comparatively, the heavily deformed region consisted of a nanocrystalline structure with carbon segregation up to 2 at.% at grain boundaries. Spheroid-shaped cementite, formed at the grain boundaries and triple junctions of the nanosized grains, was enriched with Cr and Mn but depleted with Si. Such partitioning of Cr, Mn, and Si was not observed in the elongated cementite formed in the less deformed zone. This implies that rolling contact loading induced severe plastic deformation as well as a pronounced annealing effect in the active contact region of the toothed gear during cyclic loading.

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References

  1. P. Fernandes and C. McDuling, Eng. Fail. Anal. 4, 99 (1997).

    Article  Google Scholar 

  2. A. Voskamp, R. Österlund, P. Becker, and O. Vingsbo, Met. Technol. 7, 14 (1980).

    Article  Google Scholar 

  3. M. Li, Gear Technology (March/April 2016), pp. 56–61.

  4. J.R. Davis, Surface Hardening of Steels: Understanding the Basics (Materials Park: ASM International, 2002).

    Google Scholar 

  5. J. Goldstein and A. Moren, Metall. Trans. A 9, 1515 (1978).

    Article  Google Scholar 

  6. M. Lias, T. Rao, M. Awang, and M. Khan, J. Appl. Sci. 12, 2404 (2012).

    Article  Google Scholar 

  7. J. Takahashi, K. Kawakami, and M. Ueda, Acta Mater. 58, 3602 (2010).

    Article  Google Scholar 

  8. J.H. Kang, B. Hosseinkhani, C.A. Williams, M.P. Moody, P.A.J. Bagot, and P.E.J. Rivera-Díaz-del-Castillo, Scr. Mater. 69, 630 (2013).

    Article  Google Scholar 

  9. Y. Li, M. Herbig, S. Goto, and D. Raabe, Mater. Charact. 123, 349 (2017).

    Article  Google Scholar 

  10. Y. Li, M. Herbig, S. Goto, and D. Raabe, Mater. Sci. Technol. 32, 1100 (2016).

    Article  Google Scholar 

  11. B. Behrens and D. Odening, Int. J. Mater. Form. 2, 125 (2009).

    Article  Google Scholar 

  12. K. Thompson, D. Lawrence, D. Larson, J. Olson, T. Kelly, and B. Gorman, Ultramicroscopy 107, 131 (2007).

    Article  Google Scholar 

  13. A. Stormvinter, P. Hedström, and A. Borgenstam, Mater. Sci. Technol. 29, 373 (2013).

    Article  Google Scholar 

  14. R. Valiev, A. Korznikov, and R. Mulyukov, Mater. Sci. Eng. A 168, 141 (1993).

    Article  Google Scholar 

  15. M.P. Moody, F. Tang, B. Gault, S.P. Ringer, and J.M. Cairney, Ultramicroscopy 111, 493 (2011).

    Article  Google Scholar 

  16. Y. Li, D. Raabe, M. Herbig, P.-P. Choi, S. Goto, A. Kostka, H. Yarita, C. Borchers, and R. Kirchheim, Phys. Rev. Lett. 113, 106104 (2014).

    Article  Google Scholar 

  17. Y. Li, P. Choi, S. Goto, C. Borchers, D. Raabe, and R. Kirchheim, Acta Mater. 60, 4005 (2012).

    Article  Google Scholar 

  18. Y.J. Li, P. Choi, S. Goto, C. Borchers, D. Raabe, and R. Kirchheim, Ultramicroscopy 132, 233 (2013).

    Article  Google Scholar 

  19. Y. Li, A. Kostka, P. Choi, S. Goto, D. Ponge, R. Kirchheim, and D. Raabe, Acta Mater. 84, 110 (2015).

    Article  Google Scholar 

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Acknowledgements

The authors would like to thank Prof. Tenberge and Mr. Gondecki from Ruhr University Bochum for providing the gear wheel, and Ms. Susanne Jordans for assistance with XRD sample preparation.

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Correspondence to Tong Li.

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Medghalchi, S., Jamebozorgi, V., Bala Krishnan, A. et al. Multiscale Characterization of Microstructure in Near-Surface Regions of a 16MnCr5 Gear Wheel After Cyclic Loading. JOM 70, 1758–1764 (2018). https://doi.org/10.1007/s11837-018-2931-z

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  • DOI: https://doi.org/10.1007/s11837-018-2931-z

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